Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:637-53-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:637-53-6
Min.Order:1 Gram
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Type:Manufacturers
inquiryHigh purity CAS 637-53-6 THIOACETANILIDE in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (Fluorene,Ca
Cas:637-53-6
Min.Order:1 Gram
FOB Price: $100.0
Type:Lab/Research institutions
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Cas:637-53-6
Min.Order:1 Kilogram
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Type:Trading Company
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Cas:637-53-6
Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:637-53-6
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Cas:637-53-6
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Ethanethioamide,N-phenyl- cas 637-53-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the N-Phenylethanthioamid, CAS:637-53-6 with the most competitive price and the best qual
CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio
Conditions | Yield |
---|---|
In dichloromethane for 3h; Ambient temperature; | A n/a B 100% |
Conditions | Yield |
---|---|
With 2,4-bis(4-(5,5,6,6,7,7,8,8,9,9,10,10,10-tridecafluorodecyloxy)phenyl)-1,3,2,4-dithiadiphosphetane 2,4-disulfide In tetrahydrofuran at 55℃; for 6h; | 97% |
With 2,4-{[3-[(CH2)5C8F17]-4-MeO-phenyl]}2-P2S2 2,4-disulfide for 0.05h; microwave irradiation; | 96% |
With Lawessons reagent for 0.0333333h; microwave irradiation; | 96% |
Conditions | Yield |
---|---|
Stage #1: acetophenone oxime With triethylamine; p-toluenesulfonyl chloride In acetonitrile at 0 - 20℃; Inert atmosphere; Stage #2: With thiourea In acetonitrile for 2h; Reflux; Inert atmosphere; | 90% |
With tetraphosphorus decasulfide In benzene at 80℃; for 0.5h; Beckmann Rearrangement; | 90% |
With trichlorothiophosphine; water; triethylamine at 0 - 75℃; Beckmann rearrangement; chemoselective reaction; | 78% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate; O,O-Diethyl hydrogen phosphorodithioate In 1,4-dioxane at 80 - 90℃; for 2h; Inert atmosphere; | 89% |
aniline
Thioacetic acid S-(5,5-dimethyl-2-thioxo-2λ5-[1,3,2]dioxaphosphinan-2-yl) ester
thioacetanilide
Conditions | Yield |
---|---|
Stage #1: Thioacetic acid S-(5,5-dimethyl-2-thioxo-2λ5-[1,3,2]dioxaphosphinan-2-yl) ester With 5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane In benzene for 3h; Heating; Stage #2: aniline With triethylamine In benzene cooling; Further stages.; | 87.8% |
Conditions | Yield |
---|---|
With 1H-imidazole; iodine; chloro-diphenylphosphine In dichloromethane for 0.75h; Reflux; | 85% |
With 1,2-bis(5-methylisoxazol-3-yl)hydrazine; triphenylphosphine In acetonitrile for 4.5h; Mitsunobu reaction; Reflux; | 83% |
morpholine
2-thioxo-4-thiazolidinone
Acetanilid
A
2-morpholin-4-yl-2-thiazole-4(5H)-one
B
thioacetanilide
Conditions | Yield |
---|---|
With MCM-41 mesoporous silica In ethanol; water at 80 - 90℃; for 8h; Green chemistry; | A n/a B 70% |
Conditions | Yield |
---|---|
In tetrahydrofuran; diethyl ether at -78℃; for 0.5h; | 70% |
Conditions | Yield |
---|---|
In dichloromethane for 120h; Ambient temperature; | A n/a B 59% |
Conditions | Yield |
---|---|
With O,O-Diethyl hydrogen phosphorodithioate In toluene for 8h; Heating; | 51% |
C16H16N2S2
thioacetanilide
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform at 5℃; for 15h; | 33% |
Lawessons reagent
N-Phenylacetohydroxamic acid
C
thioacetanilide
D
Acetanilid
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; Further byproducts given. Title compound not separated from byproducts; | A 5% B n/a C 28% D 50 % Spectr. |
(4-acetamidophenyl)disulfide
thioacetanilide
Conditions | Yield |
---|---|
at 240 - 260℃; |
N-phenyl-3-thio-malonamic acid
thioacetanilide
Conditions | Yield |
---|---|
With water Heating; | |
beim Erhitzen; |
Conditions | Yield |
---|---|
With toluene |
dithioacetic acid
phenyl isocyanate
toluene
A
carbon oxide sulfide
B
thioacetanilide
Conditions | Yield |
---|---|
methyl magnesium iodide
diethyl ether
phenyl isothiocyanate
thioacetanilide
Conditions | Yield |
---|---|
durch nachfolgende Behandlung des Reaktionspr. mit Wasser und verd. Schwefelsaeure; |
Conditions | Yield |
---|---|
With diethyl ether und Behandeln des Aetherrueckstandes mit Eiswasser und verd.Schwefelsaeure; |
Conditions | Yield |
---|---|
With toluene |
dithioacetic acid
phenyl isothiocyanate
toluene
A
carbon disulfide
B
thioacetanilide
Conditions | Yield |
---|---|
diethyl ether
N-phenylacetimidoyl chloride
thioacetamide
thioacetanilide
Conditions | Yield |
---|---|
reagiert analog mit N-Phenyl-benzimidchlorid; | |
Conditions | Yield |
---|---|
With diethyl ether |
diethyl ether
N-phenyl-benzimidoyl chloride
benzenecarbothioamide
thioacetanilide
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
With diethyl ether |
diethyl ether
N-phenylacetimidoyl chloride
benzenecarbothioamide
thioacetanilide
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
With diethyl ether |
Acetanilid
A
thioacetanilide
B
N,N'-diphenylacetamidine
Conditions | Yield |
---|---|
With tetraphosphorus decasulfide |
Conditions | Yield |
---|---|
With pyridine beim Behandeln anschliessend mit H2S; |
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
With 6H(1+)*Mo9O40PV3(6-); oxygen In acetonitrile at 60℃; under 760.051 Torr; for 0.5h; Inert atmosphere; Glovebox; | 99% |
With eosin; oxygen In N,N-dimethyl-formamide at 20℃; for 6h; Reagent/catalyst; Solvent; Irradiation; Green chemistry; | 93% |
With P,P-dichlorophenylphosphine oxide In acetonitrile at -4℃; for 3h; | 90% |
Conditions | Yield |
---|---|
In ethanol for 1h; Temperature; Solvent; Reflux; chemoselective reaction; | 99% |
In ethanol at 20℃; for 20h; | 63% |
thioacetanilide
phenylacetylene
N-phenyl-N-[(E)-2-phenylvinyl]thioacetamide
Conditions | Yield |
---|---|
With TOP; bis(2-methallyl)(cycloocta-1,5-diene)ruthenium(II) In toluene at 100℃; for 15h; Molecular sieve; Inert atmosphere; | 98% |
thioacetanilide
Methanesulfonyl azide
Conditions | Yield |
---|---|
In ethanol for 1h; Temperature; Solvent; Reflux; chemoselective reaction; | 97% |
thioacetanilide
Conditions | Yield |
---|---|
In diethyl ether under Ar atm. pentacarbonyl(3-(cyclohex-1-yl)-1-ethoxy-2-propyn-1-ylidene)tungsten was reacted with (N-phenyl)thioacetamide in diethyl ether at20°C for 25 min; ppt. was collected, washed with n-pentane and dried in vacuo; elem. anal.; | 96% |
thioacetanilide
Conditions | Yield |
---|---|
In ethanol at 20℃; for 17h; | 95% |
thioacetanilide
Conditions | Yield |
---|---|
In diethyl ether under Ar atm. pentacarbonyl(3-(cyclohex-1-yl)-1-ethoxy-2-propyn-1-ylidene)tungsten was reacted with (N-phenyl)thioacetamide in diethyl ether at20°C for 25 min; ppt. was collected, washed with n-pentane and dried in vacuo; elem. anal.; | 94% |
thioacetanilide
3,5-bis(trifluoromethyl)phenylsulfonyl azide
Conditions | Yield |
---|---|
In ethanol at 20℃; for 7h; | 93% |
1,3-diethyl 2-diazopropanedioate
thioacetanilide
diethyl 2-(1-(phenylamino)ethylidene)malonate
Conditions | Yield |
---|---|
With tris(triphenylphosphine)ruthenium(II) chloride In benzene at 90℃; for 4h; Reagent/catalyst; Time; Inert atmosphere; Sealed tube; | 92% |
With copper(I)-complexed magnetic nanoparticle catalyst In 1,2-dichloro-ethane at 70℃; for 5h; | 90% |
With (CuOTf)2*Tol In 1,2-dichloro-ethane at 90℃; for 9h; Inert atmosphere; Sealed tube; | 74% |
Conditions | Yield |
---|---|
With copper(I)-complexed magnetic nanoparticle catalyst In 1,2-dichloro-ethane at 70℃; for 3h; diastereoselective reaction; | 91% |
2-bromo-2-propenoic acid
thioacetanilide
Conditions | Yield |
---|---|
In toluene at 90℃; for 1h; | 90% |
In toluene at 90℃; |
thioacetanilide
Conditions | Yield |
---|---|
In ethanol soln. of ligand added to soln. of Rh-complex with stirring (1 h);; filtered, washed with absolute EtOH, dried in vacuo, washed with abundant pentane, elem. anal.;; | 90% |
thioacetanilide
[(Fe(CO)3)2( μ-S(CH3)C(CF3)C β (SC(NPh)Me) C α (N(CH3)2))]
Conditions | Yield |
---|---|
In tetrahydrofuran room temp., 3 hs, (Ar); filtration (celite), vac. evapn., washing (-50 °C, pentane), elem. anal.; | 90% |
thioacetanilide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane under Ar atm. pentacarbonyl(3-(cyclopent-1-yl)-1-ethoxy-2-propyn-1-ylidene)tungsten was reacted with (N-phenyl)thioacetamide in dichloromethanein the presence of 1 equiv. triethylamine with stirring for 20 min at 20°C; fast chromy. on silica; elem. anal.; | 89% |
thioacetanilide
1-chloro-1-phenyl-2,2,2-trifluoroethyl isocyanate
Conditions | Yield |
---|---|
With triethylamine In benzene for 3h; | 88% |
thioacetanilide
5-methyl-1-phenyl-1H-tetrazole
Conditions | Yield |
---|---|
With sodium azide; tetrachlorosilane In acetonitrile at 20 - 82℃; for 6h; | 87% |
N-nitrosoacetanilide
thioacetanilide
A
2,2'-dipyridyldisulphide
B
N-Phenyl-thioacetimidic acid phenyl ester
C
Acetanilid
Conditions | Yield |
---|---|
Product distribution; | A 86% B 71% C 75% |
thioacetanilide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane under Ar atm. pentacarbonyl(3-(cyclohept-1-yl)-1-ethoxy-2-propyn-1-ylidene)tungsten was reacted with (N-phenyl)thioacetamide in dichloromethanein the presence of 1 equiv. triethylamine with stirring for 20 min at 20°C; elem. anal.; | 86% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran byproducts: H2; addn. of N-phenylacetamide to a stirred suspn. of NaH (THF), filtn. of soln. into a stirred soln. of starting Rh-complex (THF, -78°C), all steps under N2; evapg. to dryness, extg. of residue (hexane), concg., cooling to 0°C, elem. anal.; | 84% |
With triethylamine In not given |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 20h; | 84% |
thioacetanilide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane under Ar atm. pentacarbonyl(3-(cyclohex-1-yl)-1-ethoxy-2-propyn-1-ylidene)tungsten was reacted with (N-phenyl)thioacetamide in dichloromethane in the presence of 1 equiv. triethylamine with stirring for 20 min at 20°C; elem. anal.; | 83% |
thioacetanilide
acetic acid hydrazide
3,5-dimethyl-4-phenyl-4H-[1,2,4]triazole
Conditions | Yield |
---|---|
With mercury(II) diacetate In tetrahydrofuran microwave irradiation; | 82% |
In butan-1-ol for 16h; Heating; Yield given; |
thioacetanilide
Conditions | Yield |
---|---|
Stage #1: thioacetanilide With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium In tetrahydrofuran at -5 - 5℃; for 1.5h; Inert atmosphere; Stage #2: (–)-menthone In tetrahydrofuran at -15 - -5℃; Inert atmosphere; stereoselective reaction; | 81% |
Conditions | Yield |
---|---|
In pyridine at 90 - 100℃; for 5h; | 79% |
In ethanol at 20℃; for 20h; | 46% |
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