As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryTIANFUCHEM--2113-57-7--3-Bromobiphenyl factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relati
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryProduct name: 3-Bromobiphenyl CAS No.: 2113-57-7 Molecular formula C12H9Br Appearance: light yellow liquid Assay: 98.0% Structural formul
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
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inquiry3-Bromobiphenyl CAS: 2113-57-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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inquiryName: 1,1'-Biphenyl, 3-bromo- Synonyms: PBB 2; A-2885; A815156; 113b577; AM83052; RP05622; SY015795; AN-50402; CJ-25736; ACT07931; SC-15043; BC003378; AC1Q253K; I01-2451; AC1L27Z0; AC-18410; W-107572; CJ-05682; AK-84655; AS-14527; AJ-27964; KB-30
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryAppearance:Colorless to pale yellow liquid Storage:R.T Package:25kg/Barrel Application:Organic synthesis intermediates, used as raw materials for pesticides and fungicides. Can be used as an industrial disinfectant. Transportation:Express/Sea/Air Po
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Cas:2113-57-7
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With palladium diacetate; potassium carbonate; triphenylphosphine In water; toluene at 100℃; for 24h; | 98% |
With barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane; water for 6h; Suzuki coupling; Heating; | 92% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water for 8h; Inert atmosphere; Reflux; | 80% |
Conditions | Yield |
---|---|
With C27H23ClNO3PPd; potassium carbonate In ethanol; water at 50℃; for 7h; Temperature; Suzuki-Miyaura Coupling; Schlenk technique; | 94% |
With palladium diacetate In ethanol at 20℃; for 0.25h; Suzuki-Miyaura Coupling; chemoselective reaction; | 86% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; toluene at 90℃; for 3h; | 70% |
Conditions | Yield |
---|---|
Stage #1: benzene With potassium permanganate; acetic acid Microwave irradiation; Stage #2: (3-bromophenyl)boronic acid for 0.5h; Microwave irradiation; | 91% |
With potassium permanganate; acetic acid Heating; | 90% |
With manganese triacetate for 0.5h; Heating; | 89% |
With iron(III) trifluoromethanesulfonate; di-tert-butyl peroxide; 4,7-bis[4-(trifluoromethyl)phenyl]-1,10-phenanthroline at 80℃; for 24h; | 76% |
With NH-pyrazole; potassium phosphate; iron(III) sulphate heptahydrate; 1,4,7,10-tetraazacyclododecan at 80℃; for 48h; | 55% |
Conditions | Yield |
---|---|
With potassium permanganate; acetic acid Heating; | 90% |
With manganese triacetate Heating; | 73% |
3-bromophenyl trifluoromethanesulfonate
phenylzinc(II) bromide
3-bromobiphenyl
Conditions | Yield |
---|---|
bis(diphenylphosphino)propanepalladium(II) dichloride In tetrahydrofuran at 60℃; for 11h; Negishi cross-coupling reaction; | 90% |
3-bromobiphenyl
Conditions | Yield |
---|---|
With 1% Pd/C In methanol at 50℃; for 0.5h; Suzuki-Miyaura reaction; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
at 100℃; for 12h; Sealed tube; | 89% |
With meta-dinitrobenzene |
Conditions | Yield |
---|---|
Stage #1: bromobenzene; 1-Bromo-3-iodobenzene With magnesium In tetrahydrofuran for 1h; Inert atmosphere; Reflux; Green chemistry; Stage #2: In tetrahydrofuran at 50 - 85℃; for 8h; Green chemistry; | 84.69% |
Conditions | Yield |
---|---|
With diethyl bromomethylmalonate; [4,4′-di-tert-butyl-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C}iridium(III) hexafluorophosphate; caesium carbonate at 80℃; for 22h; Irradiation; | 82% |
With dipotassium peroxodisulfate; silver nitrate In acetonitrile at 120℃; for 24h; Glovebox; Schlenk technique; Sealed tube; Inert atmosphere; | 55% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; silver nitrate In acetonitrile at 120℃; for 10h; Inert atmosphere; Sealed tube; Green chemistry; | 82% |
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-3-iodobenzene; chlorobenzene With magnesium In tetrahydrofuran for 1h; Inert atmosphere; Reflux; Green chemistry; Stage #2: In tetrahydrofuran; water; toluene at 50 - 85℃; for 8h; Inert atmosphere; Reflux; Green chemistry; | 81.37% |
Conditions | Yield |
---|---|
Stage #1: iodobenzene; 1-Bromo-3-iodobenzene With magnesium In tetrahydrofuran for 1h; Inert atmosphere; Reflux; Green chemistry; Stage #2: In tetrahydrofuran at 50 - 85℃; for 8h; Green chemistry; | 80.61% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; silver nitrate In acetonitrile at 120℃; for 20h; Sealed tube; Schlenk technique; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With potassium phosphate In 1,4-dioxane at 115℃; for 30h; Suzuki-Miyaura Coupling; Inert atmosphere; | 77% |
Conditions | Yield |
---|---|
Stage #1: 1,3-dibromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: C19H16NS(1+)*F6P(1-) In tetrahydrofuran; hexane at -78 - 23℃; for 1.5h; Inert atmosphere; | 71% |
Conditions | Yield |
---|---|
70% |
1,3-dibromobenzene
phenylboronic acid
A
1,3-diphenylbenzene
B
3-bromobiphenyl
Conditions | Yield |
---|---|
With disodium[(N,N’-bis(2-hydroxy-5-sulfonatobenzyl)-1,2-diphenyl-1,2-diaminoethano)palladate(II)]; caesium carbonate In water at 80℃; for 1h; Suzuki-Miyaura Coupling; | A 68% B 24% |
With potassium phosphate; {1,3-di(NHP(piperidinyl)2)C6H3}PdCl In toluene at 100℃; for 0.0833333h; Suzuki reaction; | A 76 % Chromat. B 24 % Chromat. |
With potassium carbonate; [{P(NC4H8NMe)3}2PdCl2] In methanol at 20℃; for 2h; Suzuki-Miyaura coupling reaction; |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; potassium 2-methylbutan-2-olate at 80℃; for 24h; Inert atmosphere; | 65% |
3-bromophenyl trifluoromethanesulfonate
A
1,3-diphenylbenzene
B
3-bromobiphenyl
Conditions | Yield |
---|---|
With lithium bromide; bis(diphenylphosphino)propanepalladium(II) dichloride In diethyl ether at 0℃; for 2h; Kumada cross-coupling reaction; | A 20% B 60% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; 1,2-Dinitrobenzene In decane at 150℃; for 12h; Inert atmosphere; Sealed tube; | 59% |
bromobenzene
phenol
A
2-Bromobiphenyl
B
4-bromo-1,1'-biphenyl
C
3-bromobiphenyl
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; iodine at 289.9℃; for 0.0272222h; Product distribution; | A 22.7% B 18.4% C 58.9% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; 1,2-Dinitrobenzene In decane at 150℃; for 12h; Inert atmosphere; Sealed tube; | 56% |
1-Bromo-3-iodobenzene
benzene
A
1,3-diphenylbenzene
B
3-bromobiphenyl
Conditions | Yield |
---|---|
With 1-(2-hydroxyethyl)piperazine; potassium tert-butylate at 100℃; for 24h; Sealed tube; Inert atmosphere; | A 50% B 25% |
Conditions | Yield |
---|---|
With (triphenylphosphine)gold(I) chloride In acetonitrile at 20℃; for 16h; Inert atmosphere; | 44% |
1-(3-bromophenyl)cyclohexanol
3-bromobiphenyl
Conditions | Yield |
---|---|
With copper; Selectfluor In acetonitrile at 80℃; for 24h; chemoselective reaction; | 41% |
1,3-dibromobenzene
benzene
A
1,3-diphenylbenzene
B
3-bromobiphenyl
Conditions | Yield |
---|---|
With potassium tert-butylate; vasicine at 20 - 110℃; for 72h; Schlenk technique; Inert atmosphere; | A 24% B 19% |
bromobenzene
N-sulphinylphenylhydrazine
A
2-Bromobiphenyl
B
4-bromo-1,1'-biphenyl
C
3-bromobiphenyl
D
diphenyldisulfane
Conditions | Yield |
---|---|
at 135℃; for 72h; Further byproducts given; | A 20.9% B 6.9% C 12.7% D 1.1% E n/a |
at 135℃; for 72h; Further byproducts given; | A 19.5% B 8.1% C 12.9% D 1.1% E n/a |
bromobenzene
N-sulphinylphenylhydrazine
A
S-Phenyl benzenethiosulfonate
B
2-Bromobiphenyl
C
4-bromo-1,1'-biphenyl
D
3-bromobiphenyl
Conditions | Yield |
---|---|
at 135℃; for 72h; Further byproducts given; | A 0.2% B 20.9% C 6.9% D 12.7% E n/a |
bromobenzene
N-sulphinylphenylhydrazine
A
2-Bromobiphenyl
B
4-bromo-1,1'-biphenyl
C
diphenyl sulfide
D
3-bromobiphenyl
Conditions | Yield |
---|---|
at 135℃; for 72h; Further byproducts given; | A 20.9% B 6.9% C 0.8% D 12.7% E n/a |
pyridine
bromobenzene
dibenzoyl peroxide
A
2-phenylpyridine
B
2-Bromobiphenyl
C
4-bromo-1,1'-biphenyl
D
3-bromobiphenyl
Conditions | Yield |
---|---|
at 70℃; |
2-ethylhexyl 3-sulfanylpropanoate
3-bromobiphenyl
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 110℃; for 18h; Inert atmosphere; | 100% |
(3-bromophenyl)(pyridin-2-yl)methanone
3-bromobiphenyl
Conditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.666667h; Stage #2: (3-bromophenyl)(pyridin-2-yl)methanone In tetrahydrofuran; hexane at -78 - 20℃; for 16h; | 99% |
Conditions | Yield |
---|---|
With tris(1-adamantyl)phosphine; palladium diacetate; lithium hexamethyldisilazane In toluene at 70℃; for 0.55h; Inert atmosphere; | 99% |
3-bromobiphenyl
m-nitrobenzene boronic acid
1‐(3‐nitrophenyl)‐3‐phenylbenzene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In 1,2-dimethoxyethane; water for 16h; Suzuki Coupling; Inert atmosphere; Reflux; | 98% |
2,5-dichloro-2,5-dimethyl hexane
3-bromobiphenyl
6-(3-bromophenyl)-1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene
Conditions | Yield |
---|---|
With aluminium trichloride In 1,2-dichloro-ethane at 0℃; Condensation; | 97% |
3-bromobiphenyl
3-methoxyphenylboronic acid
3-methoxy-[1,1';3',1'']terphenyl
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; toluene for 3h; Suzuki coupling; Heating; | 97% |
3-bromobiphenyl
phenylmethanethiol
[1,1'-biphenyl]-3-yl(benzyl)sulfane
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; Inert atmosphere; Sealed tube; | 97% |
With tris-(dibenzylideneacetone)dipalladium(0); N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; Inert atmosphere; Sealed tube; | 97% |
3-bromobiphenyl
9-(4-biphenylyl)-3,3'-bicarbazole
Conditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl; 9-(4-biphenylyl)-3,3'-bicarbazole With potassium tert-butylate In toluene for 0.5h; Inert atmosphere; Stage #2: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; XPhos In toluene for 10h; Reflux; | 97% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 2h; Inert atmosphere; Reflux; | 95% |
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 100℃; for 24h; | 85% |
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine In toluene for 120h; Reflux; | 95% |
Conditions | Yield |
---|---|
With C43H59NO2PPd(1+)*CH3O3S(1-); caesium carbonate In toluene at 80℃; Schlenk technique; Inert atmosphere; | 95% |
3-bromobiphenyl
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 110℃; for 12h; | 95% |
3-bromobiphenyl
Conditions | Yield |
---|---|
Stage #1: (R)-2,2'-(2,2'-bis(methoxymethoxy)-1,1'-binaphthyl-3,3'-diyl)bis(4,4',5,5'-tetramethyl-1,3,2-dioxaborolane); 3-bromobiphenyl With tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane; water at 120℃; Alkaline conditions; Stage #2: With hydrogenchloride In 1,4-dioxane; methanol; dichloromethane; water at 80℃; | 95% |
Conditions | Yield |
---|---|
With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) at 80℃; for 5h; Hagihara coupling; | 94% |
Conditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl With n-butyllithium In tetrahydrofuran; hexanes at -78℃; Inert atmosphere; Stage #2: 2-(diisopropylsilyl)pyridine In tetrahydrofuran; hexanes at -78 - -30℃; Inert atmosphere; | 93% |
Stage #1: 3-bromobiphenyl With n-butyllithium In tetrahydrofuran; hexanes at -78℃; Inert atmosphere; Stage #2: 2-(diisopropylsilyl)pyridine In tetrahydrofuran; hexanes at -78 - 30℃; Inert atmosphere; | 93% |
3-bromobiphenyl
Conditions | Yield |
---|---|
With water-d2; potassium carbonate; silver carbonate; cyclohexyldiphenylphosphine In toluene at 120℃; for 12h; | 93% |
3-bromobiphenyl
3-iodo-1,1'-biphenyl
Conditions | Yield |
---|---|
With copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane; sodium iodide In 1,4-dioxane Reflux; Inert atmosphere; | 92% |
With iodine; sodium iodide In acetonitrile at 20℃; for 36h; Inert atmosphere; UV-irradiation; Green chemistry; | 87% |
3-bromobiphenyl
chlorodicyclohexylphosphane
[1,1'-biphenyl]-3-yldicyclohexylphosphane
Conditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl With n-butyllithium In diethyl ether; hexane at -20℃; for 2h; Inert atmosphere; Stage #2: chlorodicyclohexylphosphane In diethyl ether; hexane at 20℃; for 6h; Cooling; | 92% |
3-bromobiphenyl
4-tert-butyl-dimethylsilyloxyphenylboronic acid anhydride
[1,1’:3’,1’’-terphenyl]-4-ol
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water at 95℃; Suzuki reaction; | 91% |
Conditions | Yield |
---|---|
With methanol; magnesium at 20℃; | 91% |
With 2-H-1,3-di-tert-butyl-1,3,2-diazaphosphorinane; 2,2'-azobis(isobutyronitrile) In toluene at 90℃; for 5h; | 83% |
With sodium formate In water; isopropyl alcohol at 50℃; for 0.00222222h; microflow reactor; | 99 %Chromat. |
3-bromobiphenyl
fullerene-C60
Conditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl With iodine; magnesium In tetrahydrofuran at 20℃; for 2.5h; Inert atmosphere; Reflux; Stage #2: With copper(I) bromide dimethylsulfide complex In tetrahydrofuran at -78℃; for 0.333333h; Inert atmosphere; Stage #3: fullerene-C60 In tetrahydrofuran; 1,2-dichloro-benzene at -78 - 20℃; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine In 1,4-dioxane at 120℃; for 18h; | 90% |
9,9-dimethyl-9H-fluoren-2-ylamine
3-bromobiphenyl
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos In toluene at 108℃; for 4h; Buchwald-Hartwig Coupling; Inert atmosphere; | 90% |
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos In toluene at 108℃; for 4h; Inert atmosphere; | 74.94% |
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