CAS No.64701-47-9,1-Pyrenedecanoic acid Suppliers

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Synthetic route

: 228243-58-1
pyrenoylnonanoic acid methyl ester

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
With potassium hydroxide; hydrazine hydrate In ethylene glycol Kischner-Wolf reaction;	89%

: 70700-34-4
1-(9-carbethoxy-1-oxononanyl)pyrene

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
With potassium hydroxide; hydrazine hydrate In diethylene glycol at 162 - 178℃; for 4h;	86%

: 129-00-0
pyrene

: 693-55-0
monoethyl sebacate

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
2.) Wolf-Kischner reduction; Multistep reaction;

: 448210-97-7
3,5-Dinitro-benzoic acid (E)-(15R,16S)-15,17-dihydroxy-16-(10-pyren-1-yl-decanoylamino)-heptadec-13-enyl ester

A: 64701-47-9
10-(1-pyrenyl)decanoic acid

B: 448211-01-6
(4E,2S,3R)-2-amino-1,3,17-trihydroxy-17-(3,5-dinitrobenzoyl)-4-heptadecene

Conditions

Conditions	Yield
With ceramidase from Pseudomonas aeruginosa PA01; calcium chloride; Triton X-100 In water at 30℃; for 0.333333h; pH=8.5; Enzyme kinetics; Further Variations:; pH-values; Reagents;

: 14065-32-8
methyl 10-chloro-10-oxodecanoate

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 48.9 percent / AlCl3 / CH2Cl2 2: 89 percent / hydrazine hydrate; KOH / ethane-1,2-diol View Scheme

: 818-88-2
sebacic acid mono methyl ester

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: oxalyl chloride 2: 48.9 percent / AlCl3 / CH2Cl2 3: 89 percent / hydrazine hydrate; KOH / ethane-1,2-diol View Scheme

: 111-20-6
1,10-decanedioic acid

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 82 percent / diethyl sebacate, HCl / dibutyl ether 2: 93 percent / thionyl chloride / petroleum ether 3: 62 percent / AlCl3 / CS2 / 1.) 0 deg C, 1 h, 2.) 25 deg C, 11 h 4: 86 percent / potassium hydroxide, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 4 h / 162 - 178 °C View Scheme

: 693-55-0
monoethyl sebacate

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 93 percent / thionyl chloride / petroleum ether 2: 62 percent / AlCl3 / CS2 / 1.) 0 deg C, 1 h, 2.) 25 deg C, 11 h 3: 86 percent / potassium hydroxide, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 4 h / 162 - 178 °C View Scheme

: 6946-46-9
9-ethoxycarbonylnonanoic acid chloride

: 64701-47-9
10-(1-pyrenyl)decanoic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 62 percent / AlCl3 / CS2 / 1.) 0 deg C, 1 h, 2.) 25 deg C, 11 h 2: 86 percent / potassium hydroxide, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 4 h / 162 - 178 °C View Scheme

: 100-02-7
4-nitro-phenol

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 228243-59-2
10-(1-pyrenyl)decanoic acid p-nitrophenyl ester

Conditions

Conditions	Yield
With dicyclohexyl-carbodiimide In dichloromethane Esterification;	94%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 228243-60-5
10-(1-pyrenyl)decanoic acid pentafluorophenyl ester

Conditions

Conditions	Yield
With dicyclohexyl-carbodiimide In dichloromethane Esterification;	91.9%

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 70796-35-9
Pyrendecanoylchlorid

Conditions

Conditions	Yield
With thionyl chloride In Petroleum ether at 40 - 60℃; for 9h;

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 3-O-benzoyl-2-N-(4-(1-pyrenyl)decanoyl)-D,L-erythro-sphinganine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 94 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 55.1 percent / pyridine; Et3N / 5 h / 20 °C View Scheme
Multi-step reaction with 2 steps 1: 91.9 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 49 percent / pyridine / 20 °C View Scheme

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 3-O-benzoyl-2-N-(4-(1-pyrenyl)decanoyl)-D,L-erythro-sphinganine-1-O-(N,N-diisopropylamino)-2-cyanoethylphosphine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 94 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 55.1 percent / pyridine; Et3N / 5 h / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile View Scheme
Multi-step reaction with 3 steps 1: 91.9 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 49 percent / pyridine / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile View Scheme

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 2-N-(4-(1-pyrenyl)decanoyl)-D,L-erythro-sphinganine-1-O-phospho-5'-thymidine

Conditions

Conditions	Yield
Multi-step reaction with 7 steps 1: 94 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 55.1 percent / pyridine; Et3N / 5 h / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C 5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h 6: 54.5 percent / toluene / 4 h / 20 °C 7: 89.9 percent / 0.2 N MeONa / diethyl ether; methanol / 1 h / 20 °C View Scheme
Multi-step reaction with 7 steps 1: 91.9 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 49 percent / pyridine / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C 5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h 6: 54.5 percent / toluene / 4 h / 20 °C 7: 89.9 percent / 0.2 N MeONa / diethyl ether; methanol / 1 h / 20 °C View Scheme

Yield

Multi-step reaction with 7 steps
1: 94 percent / dicyclohexylcarbodiimide / CH2Cl2
2: 55.1 percent / pyridine; Et3N / 5 h / 20 °C
3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile
4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C
5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h
6: 54.5 percent / toluene / 4 h / 20 °C
7: 89.9 percent / 0.2 N MeONa / diethyl ether; methanol / 1 h / 20 °C
View Scheme

Multi-step reaction with 7 steps
1: 91.9 percent / dicyclohexylcarbodiimide / CH2Cl2
2: 49 percent / pyridine / 20 °C
3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile
4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C
5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h
6: 54.5 percent / toluene / 4 h / 20 °C
7: 89.9 percent / 0.2 N MeONa / diethyl ether; methanol / 1 h / 20 °C
View Scheme

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: Benzoic acid 1-[2-[[(2R,3S,5R)-3-acetoxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethoxy]-(2-cyano-ethoxy)-phosphanyloxy]-1-(10-pyren-1-yl-decanoylamino)-ethyl]-hexadecyl ester

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 94 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 55.1 percent / pyridine; Et3N / 5 h / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C View Scheme
Multi-step reaction with 4 steps 1: 91.9 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 49 percent / pyridine / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C View Scheme

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: Benzoic acid 1-[2-[[(2R,3S,5R)-3-acetoxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethoxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-(10-pyren-1-yl-decanoylamino)-ethyl]-hexadecyl ester

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: 94 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 55.1 percent / pyridine; Et3N / 5 h / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C 5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h View Scheme
Multi-step reaction with 5 steps 1: 91.9 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 49 percent / pyridine / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C 5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h View Scheme

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 3-O-benzoyl-2-N-(4-(1-pyrenyl)decanoyl)-D,L-erythro-sphinganine-1-O-phospho-5'-(3'-O-acetyl)thymidine triethylammonium salt

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: 94 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 55.1 percent / pyridine; Et3N / 5 h / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C 5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h 6: 54.5 percent / toluene / 4 h / 20 °C View Scheme
Multi-step reaction with 6 steps 1: 91.9 percent / dicyclohexylcarbodiimide / CH2Cl2 2: 49 percent / pyridine / 20 °C 3: 75.9 percent / diisopropylammonium tetrazolide / CH2Cl2; acetonitrile 4: 1H-tetrazole / CH2Cl2; acetonitrile / 0.5 h / 20 °C 5: tert-butyl hydroperoxide / CH2Cl2; acetonitrile / 0.67 h 6: 54.5 percent / toluene / 4 h / 20 °C View Scheme

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: 73116-44-6
ethyl ω-(1-pyreno)decanoate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SOCl2 / petroleum ether / 9 h / 40 - 60 °C 2: petroleum ether View Scheme

: 64701-47-9
10-(1-pyrenyl)decanoic acid

: C10H24O3Si

: C36H50O4Si

Conditions

Conditions	Yield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane

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