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PYRENE CAS NO.:129-00-0 Appearance:Yellow green crystal Purity:90%Min, 93%Min,95%Min,98%Min Fluoranthene:3.5% Max Phenanthrene:1% Max Carbazole:1% Max Packing:25Kg/Drum ADVANTAGE 1.Professional: More than 10 years chemical exporting experienc
Cas:129-00-0
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Cas:129-00-0
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inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
Cas:129-00-0
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
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inquiryProduct Description Product Name Pyrene CAS No. 129-00-0 Appearance Yellowish-green powder Assay ≥99% Capacity 500mt/year Min.packing 100gram Ap
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Cas:129-00-0
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Tianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
Cas:129-00-0
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inquiryName Pyrene CAS 129-00-0 Purity 99%min Appearance YELLOW POWDER Appearance: yellow powder Storage:Store in cool and dry place, away from sun light
Appearance:Yellow green cystal Storage:R T Package:25kg/drum Application:Raw materials for organic synthesis, 1,4,5,8-naphthalenetetracarboxylic acid can be prepared by oxidation, which is used in dyes, synthetic resins and engineering plastics; Aft
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Min.Order:10 Gram
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inquiryPyrene Basic information Product Name: Pyrene Synonyms: Pyrene (purity);Pyrenepract;PYRENE, FOR FLUORESCENCE;PYRENE, 1X1ML, CH2CL2, 200UG/ML;41164, Pyrene (purity);PYRENE, 5000MG, NEAT;PYRENE-D10, 25MG, NEAT;PYRENE, 1X1ML, MEOH, 1000UG/ML CAS:
Pyrene CAS:129-00-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, stero
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Product Detail Minimum Order Qty. 10 Gram
Cas:129-00-0
Min.Order:20 Metric Ton
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
4-ethynyl-phenanthrene
pyrene
Conditions | Yield |
---|---|
at 800℃; under 0.01 Torr; Product distribution; other temperatures; | 100% |
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In benzene for 4h; Heating; | 98% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In benzene for 48h; Ambient temperature; | 80% |
With triphenylmethyl perchlorate; acetic acid |
Conditions | Yield |
---|---|
With triethylamine In methanol; water at 4℃; for 0.25h; Irradiation; sensitizer: methylene blue; | 98% |
With tetraethylammonium perchlorate; triethylamine In ethanol; dimethyl sulfoxide at 20℃; for 12h; Electrolysis; Green chemistry; | 92% |
With tetrabutylammonium perchlorate In N,N-dimethyl-formamide at 22℃; Mechanism; electroreduction at Hg electrode, Pt counter electrode, current oscillations, other temperatures; | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran / 3 h / -78 °C 1.2: -78 - 20 °C 1.3: 1 h 2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one; water / 10 h / 100 °C View Scheme |
pyrene
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at 0℃; for 0.0166667h; | 95% |
Conditions | Yield |
---|---|
With palladium diacetate In cyclohexane at 140℃; for 24h; Molecular sieve; air; | 95% |
With palladium diacetate; potassium carbonate In ethyl acetate at 150℃; under 12929 Torr; for 0.833333h; Microwave irradiation; Molecular sieve; | 95% |
pyrene
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In tetrahydrofuran; N,N-dimethyl-formamide at 60℃; for 1h; | 91% |
2,7-di-tertbutylpyrene
pyrene
Conditions | Yield |
---|---|
With Nafion-H In toluene for 24h; Heating; | 90% |
pyrene
Conditions | Yield |
---|---|
With potassium tert-butylate at -80℃; | 90% |
With potassium tert-butylate at -80℃; Mechanism; reaction with other sulfonium salt was investigated; | 90% |
1-pyrenemethanol
pyrene
Conditions | Yield |
---|---|
With oxygen; palladium diacetate; sodium carbonate at 130℃; for 36h; Molecular sieve; Schlenk technique; | 88% |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; tetrahydroxydiboron; 5%-palladium/activated carbon In 1,2-dichloro-ethane at 50℃; for 3h; | 86% |
[2.2]Metacyclophan
A
pyrene
B
4,5-dihydropyrene
C
4,5,9,10-tetrahydropyrene
D
1,2,3,3a,4,5,9,10-octahydropyrene
E
1,2,3,3a,4,5-hexahydropyrene
F
1,2,3,3a,4,5,9,10,10a,10b-decahydropyrene
Conditions | Yield |
---|---|
With hydrogenchloride; aluminium trichloride In carbon disulfide Product distribution; Heating; | A 3% B n/a C n/a D 12% E 84% F 1% |
[2.2]Metacyclophan
A
pyrene
B
1,2,3,3a,4,5,9,10-octahydropyrene
C
1,2,3,3a,4,5-hexahydropyrene
D
1,2,3,3a,4,5,9,10,10a,10b-decahydropyrene
Conditions | Yield |
---|---|
With hydrogenchloride; aluminium trichloride In carbon disulfide Heating; | A 3% B 12% C 84% D 1% |
pyrene
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); ethyl-diphenyl-phosphane In toluene at 130℃; for 24h; Inert atmosphere; | 84% |
With bis(1,5-cyclooctadiene)nickel (0); 1,1,3,3-Tetramethyldisiloxane; ethyl-diphenyl-phosphane In toluene at 130℃; Inert atmosphere; | 84% |
N-(2,6-diisopropylphenyl)-4,5-dibromonaphthalene-1,8-dicarboximide
A
pyrene
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) In water; toluene at 90℃; Suzuki-Miyaura Coupling; | A 76% B n/a |
Conditions | Yield |
---|---|
With Nafion-H In toluene for 24h; Heating; | A 8% B 72% |
pyrene
Conditions | Yield |
---|---|
With iron(III) chloride In 1,2-dichloro-ethane at 20℃; for 0.5h; regioselective reaction; | 70% |
Conditions | Yield |
---|---|
With aluminum (III) chloride; sodium chloride at 160℃; for 1h; Temperature; Schlenk technique; Inert atmosphere; regioselective reaction; | A 7% B 70% |
A
pyrene
Conditions | Yield |
---|---|
With W-7 Raney Nickel In ethanol for 14h; Heating; | A 19% B 63% |
Conditions | Yield |
---|---|
With sodium methylate In methanol for 3h; Irradiation; | A 57% B 31% |
α,α,α',α'-tetrabromo-m-xylene
pyrene
Conditions | Yield |
---|---|
With magnesium at 600℃; | 54% |
N-(2,6-diisopropylphenyl)-4,5-dibromonaphthalene-1,8-dicarboximide
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrene
A
pyrene
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) In water; toluene at 90℃; Solvent; Reagent/catalyst; Suzuki-Miyaura Coupling; | A 50% B n/a C 50% |
Conditions | Yield |
---|---|
at 450 - 460℃; Mechanism; 5-6 h; | 45% |
at 500 - 510℃; under 0.0001 Torr; for 1h; Product distribution; | 40% |
2,6-bis[(trimethylsilyl)ethynyl]biphenyl
pyrene
Conditions | Yield |
---|---|
With [(t-BuXPhos)Au]NTf2 In para-xylene at 150℃; for 24h; | 42% |
Multi-step reaction with 2 steps 1: potassium carbonate / methanol / 20 °C 2: [(t-BuXPhos)Au]NTf2 / 1,2-dichloro-ethane / 24 h / 80 °C View Scheme |
Conditions | Yield |
---|---|
With aluminum (III) chloride; sodium chloride at 160℃; for 1h; Schlenk technique; Inert atmosphere; regioselective reaction; | A 35% B 12% |
2,6-diethynylbiphenyl
pyrene
Conditions | Yield |
---|---|
With [(t-BuXPhos)Au]NTf2 In 1,2-dichloro-ethane at 80℃; for 24h; | 30% |
3-(1-pyrenyl)propionic acid
A
pyrene
B
6H-benzopyrene
C
5-oxo-5H-benzo[cd]pyrene
D
naphthanthrone
F
4,5-dihydro-3H-benzo[cd]pyrene
G
7,8-dihydro-9H-cyclopentapyrene
Conditions | Yield |
---|---|
With polyphosphoric acid at 80℃; for 24h; Inert atmosphere; | A n/a B 26% C 30% D 29% E n/a F n/a G n/a |
3-(4H-cyclopentaphenanthrylidene)-1,5-bis(trimethylsilyl)-1,4-pentadiyne
A
pyrene
B
benzo[e]pyrene
C
4H-Cyclopenta[def]phenanthrene
D
cyclopenta[c,d]pyrene
E
benzo[ghi]fluoranthene
F
Coarannulen
Conditions | Yield |
---|---|
With hydrogen In gas at 900℃; Product distribution; electrically heated vertical laboratory tubular furnace; | A n/a B n/a C n/a D n/a E n/a F 15% |
3-(4H-cyclopentaphenanthrylidene)-1,5-bis(trimethylsilyl)-1,4-pentadiyne
A
pyrene
B
benzo[e]pyrene
C
cyclopenta[c,d]pyrene
D
Coarannulen
Conditions | Yield |
---|---|
With hydrogen In gas at 900℃; electrically heated vertical laboratory tubular furnace; Further byproducts given; | A n/a B n/a C n/a D 15% |
4,5-epoxy-4,5-dihydro-pyrene
pyrene
Conditions | Yield |
---|---|
With tetraphenylporphinatoiron(II)(pyridine)2 for 30h; Ambient temperature; | 12% |
(E,E)-1,3-distyrylbenzene
A
pyrene
B
benzo[c]chrysene
C
(1α,2α,3β,4β)-1,3-Di-2-phenanthryl-2,4-diphenylcyclobutan
D
(1α,2α,3β,4β)-1,2-Di-2-phenanthryl-3,4-diphenylcyclobutan
E
3,4,12,13-Tetraphenylpentacyclo<13.3.1.16,10.02,5.011,14>eicosa-1(19),6,8,10(20),15,17-hexaen
F
3b,4,5,5a,8b,9,10,10a-Octahydro-4,5,9,10-tetraphenyldicyclobutapyren
Conditions | Yield |
---|---|
With iodine In benzene for 1.5h; Product distribution; Mechanism; Irradiation; further without I2, var. conc.; | A 3% B 7% C 7% D 7% E n/a F n/a G n/a |
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane for 2h; | 100% |
With hydrogen bromide; dihydrogen peroxide In methanol; diethyl ether; water at 15 - 20℃; for 12.25h; | 96% |
With N-Bromosuccinimide; dibenzoyl peroxide In N,N-dimethyl-formamide at 20℃; | 96% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts Acylation; Inert atmosphere; | 100% |
With aluminum (III) chloride In 1,2-dichloro-ethane at 20℃; for 24h; | 98.3% |
With aluminum (III) chloride In dichloromethane at 25℃; for 0.5h; | 98.4% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere; | 100% |
With aluminum tri-bromide In carbon disulfide at 40℃; for 0.5h; | 99% |
aluminium trichloride In carbon disulfide Heating; | 99% |
pyrene
11-bromoundecanoyl chloride
11-bromo-1-(pyren-1-yl)undecan-1-one
Conditions | Yield |
---|---|
Stage #1: 11-bromoundecanoyl chloride With aluminum (III) chloride In dichloromethane Stage #2: pyrene In dichloromethane at 0 - 20℃; for 16.5h; | 100% |
With aluminium trichloride In dichloromethane at 0℃; for 3h; | 80% |
Conditions | Yield |
---|---|
In water-d2 Pd complex was treated with decalin and pyrene in D2O at room temp.; NMR monitoring; | 100% |
pyrene
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride
Conditions | Yield |
---|---|
With sulfuric acid | 100% |
pyrene
Conditions | Yield |
---|---|
In methanol at 40℃; for 2h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
With aluminum (III) chloride at 20℃; for 6h; | 100% |
With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 1.16667h; | 95% |
pyrene
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | 100% |
pyrene
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 16-bromohexadecanoyl chloride, With aluminum (III) chloride In dichloromethane at 0℃; for 1h; Stage #2: pyrene In dichloromethane at 0 - 20℃; for 16h; | 100% |
Conditions | Yield |
---|---|
With nitric acid; acetic acid at 60℃; for 0.5h; Inert atmosphere; regioselective reaction; | 99% |
With ammonium persulfate; sodium nitrite In acetonitrile for 21h; Ambient temperature; | 98% |
With dinitrogen tetraoxide In dichloromethane for 0.5h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
With bromine In nitrobenzene at 120℃; for 2h; | 99% |
With bromine In nitrobenzene at 120℃; for 14h; | 98% |
With bromine In nitrobenzene at 120℃; Inert atmosphere; | 98% |
pyrene
2,4-dichloro-2,4-dimethylpentane
Conditions | Yield |
---|---|
aluminium trichloride In carbon disulfide for 1h; Heating; | 99% |
pyrene
tertiary butyl chloride
A
2,7-di-tertbutylpyrene
B
2-(tert-butyl)pyrene
Conditions | Yield |
---|---|
aluminium trichloride In carbon disulfide for 1h; Mechanism; Heating; various solvents; | A n/a B 99% |
With aluminium trichloride In dichloromethane for 3h; Ambient temperature; | A n/a B 63% |
With aluminum (III) chloride In dichloromethane at 0℃; for 3h; Inert atmosphere; | A 11% B 40% |
With aluminium trichloride In dichloromethane for 3h; Ambient temperature; Yields of byproduct given; |
Conditions | Yield |
---|---|
aluminium trichloride In carbon disulfide for 1h; Heating; | 99% |
Conditions | Yield |
---|---|
In toluene under N2 or Ar; pyrene was added to the samarocene in toluene, stirred for 5 min; solvent was removed by rotary evapn.; elem. anal.; | 99% |
Conditions | Yield |
---|---|
Stage #1: phthalic anhydride; pyrene With aluminum (III) chloride In dichloromethane; water for 3h; Friedel-Crafts Acylation; Reflux; Inert atmosphere; Stage #2: With hydrogenchloride In dichloromethane; water Inert atmosphere; | 98% |
Stage #1: phthalic anhydride; pyrene With aluminum (III) chloride In dichloromethane for 3h; Inert atmosphere; Reflux; Stage #2: With acetic acid at 130℃; for 0.0833333h; Inert atmosphere; | 87% |
With aluminum (III) chloride In neat (no solvent) for 2h; Friedel-Crafts Acylation; Milling; | 79% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With hydrogen; 10percent Pd/C under 2327.23 Torr; for 144h; | 97% |
With palladium 10% on activated carbon; hydrogen In tetrahydrofuran; methanol at 90℃; under 7500.75 Torr; for 168h; Autoclave; | 90% |
Stage #1: pyrene With ethyl acetate at 20℃; for 48h; Inert atmosphere; Stage #2: With palladium 10% on activated carbon; hydrogen at 60℃; under 4500.45 Torr; for 48h; Inert atmosphere; | 89% |
pyrene
bis(pinacol)diborane
Conditions | Yield |
---|---|
With dtbpy; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer In cyclohexane at 80℃; for 16h; | 97% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine In tetrahydrofuran at 80℃; for 16h; Inert atmosphere; regiospecific reaction; | 94% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer In tetrahydrofuran for 12h; Inert atmosphere; Reflux; | 94% |
pyrene
bis(pinacol)diborane
4,4,5,5-tetramethyl-2-pyren-2-yl-[1, 3, 2]dioxaborolane
Conditions | Yield |
---|---|
With catalyst:[Ir(OMe)COD]2/dtbpy In not given 2.2 molar equiv. of B2pin2, (Ir(OMe)COD)2 (5 mol%) + 4,4'-di-tert-butyl-2,2'-bipyridine (10 mol%); chromd. on silica pad (CH2Cl2); solvent removed (vac. 150°C); elem. anal.; | 97% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine In hexane at 80℃; for 16h; Inert atmosphere; regioselective reaction; | 65% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine In cyclohexene at 80℃; for 12h; Inert atmosphere; | 65% |
Conditions | Yield |
---|---|
With aluminum tri-bromide In carbon disulfide at 40℃; for 1h; | 96% |
With aluminum (III) chloride In dichloromethane at 5 - 20℃; for 4h; | 92% |
With aluminum (III) chloride In dichloromethane at 5 - 20℃; for 4.5h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at 0 - 20℃; for 2.5h; | 96% |
With titanium tetrachloride In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere; | 91% |
With titanium tetrachloride In dichloromethane for 3h; Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With [mesitylenium]B(C6F5)4; benzene-d6 In benzene-d6 at 70℃; for 72h; Inert atmosphere; | 96% |
With d7-N,N-dimethylformamide; potassium tert-butylate at 170℃; for 1h; Microwave irradiation; | 95% |
With water-d2; hydrogen chloride at 250℃; for 50h; | 89% |
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