Product name :(1S,5R)-1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one CAS:63106-93-4 We are also manufacture and supply below milnacipran intermediates with high quality ,competitive price and best service. (1S,5R)-1-phenyl-3-oxa-bi
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inquiryName (1S,5R)-1-Phenyl-3-oxabicyclo[3.1.0]hexan-2-one Molecular Structure Molecular Formula C11H10O2 Molec
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inquiryName: (1S,5R)-1-Phenyl-3-oxabicyclo[3.1.0]hexan-2-one Molecular Formula:C11H10O2 Molecular Weight:174.2 CAS No.:63106-93-4 Appearance:Similar White To Slight Yellow Powder Appearance:Similar White To Slight Yellow Powder Storage:Store in cool and
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiry(1S,5R)-1-PHENYL-3-OXA-BICYCLO[3.1.0]HEXAN-2-ONE CAS:63106-93-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing
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inquiryProduct Name: (1S,5R)-1-PHENYL-3-OXA-BICYCLO[3.1.0]HEXAN-2-ONE Synonyms: (1S,5R)-1-PHENYL-3-OXA-BICYCLO[3.1.0]HEXAN-2-ONE;2-Oxo-1-phenyl-3-oxabicyclo[3.1.0]-hexane;1-Phenyl-3-oxabicyclo[3.1.0]hexan-2-one;(1R,2S)-rel-2-Oxo-1-phenyl-3-oxabicyclo[3
Cas:63106-93-4
Min.Order:100 Gram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:63106-93-4
Min.Order:10 Gram
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inquiryProduct name: 2-Oxo-1-Phenyl-3-Oxbicyclo[3.1.0]-Hexane CAS No.:63106-93-4 Molecule Formula:C11H10O2 Molecule Weight:174.20 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard
Cas:63106-93-4
Min.Order:1 Kilogram
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:63106-93-4
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inquiry(1S,5R)-1-PHENYL-3-OXA-BICYCLO[3.1.0]HEXAN-2-ONE Chemical Properties Melting point 49-50 °C Boiling point 119 °C(Press: 0.1 Torr) density 1.300±0.06 g/cm3(Predicted)
Cas:63106-93-4
Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryProduct Name: (1S,5R)-1-PHENYL-3-OXA-BICYCLO[3.1.0]HEXAN-2-ONE Synonyms: (1S,5R)-1-PHENYL-3-OXA-BICYCLO[3.1.0]HEXAN-2-ONE;2-Oxo-1-phenyl-3-oxabicyclo…Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:aluminum foil bag,carton
Cas:63106-93-4
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
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inquiryallyl α-phenyl-α-diazoacetate
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
With dirhodium(II) tetrakis[methyl2-oxaazetidine-4(S)carboxylate] In dichloromethane for 0.5h; Cyclization; Heating; | 80% |
With dirhodium tetraacetate; trimethylsilylazide In dichloromethane at 40℃; for 1h; Reagent/catalyst; | 78% |
phenylacetonitrile
epichlorohydrin
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
Stage #1: phenylacetonitrile; epichlorohydrin With sodium hydride In N,N'-dimethylimidazolidinone; toluene at 10 - 20℃; Stage #2: With potassium hydroxide; tetrabutylammonium sulfate In water; toluene Heating / reflux; Stage #3: With hydrogenchloride In water; toluene at 60 - 70℃; for 2h; | 68.1% |
Stage #1: phenylacetonitrile With sodium hydride In 1,3-dimethyl-2-imidazolidinone; toluene at 10 - 20℃; for 2h; Stage #2: epichlorohydrin In 1,3-dimethyl-2-imidazolidinone; toluene at 10 - 20℃; Stage #3: With hydrogenchloride; potassium hydroxide; tetrabutylammonium sulfate more than 3 stages; | 68.1% |
Stage #1: phenylacetonitrile With sodium amide In benzene at 35℃; for 3h; Cooling with ice; Stage #2: epichlorohydrin In benzene at 35℃; for 4h; Cooling with ice; Stage #3: With potassium hydroxide In ethanol; water for 16.5h; Reflux; | |
Stage #1: phenylacetonitrile at 0 - 20℃; for 3h; Stage #2: epichlorohydrin at 0 - 20℃; for 4h; Stage #3: With potassium hydroxide In ethanol; water Reflux; | 14.5 g |
epichlorohydrin
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
Stage #1: phenylacetonitrile With sodium hydride In 1,3-dimethyl-2-imidazolidinone; toluene at 10 - 20℃; for 2h; Stage #2: epichlorohydrin In 1,3-dimethyl-2-imidazolidinone; toluene at 10 - 20℃; Stage #3: With hydrogenchloride; potassium hydroxide; tetrabutylammonium sulfate more than 3 stages; | 68.1% |
phenyl toluenesulfonamide
allyl α-phenyl-α-diazoacetate
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
With dirhodium tetraacetate In dichloromethane at 23℃; | 64% |
6a-Phenyl-3a,6a-dihydro-3H-furo[3,4-c]pyrazole-4,6-dione
A
4-methyl-3-phenyl-2,5-dihydrofuran-2-one
B
3-methyl-4-phenylfuran-2(5H)-one
C
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
D
5-phenyl-3-oxabicyclo<3.1.0>hexan-2-one
Conditions | Yield |
---|---|
With sodium tetrahydroborate 1.) benzene, 70 deg C, 2.) THF, 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given; |
allyl phenylacetate
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 74 percent / 1,8-diazobicyclo[5.4.0]undec-7-ene; p-acetamidobenzenesulfonyl azide / tetrahydrofuran / 11 h / 20 °C 2: 80 percent / dirhodium(II) tetrakis[methyl2-oxaazetidine-4(S)carboxylate] / CH2Cl2 / 0.5 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1.1: 4-acetamidobenzenesulfonyl azide / acetonitrile / 0.25 h / Inert atmosphere; Cooling with ice 1.2: 16 h / 20 °C / Inert atmosphere 2.1: dirhodium tetraacetate; trimethylsilylazide / dichloromethane / 1 h / 40 °C View Scheme |
phenylacetyl chloride
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Et3N 2: 74 percent / 1,8-diazobicyclo[5.4.0]undec-7-ene; p-acetamidobenzenesulfonyl azide / tetrahydrofuran / 11 h / 20 °C 3: 80 percent / dirhodium(II) tetrakis[methyl2-oxaazetidine-4(S)carboxylate] / CH2Cl2 / 0.5 h / Heating View Scheme |
A
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium pivalate In dimethyl sulfoxide; toluene at 140℃; for 16h; Inert atmosphere; | A 21 %Spectr. B 48 %Spectr. |
A
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diisobutylaluminium hydride / tetrahydrofuran / 16 h / 0 °C 2: tetrakis(triphenylphosphine) palladium(0); potassium pivalate / toluene; dimethyl sulfoxide / 16 h / 140 °C / Inert atmosphere View Scheme |
(±)-methyl 2-(2-bromophenyl)propanoate
A
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C 1.2: 16 h / -78 - 20 °C 2.1: diisobutylaluminium hydride / tetrahydrofuran / 16 h / 0 °C 3.1: tetrakis(triphenylphosphine) palladium(0); potassium pivalate / toluene; dimethyl sulfoxide / 16 h / 140 °C / Inert atmosphere View Scheme |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
With hydrogen bromide at 80℃; for 2h; | 98% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(1S,2R)/(1R,2S)-2-(bromomethyl)-1-phenylcyclopropanecarboxylic acid
Conditions | Yield |
---|---|
With hydrogen bromide In acetic acid at 80℃; for 2h; | 96% |
With hydrogen bromide In acetic acid at 80℃; for 2h; |
Conditions | Yield |
---|---|
With thionyl chloride at 20℃; for 10h; Temperature; | 94.5% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
diethylamine
Conditions | Yield |
---|---|
Stage #1: 1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one; diethylamine With sodium methylate In methanol; toluene at 20 - 30℃; for 8h; Stage #2: With water; acetic acid In methanol; toluene | 93.8% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
ethanol
ethyl (+/-)-cis-2-(bromomethyl)-1-phenylcyclopropanecarboxylate
Conditions | Yield |
---|---|
With dibromo sulfoxide at -15 - 20℃; | 90% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
diethylamine
Conditions | Yield |
---|---|
With sodium methylate In methanol; toluene at 20 - 30℃; for 15h; Product distribution / selectivity; | 87% |
With sodium methylate In toluene at 60℃; for 15h; Product distribution / selectivity; | |
With sodium methylate In methanol at 20 - 60℃; for 15h; Product distribution / selectivity; |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(1R,2S)-1-phenyl-2-(hydroxymethyl)-N,N-diethylcyclopropanecarboxamide
Conditions | Yield |
---|---|
Stage #1: diethylamine With n-butyllithium In tetrahydrofuran; hexane at -75℃; for 1h; Stage #2: 1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one In tetrahydrofuran; hexane at -78 - -60℃; Stage #3: With water; ammonium chloride In tetrahydrofuran; hexane | 66.8% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
potassium phtalimide
(Z)-1-phenyl-2-(phthalimidomethyl)cyclopropanecarboxylic acid
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 15h; Heating; | 57% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
potassium phtalimide
Conditions | Yield |
---|---|
Stage #1: 1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one; potassium phtalimide In dimethyl sulfoxide at 150℃; for 20h; Stage #2: With acetic acid pH=5 - 6; Product distribution / selectivity; | 51% |
Stage #1: 1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one; potassium phtalimide With tetra-(n-butyl)ammonium iodide In 1-methyl-pyrrolidin-2-one at 150℃; for 20h; Stage #2: With acetic acid pH=5 - 6; Product distribution / selectivity; | > 90 %Chromat. |
Stage #1: 1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one; potassium phtalimide In 1-methyl-pyrrolidin-2-one at 150℃; for 20h; Stage #2: With acetic acid pH=5 - 6; Product distribution / selectivity; | > 90 %Chromat. |
Stage #1: 1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one; potassium phtalimide In DMF (N,N-dimethyl-formamide) at 50 - 150℃; for 20 - 24h; Stage #2: With acetic acid pH=5 - 6; Product distribution / selectivity; | 70 - > 90 %Chromat. |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
1,2-diphenyl-2-hydroxy-3-oxabicyclo <3,1,0> hexane
Conditions | Yield |
---|---|
In diethyl ether for 1.5h; Heating; | 47% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With 2-hydroxypyridin In toluene for 24h; Heating; | A 33% B 32% |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
B
(1S,5R)-1-phenyl-3-oxabicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
With Cunninghamella blakesleeana; water In N,N-dimethyl-formamide at 30℃; for 41h; biohydrolysis, pH 8; | A n/a B 32% |
NH-pyrazole
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(1R,2S)-1-Phenyl-2-pyrazol-1-ylmethyl-cyclopropanecarboxylic acid
Conditions | Yield |
---|---|
With sodium hydride 1.) DMF, 60 deg C, 1 h, 2.) DMF, 60 deg C, 5 h; Yield given. Multistep reaction; |
2-methyl-1H-pyrrole
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(1S,2R)-2-(2-Methyl-pyrrol-1-ylmethyl)-1-phenyl-cyclopropanecarboxylic acid
Conditions | Yield |
---|---|
With sodium hydride 1.) DMF, 60 deg C, 1 h, 2.) DMF, 60 deg C, 5 h; Yield given. Multistep reaction; |
indole
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(1R,2S)-2-Indol-1-ylmethyl-1-phenyl-cyclopropanecarboxylic acid
Conditions | Yield |
---|---|
With sodium hydride 1.) DMF, 60 deg C, 1 h, 2.) DMF, 60 deg C, 5 h; Yield given. Multistep reaction; |
methanol
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(+/-)-methyl cis-2-(bromomethyl)-1-phenylcyclopropanecarboxylate
Conditions | Yield |
---|---|
With dibromo sulfoxide at -15 - 20℃; |
propan-1-ol
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
n-propyl (1R,2S/1S,2R)-2-(chloromethyl)-1-phenylcyclopropanecarboxylate
Conditions | Yield |
---|---|
With thionyl chloride at -15 - 20℃; |
3-Methylindole
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(1S,2R)-2-(3-Methyl-indol-1-ylmethyl)-1-phenyl-cyclopropanecarboxylic acid
Conditions | Yield |
---|---|
With sodium hydride 1.) DMF, 60 deg C, 1 h, 2.) DMF, 60 deg C, 5 h; Yield given. Multistep reaction; |
pyrrole
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
(1R,2S)-1-Phenyl-2-pyrrol-1-ylmethyl-cyclopropanecarboxylic acid
Conditions | Yield |
---|---|
With sodium hydride 1.) DMF, 60 deg C, 1 h, 2.) DMF, 60 deg C, 5 h; Yield given. Multistep reaction; |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
isopropyl alcohol
(Z)-isopropyl 1-phenyl-2-(phthalimidomethyl)cyclopropanecarboxylate
Conditions | Yield |
---|---|
With thionyl chloride at -15 - 20℃; |
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
diethylamine
(1 S,2 R)-N,N-diethyl-2-(hydroxymethyl)-1-phenylcyclopropane-carboxamide
Conditions | Yield |
---|---|
With n-butyllithium 1) THF, hexane, 0 - -78 deg C; 2) THF, hexane, -78 deg C, 2 h; Yield given. Multistep reaction; |
methanol
1-phenyl-3-oxa-bicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
With thionyl chloride; zinc(II) chloride In benzene |
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