Products

Refine

Country

Business Type

Certificate

Display

Suzhou Sinosun Imp.&Exp. Corporation

We supply high purity 1-Bromopyrene CAS# 1714-29-0 at best price in China, Our 1-Bromopyrene CAS# 1714-29-0 has been exported to many countries and regions. If you are looking for 1-Bromopyrene CAS# 1714-29-0 suppliers in China, Sinosun is your b

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------

High purity 1714-29-0 1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Trading Company

inquiry

Henan Allgreen Chemical Co.,Ltd

The company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:solid Storage:Sealed, dry, microtherm , avo

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1-Bromopyrene

Cas:1714-29-0

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 1714-29-0 1 – bromopyrene Manufacturer

Cas:1714-29-0

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-Bromopyrene

Cas:1714-29-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/1365.html Product Name 1-Bromopyrene CAS No.

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Gram

FOB Price: $11.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: 1-Bromopyrene Synonyms: 1-BROMOPYRENE;Pyrene, 1-bromo-;2-Bromopyrene;1-Pyrenyl bromide;1-Bromopyene;1-Bromopyrene 96% CAS: 1714-29-0 MF: C16H9Br MW: 281.15 EINECS: 1312995-182-4 398- App

1714-29-0 1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Gram

FOB Price: $8900.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

1-Bromopyrene CAS NO 1714-29-0

Cas:1714-29-0

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 1714-29-0 with best quality

Cas:1714-29-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

1-Bromopyrene CAS1714-29-0

Cas:1714-29-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product Name: 1,4-DIBROMONAPHTHALENE Synonyms: 1,4-DIBROMONAPHTHALENE;1,4-DIBROMONAPTHALENE;1,4-dibromo-naphthalen;1,4-Dibromonaphthalene,99%;1,4-DIBROMONAPHTHALE;1,4-Dibromonaphthalene, 98+%

1-Bromopyrene CAS: 1714-29-0

Cas:1714-29-0

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Other

inquiry

Wuhan Fortuna Chemical Co.,Ltd

1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers 3.Safe a

1-Bromopyrene

Cas:1714-29-0

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1-Bromopyrene 1714-29-0

Cas:1714-29-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Leader Biochemical Group

About Product Details Items Specifications Test Results Appearance White to white crystalline powde

China Biggest Factory Manufacturer Supply 1-Bromopyrene CAS 1714-29-0

Cas:1714-29-0

Min.Order:100 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram

1-Bromopyrene CAS NO.1714-29-0 CAS NO.1714-29-0

Cas:1714-29-0

Min.Order:20 Metric Ton

Negotiable

Type:Trading Company

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Kilogram

FOB Price: $10.0 / 100.0

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

1-Bromopyrene

Cas:1714-29-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Triumph International Development Limilted

Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By

1-BroMo-Pyrene

Cas:1714-29-0

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

1-Bromopyrene

Cas:1714-29-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-Bromopyrene

Cas:1714-29-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1-Bromopyrene

Cas:1714-29-0

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products 1-BroMo-Pyrene

Cas:1714-29-0

Min.Order:100 Gram

Negotiable

Type:Other

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1-Bromopyrene

Cas:1714-29-0

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 1-Bromopyrene CAS No.: 1714-29-0 Molecule Formula:C16H9Br Molecule Weight:281.15 Purity: 99.0% Package: 25kg/bag Description:Light yellow powder Manufacture Standards:Enterprise Standard TESTING ITEMS

Lower Price 1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

1-Bromo-PyreneCAS NO.: 1714-29-0

Cas:1714-29-0

Min.Order:1 Gram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

1-Bromopyrene

Cas:1714-29-0

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Synthetic route

pyrene
129-00-0

pyrene

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
With N-Bromosuccinimide In dichloromethane for 2h;100%
With hydrogen bromide; dihydrogen peroxide In methanol; diethyl ether; water at 15 - 20℃; for 12.25h;96%
With N-Bromosuccinimide; dibenzoyl peroxide In N,N-dimethyl-formamide at 20℃;96%
C24H29BrO2

C24H29BrO2

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
With methanesulfonic acid In dichloromethane at 0 - 20℃; for 1h;96.08%
C24H29BrO2

C24H29BrO2

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
With methanesulfonic acid In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;93.24%
C18H17BrO2

C18H17BrO2

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
With methanesulfonic acid In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;91.1%
C18H17BrO2

C18H17BrO2

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
With methanesulfonic acid In dichloromethane at 0 - 20℃; for 1h;84.7%
tetrachloromethane
56-23-5

tetrachloromethane

N-Bromosuccinimide
128-08-5

N-Bromosuccinimide

pyrene
129-00-0

pyrene

1-bromopyrene
1714-29-0

1-bromopyrene

N-Bromosuccinimide
128-08-5

N-Bromosuccinimide

pyrene
129-00-0

pyrene

benzene
71-43-2

benzene

1-bromopyrene
1714-29-0

1-bromopyrene

Pyrene-1-carbonyl bromide

Pyrene-1-carbonyl bromide

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
With RhCl(PPh3)3 at 290℃;
pyridine
110-86-1

pyridine

pyrene
129-00-0

pyrene

bromine
7726-95-6

bromine

1-bromopyrene
1714-29-0

1-bromopyrene

tetrachloromethane
56-23-5

tetrachloromethane

pyrene
129-00-0

pyrene

bromine
7726-95-6

bromine

1-bromopyrene
1714-29-0

1-bromopyrene

pyrene
129-00-0

pyrene

chloroform
67-66-3

chloroform

bromine
7726-95-6

bromine

1-bromopyrene
1714-29-0

1-bromopyrene

pyrene
129-00-0

pyrene

water
7732-18-5

water

bromine
7726-95-6

bromine

1-bromopyrene
1714-29-0

1-bromopyrene

3-bromo-2,2'-diiodo-1,1'-biphenyl

3-bromo-2,2'-diiodo-1,1'-biphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
2.2: 2 h / 5 - 30 °C
3.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
View Scheme
3-bromo-2,2'-diformyl-1,1'-biphenyl

3-bromo-2,2'-diformyl-1,1'-biphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
1.2: 2 h / 5 - 30 °C
2.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
View Scheme
1-chloro-2,6-dinitrobenzene
606-21-3

1-chloro-2,6-dinitrobenzene

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / ethanol; water; toluene / 8 h / 30 - 40 °C / Inert atmosphere
2.1: hydrogen; 5%-palladium/activated carbon / ethanol / 40 °C / 2250.23 Torr / Autoclave
3.1: copper(l) iodide; sodium nitrite; hydrogen iodide / water / 3 h / 5 - 60 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C
4.2: 20 °C
5.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
5.2: 2 h / 5 - 20 °C
6.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
(3-bromophenyl)boronic acid
89598-96-9

(3-bromophenyl)boronic acid

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / ethanol; water; toluene / 8 h / 30 - 40 °C / Inert atmosphere
2.1: hydrogen; 5%-palladium/activated carbon / ethanol / 40 °C / 2250.23 Torr / Autoclave
3.1: copper(l) iodide; sodium nitrite; hydrogen iodide / water / 3 h / 5 - 60 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C
4.2: 20 °C
5.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
5.2: 2 h / 5 - 20 °C
6.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
3'-bromo-2,6-dinitro-1,1'-biphenyl

3'-bromo-2,6-dinitro-1,1'-biphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: hydrogen; 5%-palladium/activated carbon / ethanol / 40 °C / 2250.23 Torr / Autoclave
2.1: copper(l) iodide; sodium nitrite; hydrogen iodide / water / 3 h / 5 - 60 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C
3.2: 20 °C
4.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
4.2: 2 h / 5 - 20 °C
5.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
3'-bromo-2,6-diamino-1,1'-biphenyl

3'-bromo-2,6-diamino-1,1'-biphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: copper(l) iodide; sodium nitrite; hydrogen iodide / water / 3 h / 5 - 60 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C
2.2: 20 °C
3.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
3.2: 2 h / 5 - 20 °C
4.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
3'-bromo-2,6-diiodo-1,1'-biphenyl

3'-bromo-2,6-diiodo-1,1'-biphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C
1.2: 20 °C
2.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
2.2: 2 h / 5 - 20 °C
3.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
3'-bromo-2,6-diformyl-1,1'-biphenyl

3'-bromo-2,6-diformyl-1,1'-biphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
1.2: 2 h / 5 - 20 °C
2.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
3-bromobiphenyl
2113-57-7

3-bromobiphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: nitric acid; sulfuric acid; acetic anhydride / dichloromethane / 4 h / 5 - 25 °C
2.1: hydrogen; 5%-palladium/activated carbon / ethanol / 40 °C / 2250.23 Torr / Autoclave
3.1: copper(l) iodide; sodium nitrite; hydrogen iodide / water / 3 h / 5 - 60 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
5.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
5.2: 2 h / 5 - 30 °C
6.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
View Scheme
3-bromo-2,2'-dinitro-1,1'-biphenyl

3-bromo-2,2'-dinitro-1,1'-biphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: hydrogen; 5%-palladium/activated carbon / ethanol / 40 °C / 2250.23 Torr / Autoclave
2.1: copper(l) iodide; sodium nitrite; hydrogen iodide / water / 3 h / 5 - 60 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
4.2: 2 h / 5 - 30 °C
5.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
View Scheme
3-bromo-2,2′-diaminebiphenyl

3-bromo-2,2′-diaminebiphenyl

1-bromopyrene
1714-29-0

1-bromopyrene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: copper(l) iodide; sodium nitrite; hydrogen iodide / water / 3 h / 5 - 60 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -85 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 5 °C
3.2: 2 h / 5 - 30 °C
4.1: methanesulfonic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
View Scheme
1-bromopyrene
1714-29-0

1-bromopyrene

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

trimethyl(2-(pyren-1-yl)ethynyl)silane
253271-87-3

trimethyl(2-(pyren-1-yl)ethynyl)silane

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 70℃; for 20h;100%
With bis-triphenylphosphine-palladium(II) chloride; triethylamine at 70℃; for 23h; Sonogashira coupling; Inert atmosphere; Neat (no solvent); Sealed tube;99%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine at 20℃; for 24h; Inert atmosphere;99%
1-bromopyrene
1714-29-0

1-bromopyrene

1-pyrenylboronic acid
164461-18-1

1-pyrenylboronic acid

Conditions
ConditionsYield
With n-butyllithium; Triisopropyl borate100%
Stage #1: 1-bromopyrene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 0.833333h;
Stage #2: With Triisopropyl borate In tetrahydrofuran at 20℃; for 36h;
82%
Stage #1: 1-bromopyrene With n-butyllithium In diethyl ether at 0℃; for 0.5h;
Stage #2: With Trimethyl borate In diethyl ether at -78 - 20℃; for 26h;
Stage #3: In diethyl ether at 20℃; for 3h; Acid hydrolysis;
73%
1-bromopyrene
1714-29-0

1-bromopyrene

tributyl(thien-2-yl)stannane
54663-78-4

tributyl(thien-2-yl)stannane

2-(pyren-1-yl)thiophene
1040100-95-5

2-(pyren-1-yl)thiophene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0) In toluene at 110℃; for 24h; Stille Cross Coupling; Inert atmosphere;100%
With tetrakis(triphenylphosphine) palladium(0) In toluene at 110℃; for 96h; Stille Cross-Coupling (Migita-Kosugi-Stille Coupling); Inert atmosphere;95%
With tetrakis(triphenylphosphine) palladium(0) In toluene for 24h; Inert atmosphere; Reflux;83.6%
With tetrakis(triphenylphosphine) palladium(0) In toluene Stille Cross Coupling; Inert atmosphere;
(4-(naphthalen-1-yl)phenyl)boronic acid
870774-25-7

(4-(naphthalen-1-yl)phenyl)boronic acid

1-bromopyrene
1714-29-0

1-bromopyrene

1-(4-naphthalene-1-yl-phenyl)pyrene

1-(4-naphthalene-1-yl-phenyl)pyrene

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water for 8h; Heating / reflux;99%
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
61676-62-8

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

1-bromopyrene
1714-29-0

1-bromopyrene

1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrene
349666-24-6

1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrene

Conditions
ConditionsYield
Stage #1: 1-bromopyrene With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane In tetrahydrofuran for 1h;
99%
Stage #1: 1-bromopyrene With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane In tetrahydrofuran for 1h;
99%
Stage #1: 1-bromopyrene With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane In tetrahydrofuran
99%
1-bromopyrene
1714-29-0

1-bromopyrene

tri(2-naphthyl)indium

tri(2-naphthyl)indium

1-(1-naphthalenyl)pyrene
88812-42-4

1-(1-naphthalenyl)pyrene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); DavePhos In tetrahydrofuran at 80℃; Schlenk technique; Inert atmosphere;99%
2-methyl-3-buten-2-ol
115-18-4

2-methyl-3-buten-2-ol

1-bromopyrene
1714-29-0

1-bromopyrene

1-(3-hydroxy-3-methyl-1-butynyl)pyrene

1-(3-hydroxy-3-methyl-1-butynyl)pyrene

Conditions
ConditionsYield
With copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; triethylamine; triphenylphosphine In toluene at 80℃; Inert atmosphere;99%
methanol
67-56-1

methanol

1-bromopyrene
1714-29-0

1-bromopyrene

1-methoxypyrene
34246-96-3

1-methoxypyrene

Conditions
ConditionsYield
With copper(l) iodide; sodium for 36h; Reflux; Inert atmosphere;98%
With copper(l) iodide In N,N-dimethyl-formamide for 3h; Heating;91%
With copper(l) iodide; sodium methylate In N,N-dimethyl-formamide for 30h; Heating;74%
1-bromopyrene
1714-29-0

1-bromopyrene

pyrene
129-00-0

pyrene

Conditions
ConditionsYield
With triethylamine In methanol; water at 4℃; for 0.25h; Irradiation; sensitizer: methylene blue;98%
With tetraethylammonium perchlorate; triethylamine In ethanol; dimethyl sulfoxide at 20℃; for 12h; Electrolysis; Green chemistry;92%
With tetrabutylammonium perchlorate In N,N-dimethyl-formamide at 22℃; Mechanism; electroreduction at Hg electrode, Pt counter electrode, current oscillations, other temperatures;
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 3 h / -78 °C
1.2: -78 - 20 °C
1.3: 1 h
2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one; water / 10 h / 100 °C
View Scheme
1-bromopyrene
1714-29-0

1-bromopyrene

phenylacetylene
536-74-3

phenylacetylene

1-(phenylethynyl)pyrene
23975-18-0

1-(phenylethynyl)pyrene

Conditions
ConditionsYield
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine for 48h; Reflux;98%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine at 80℃; for 48h; Inert atmosphere;69%
1-bromopyrene
1714-29-0

1-bromopyrene

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrene
349666-24-6

1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrene

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane at 90℃; for 4h; Inert atmosphere; Schlenk technique;98%
With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate In 1,4-dioxane at 80℃; Inert atmosphere;81%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane at 90℃; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique;80%
1-bromopyrene
1714-29-0

1-bromopyrene

2-methyl-but-3-yn-2-ol
115-19-5

2-methyl-but-3-yn-2-ol

1-(3-hydroxy-3-methyl-1-butynyl)pyrene

1-(3-hydroxy-3-methyl-1-butynyl)pyrene

Conditions
ConditionsYield
Stage #1: 1-bromopyrene With bis-triphenylphosphine-palladium(II) chloride; diethylamine at 50℃; Sonogashira Cross-Coupling;
Stage #2: 2-methyl-but-3-yn-2-ol With copper(l) iodide Reflux;
97%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; triphenylphosphine In tetrahydrofuran Sonogashira Cross-Coupling; Reflux;76%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide In various solvent(s)60%
With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine; lithium bromide; copper(ll) bromide In tetrahydrofuran at 90℃; for 2h; Substitution; Title compound not separated from byproducts;
Stage #1: 1-bromopyrene; 2-methyl-but-3-yn-2-ol With piperidine; lithium bromide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triphenylphosphine In tetrahydrofuran at 90℃; for 3h; Inert atmosphere;
Stage #2: With hydrogenchloride In tetrahydrofuran; dichloromethane; water
Thien-3-ylboronic acid
6165-69-1

Thien-3-ylboronic acid

1-bromopyrene
1714-29-0

1-bromopyrene

3-pyren-1-yl-thiophene

3-pyren-1-yl-thiophene

Conditions
ConditionsYield
With potassium carbonate In water; toluene at 90℃; for 0.5h; Suzuki-Miyaura Coupling;97%
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran; water Suzuki condensation;82%
morpholine
110-91-8

morpholine

1-bromopyrene
1714-29-0

1-bromopyrene

N-(1-pyrenyl)morpholine
1021359-33-0

N-(1-pyrenyl)morpholine

Conditions
ConditionsYield
With sodium t-butanolate; palladium diacetate In toluene at 80℃; for 1h; Buchwald-Hartwig amination;97%
1-bromopyrene
1714-29-0

1-bromopyrene

4-cyanophenylacetylene
3032-92-6

4-cyanophenylacetylene

4-(2-(pyren-1-yl)ethynyl)benzonitrile
54273-36-8

4-(2-(pyren-1-yl)ethynyl)benzonitrile

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); copper(II) sulfate; sodium L-ascorbate; triethylamine In N,N-dimethyl-formamide at 80℃; for 4h; Sonogashira coupling; Inert atmosphere;97%
Dichloromethyl methyl ether
4885-02-3

Dichloromethyl methyl ether

1-bromopyrene
1714-29-0

1-bromopyrene

6-bromo-pyrene-1-carbaldehyde

6-bromo-pyrene-1-carbaldehyde

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane at 20℃; for 3h; Cooling with ice;97%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

1-bromopyrene
1714-29-0

1-bromopyrene

2-mercaptoethylamine hydrochloride
156-57-0

2-mercaptoethylamine hydrochloride

C23H23NO2S
1492816-10-0

C23H23NO2S

Conditions
ConditionsYield
Stage #1: 1-bromopyrene; 2-mercaptoethylamine hydrochloride With potassium hydroxide In N,N-dimethyl-formamide at 20 - 110℃; for 1h; Inert atmosphere;
Stage #2: di-tert-butyl dicarbonate In N,N-dimethyl-formamide at 20℃; for 2h;
96%
ferroceneacetylene
1271-47-2

ferroceneacetylene

1-bromopyrene
1714-29-0

1-bromopyrene

(1-pyrenyl)ethynylferrocene
851537-08-1

(1-pyrenyl)ethynylferrocene

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; triphenylphosphine at 88℃; for 8h; Sonogashira Cross-Coupling; Inert atmosphere; Schlenk technique;96%
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 70℃; for 24h; Sonogashira Cross-Coupling; Inert atmosphere;68%
2,5-Dimethylpyrrole
625-84-3

2,5-Dimethylpyrrole

1-bromopyrene
1714-29-0

1-bromopyrene

2-(pyrene-1-yl)-2,5-dimethyl-2H-pyrrole

2-(pyrene-1-yl)-2,5-dimethyl-2H-pyrrole

Conditions
ConditionsYield
Stage #1: 2,5-Dimethylpyrrole With n-butyllithium at 0℃; for 0.25h; Inert atmosphere;
Stage #2: 1-bromopyrene With bis(dibenzylideneacetone)-palladium(0); ruphos at 100℃; for 12h; Inert atmosphere; regioselective reaction;
96%
1-bromopyrene
1714-29-0

1-bromopyrene

phenylboronic acid
98-80-6

phenylboronic acid

1-phenyl pyrene
5101-27-9

1-phenyl pyrene

Conditions
ConditionsYield
Stage #1: 1-bromopyrene; phenylboronic acid With sodium methylate In ethanol Suzuki-Miyaura Coupling; Inert atmosphere;
Stage #2: In ethanol at 60℃; for 1h; Inert atmosphere;
96%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene at 90℃; for 24h; Inert atmosphere;70%
1-bromopyrene
1714-29-0

1-bromopyrene

sodium methylate
124-41-4

sodium methylate

1-methoxypyrene
34246-96-3

1-methoxypyrene

Conditions
ConditionsYield
In methanol for 15h; Inert atmosphere; Reflux; Large scale;95.2%
With copper(l) iodide In methanol for 36h; Inert atmosphere; Reflux;87.7%
With copper(l) iodide In N,N-dimethyl-formamide at 85℃; for 4h;84%
acrylaldehyde diethyl acetal
3054-95-3

acrylaldehyde diethyl acetal

1-bromopyrene
1714-29-0

1-bromopyrene

3-(pyrene-1-yl)propionic acid ethyl ester
83671-44-7

3-(pyrene-1-yl)propionic acid ethyl ester

Conditions
ConditionsYield
Stage #1: acrylaldehyde diethyl acetal; 1-bromopyrene With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); sodium acetate In 1-methyl-pyrrolidin-2-one at 140℃; for 6h;
Stage #2: With hydrogenchloride; water In 1-methyl-pyrrolidin-2-one
95%
4,4-difluoro-8-(p-(9-acetylenyl-1-ethynylpyrenyl)phenyl)-1,3,5,7-tetramethyl-2,4-diethyl-4-bora-3a,4a-diaza-s-indacene

4,4-difluoro-8-(p-(9-acetylenyl-1-ethynylpyrenyl)phenyl)-1,3,5,7-tetramethyl-2,4-diethyl-4-bora-3a,4a-diaza-s-indacene

1-bromopyrene
1714-29-0

1-bromopyrene

4,4-difluoro-8-(p-(9-(1-acetylenylpyrenyl)-1-ethynylpyrenyl)phenyl)-1,3,5,7-tetramethyl-2,4-diethyl-4-bora-3a,4a-diaza-s-indacene

4,4-difluoro-8-(p-(9-(1-acetylenylpyrenyl)-1-ethynylpyrenyl)phenyl)-1,3,5,7-tetramethyl-2,4-diethyl-4-bora-3a,4a-diaza-s-indacene

Conditions
ConditionsYield
With diisopropylamine; tetrakis(triphenylphosphine) palladium(0) In benzene at 20℃; for 16h; Sonogashira coupling;95%
1-bromopyrene
1714-29-0

1-bromopyrene

propargyl alcohol
107-19-7

propargyl alcohol

3-(pyren-1-yl)prop-2-yn-1-ol
1392406-87-9

3-(pyren-1-yl)prop-2-yn-1-ol

Conditions
ConditionsYield
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-butylamine at 90℃; Inert atmosphere;95%
With tetrakis(triphenylphosphine) palladium(0); N-butylamine for 3h; Sonogashira Cross-Coupling; Reflux; Inert atmosphere;95%
1-bromopyrene
1714-29-0

1-bromopyrene

4-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-9H-carbazole

4-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-9H-carbazole

4-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-9-(pyren-1-yl)-9H-carbazole

4-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-9-(pyren-1-yl)-9H-carbazole

Conditions
ConditionsYield
With copper(l) iodide; 18-crown-6 ether; potassium carbonate In 1,2-dichloro-benzene at 190℃; for 24h; Reflux;95%
1-bromopyrene
1714-29-0

1-bromopyrene

N3,N3,N6,N6-tetrakis(4-methoxyphenyl)-9-H-carbazole-3,6-diamine

N3,N3,N6,N6-tetrakis(4-methoxyphenyl)-9-H-carbazole-3,6-diamine

N3,N3,N6,N6,tetrakis(4-methoxyphenyl)-9-(1-pyrene)-carbazole-3,6-diamine

N3,N3,N6,N6,tetrakis(4-methoxyphenyl)-9-(1-pyrene)-carbazole-3,6-diamine

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene for 7h; Buchwald-Hartwig Coupling; Schlenk technique; Inert atmosphere; Reflux;95%
4-tert-Butylstyrene
1746-23-2

4-tert-Butylstyrene

1-bromopyrene
1714-29-0

1-bromopyrene

(E)-1-(4-tert-butylstyryl)pyrene
1338347-88-8

(E)-1-(4-tert-butylstyryl)pyrene

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate; XPhos In N,N-dimethyl-formamide at 60℃; for 6h; Mizoroki-Heck reaction; Inert atmosphere; Pressure tube;94%
1-bromopyrene
1714-29-0

1-bromopyrene

4-Chlorophenylboronic acid
1679-18-1

4-Chlorophenylboronic acid

1-(4-chlorophenyl)pyrene
929099-49-0

1-(4-chlorophenyl)pyrene

Conditions
ConditionsYield
With sodium carbonate; palladium diacetate In 1,2-dimethoxyethane; water for 6.5h; Inert atmosphere; Reflux;94%

Hot Products

Post buying leads

About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia

Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog

©2008 LookChem.com,License: ICP

NO.:Zhejiang16009103

complaints:service@lookchem.com Desktop View