As a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences,
Cas:62932-94-9
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inquiryPurity: 99.0% up; Stable supply with over 100kg annually; Appearance:colorless transpartent liquid Storage:room temprature Package:25kg/drum Application:Organic Building Block Port:Beijing/Shanghai/Shenzhen/Hangzhou
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Type:Trading Company
inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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Min.Order:1 Kilogram
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Type:Manufacturers
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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FOB Price: $1.0 / 2.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:62932-94-9
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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Min.Order:10 Kilogram
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Type:Trading Company
inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
Cas:62932-94-9
Min.Order:1 Kilogram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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Type:Lab/Research institutions
inquiry2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE CAS:62932-94-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, spec
Cas:62932-94-9
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:62932-94-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: 2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE Synonyms: 2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE;2-Bromo-4-hydroxy-3-(hydroxymethyl)acetophenone;Ethanone, 2-broMo-1-[4-hydroxy-3-(hydroxyMethyl)phenyl]-;2-
Cas:62932-94-9
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and quality c
Cas:62932-94-9
Min.Order:100 Metric Ton
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Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:62932-94-9
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:62932-94-9
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:62932-94-9
Min.Order:100 Gram
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Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:62932-94-9
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:62932-94-9
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:62932-94-9
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:62932-94-9
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m
Cas:62932-94-9
Min.Order:1 Kilogram
FOB Price: $8.2 / 8.8
Type:Trading Company
inquiryProduct Name: 2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE Synonyms: 2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE;2-Bromo-4-hydroxy-3-(hydroxymethyl)acetophenone;Ethanone, 2-broMo-1-[4-hydroxy-3-(hydroxyMethyl)phenyl]-;2-br
Cas:62932-94-9
Min.Order:1 Kilogram
FOB Price: $230.0
Type:Lab/Research institutions
inquiryProduct name: 2-Bromo-1-[4-Hydroxy-3-(Hydroxymethyl)Phenyl]Ethanone CAS No.:62932-94-9 Molecule Formula:C9H9BrO3 Molecule Weight:245.07 Purity: 98% Package: 25kg/drum Description:White to off-white powder Manufacture Standards:Enterprise Stand
Cas:62932-94-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:62932-94-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:62932-94-9
Min.Order:0
Negotiable
Type:Trading Company
inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)
Cas:62932-94-9
Min.Order:1 Gram
Negotiable
Type:Trading Company
inquiry2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE Basic information Product Name: 2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE Synonyms: 2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE;2-Bromo-4-hydroxy-3-(hydroxyme
Cas:62932-94-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:62932-94-9
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:62932-94-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry5-(2-bromoacetyl)-2-hydroxybenzaldehyde
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Stage #1: 5-(2-bromoacetyl)-2-hydroxybenzaldehyde With propionic acid In tetrahydrofuran at 5 - 10℃; for 0.5h; Stage #2: With sodium tetrahydroborate In tetrahydrofuran at 0 - 5℃; for 1h; Solvent; Reagent/catalyst; | 94% |
With sodium tetrahydroborate; acetic acid at 0 - 20℃; Inert atmosphere; | 88% |
With sodium tetrahydroborate; acetic acid at 8 - 20℃; | 85% |
With sodium tetrahydroborate; acetic acid at 10℃; for 1h; | 85% |
With sodium tetrahydroborate; acetic acid at 25℃; for 1h; | 80% |
3'-acetoxymethyl-4'-acetoxy-2-bromoacetophenone
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
With hydrogen bromide In tetrahydrofuran at 75℃; | |
With hydrogen bromide In methanol; water | |
With hydrogen bromide In methanol; water |
4'-acetoxy-3'-(acetoxymethyl)acetophenone
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: polyvinylpyridinium bromide perbromide resin / CH2Cl2 2: 1N HBr / tetrahydrofuran / 75 °C View Scheme |
4-Hydroxyacetophenone
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: resin-bound piperazinomethylpolystyrene / H2O; tetrahydrofuran 1.2: 14 percent / pTSA / toluene / 110 °C 2.1: polyvinylpyridinium bromide perbromide resin / CH2Cl2 3.1: 1N HBr / tetrahydrofuran / 75 °C View Scheme |
salicylaldehyde
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aluminum (III) chloride / dichloromethane / 15 h / Reflux 2: sodium tetrahydroborate; acetic acid / 1 h / 10 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: aluminum (III) chloride / dichloromethane / 0.5 h / 50 °C 1.2: 12 h / 40 °C 2.1: sodium tetrahydroborate; acetic acid / 0 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: aluminum (III) chloride / dichloromethane / 0.5 h / 10 - 30 °C 1.2: 24 h / 35 °C 2.1: acetic acid; sodium tetrahydroborate / 1 h / 25 °C View Scheme |
2-Methoxypropene
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
2-bromo-1-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethanone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In dichloromethane at 0℃; for 0.666667h; | 100% |
With resin-SO3H In dichloromethane | |
With toluene-4-sulfonic acid In tetrahydrofuran at -10 - 10℃; for 1h; |
2,2-dimethoxy-propane
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
2-bromo-1-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethanone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In dichloromethane | 99% |
With toluene-4-sulfonic acid In dichloromethane at 20℃; | 84% |
In dichloromethane at 20℃; for 10h; | 82% |
2-Methoxypropene
N-tert-butylbenzylamine
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Stage #1: 2-Methoxypropene; 2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone With toluene-4-sulfonic acid In acetone at 0 - 5℃; for 1h; Stage #2: N-tert-butylbenzylamine In acetone at 55℃; for 22h; | 80% |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: resin-SO3H / CH2Cl2 2.1: resin-N(iPr)2 / tetrahydrofuran 3.1: CaCl2 / methanol / 0.17 h / 0 °C 3.2: 76 percent / resin-NMe3(1+)*BH4(1-) / methanol / 2 h / 0 - 20 °C 4.1: (polystyrylmethyl)trimethylammonium cyanoborohydride; AcOH / CH2Cl2 4.2: 98 percent / resin-NMe3(1+)*NaCO3(1-) / CH2Cl2 5.1: H2 / Pd(OH)2/C / ethyl acetate / 2 h 5.2: 87 percent / SCX-2 View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
(1'S)-1-(2,2-dimethyl-4H-benzo[1,3]dioxin-6-yl)-2-(2-hydroxy-1-phenyl-ethylamino)-ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: resin-SO3H / CH2Cl2 2: resin-N(iPr)2 / tetrahydrofuran View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
(1R,1'S)-1-(2,2-dimethyl-4H-benzo[1,3]dioxin-6-yl)-2-(2-hydroxy-1-phenyl-ethylamino)-ethanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: resin-SO3H / CH2Cl2 2.1: resin-N(iPr)2 / tetrahydrofuran 3.1: CaCl2 / methanol / 0.17 h / 0 °C 3.2: 76 percent / resin-NMe3(1+)*BH4(1-) / methanol / 2 h / 0 - 20 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
(1R,1'S)-1-(2,2-dimethyl-4H-benzo[1,3]dioxin-6-yl)-2-{(2-hydroxy-1-phenyl-ethyl)-[6-(4-phenyl-butoxy)-hexyl]-amino}-ethanol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: resin-SO3H / CH2Cl2 2.1: resin-N(iPr)2 / tetrahydrofuran 3.1: CaCl2 / methanol / 0.17 h / 0 °C 3.2: 76 percent / resin-NMe3(1+)*BH4(1-) / methanol / 2 h / 0 - 20 °C 4.1: (polystyrylmethyl)trimethylammonium cyanoborohydride; AcOH / CH2Cl2 4.2: 98 percent / resin-NMe3(1+)*NaCO3(1-) / CH2Cl2 View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: resin-SO3H / CH2Cl2 2.1: resin-N(iPr)2 / tetrahydrofuran 3.1: CaCl2 / methanol / 0.17 h / 0 °C 3.2: 76 percent / resin-NMe3(1+)*BH4(1-) / methanol / 2 h / 0 - 20 °C 4.1: H2 / Pd(OH)2/C / ethyl acetate View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
(1S)-2-amino-1-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)ethanol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: 94 percent / Pichia angusta / acetonitrile / 48 h / 28 °C 4: 86 percent / H2 / Pd/C / ethanol / 3 h View Scheme | |
Multi-step reaction with 4 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: Mucor racemosus / 42 h 4: 86 percent / H2 / Pd/C / ethanol / 3 h View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
2-azido-1-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
(1S)-2-azido-1-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)ethanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: 94 percent / Pichia angusta / acetonitrile / 48 h / 28 °C View Scheme | |
Multi-step reaction with 3 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: Mucor racemosus / 42 h View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
(1R)-2-AZIDO-1-(2,2-DIMETHYL-4H-1,3-BENZODIOXIN-6-YL)ETHANOL
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: Mucor racemosus / 42 h View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
(1S)-1-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-{[6-(4-phenylbutoxy)hexyl]amino}ethanol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: 94 percent / Pichia angusta / acetonitrile / 48 h / 28 °C 4: 86 percent / H2 / Pd/C / ethanol / 3 h 5: 70 percent / dimethylformamide / 67 h / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: Mucor racemosus / 42 h 4: 86 percent / H2 / Pd/C / ethanol / 3 h 5: 70 percent / dimethylformamide / 67 h / 20 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: 94 percent / Pichia angusta / acetonitrile / 48 h / 28 °C 4: 86 percent / H2 / Pd/C / ethanol / 3 h 5: 70 percent / dimethylformamide / 67 h / 20 °C 6: 100 percent / H2O / 0.5 h / 71 °C View Scheme | |
Multi-step reaction with 6 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: Mucor racemosus / 42 h 4: 86 percent / H2 / Pd/C / ethanol / 3 h 5: 70 percent / dimethylformamide / 67 h / 20 °C 6: 100 percent / H2O / 0.5 h / 71 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: 94 percent / Pichia angusta / acetonitrile / 48 h / 28 °C 4: 86 percent / H2 / Pd/C / ethanol / 3 h 5: dimethylformamide / 67 h / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: 100 percent / TsOH*H2O / CH2Cl2 / 0.67 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 2 h / 20 °C 3: Mucor racemosus / 42 h 4: 86 percent / H2 / Pd/C / ethanol / 3 h 5: dimethylformamide / 67 h / 20 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
3-(3-(2-(tert-butyldimethylsilyloxy)-2-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethylamino)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
3-(4-(2-(tert-butyldimethylsilyloxy)-2-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethylamino)butoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
3-(5-(2-(tert-butyldimethylsilyloxy)-2-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethylamino)pentyloxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
3-(6-(2-(tert-butyldimethylsilyloxy)-2-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethylamino)hexyloxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C 5: ammonium fluoride / water; ethanol / 48 h / 45 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C 5: ammonium fluoride / water; ethanol / 48 h / 45 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C 5: ammonium fluoride / water; ethanol / 48 h / 45 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C 5: ammonium fluoride / water; ethanol / 48 h / 45 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
C25H27Cl2N3O6
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C 5: ammonium fluoride / water; ethanol / 48 h / 45 °C 6: hydrogenchloride / water; ethanol / 12 h / 20 °C View Scheme |
2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
C26H29Cl2N3O6
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: dichloromethane / 10 h / 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C 4: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C 5: ammonium fluoride / water; ethanol / 48 h / 45 °C 6: hydrogenchloride / water; ethanol / 12 h / 20 °C View Scheme |
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