Puyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesis.
Cas:657408-07-6
Min.Order:100 Gram
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Type:Manufacturers
inquiryBeiJing Greenchem Technology Co.,Ltd. was established by many people who are experienced in both management and professional technology in large and medium-sized pharmaceutical enterprises. It is located in Zhongguancun Technology Park, the synthesis
Cas:657408-07-6
Min.Order:0 Metric Ton
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:657408-07-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:657408-07-6
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryGIHI CHEMICALS exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, GIHI CHEMICALS is your best choice. pls contact with us freely for getting detailed produc
Cas:657408-07-6
Min.Order:1 Kilogram
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inquiryProduct description: Product name 2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl CAS number 657408-07-6 Assay ≥99% Appearance White powder Capacity 200mt/year Applicati
Cas:657408-07-6
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryHebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
Cas:657408-07-6
Min.Order:1 Metric Ton
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inquiryhigh quality Appearance:White or off white powder Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai
Cas:657408-07-6
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:657408-07-6
Min.Order:1
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:657408-07-6
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiry
Cas:657408-07-6
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.
Cas:657408-07-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryEnterprice standard Appearance:white Storage:dry Package:25kg net/paper drum Application:Diphenyl phosphine catalyst Transportation:by air , by sea Port:Shanghai
Cas:657408-07-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:657408-07-6
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:657408-07-6
Min.Order:1 Kilogram
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Type:Trading Company
inquiryName 2-Dicyclohexylphosphino-2',6'-dimethoxy-1,1'-biphenyl/Sphos Structural Formula CAS No. 657408-07-6
Cas:657408-07-6
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:657408-07-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: 2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl Synonyms: 98% SPhos;2-Dicyclohexylphosphino-2',6'-diMethoxy-1,1'-biphenyl ,98%;2-Dicyclohexylphosphino-2', 6-diMethoxybihenyl;2-DicyclohexylphosphiNA-2',6
Cas:657408-07-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:657408-07-6
Min.Order:1 Kilogram
FOB Price: $69.0 / 76.0
Type:Trading Company
inquiry2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl CAS:657408-07-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, speci
Cas:657408-07-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:657408-07-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:657408-07-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:657408-07-6
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
High qualityHangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service professional enterprise, Our company mainly engages in global phar
Cas:657408-07-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Cas:657408-07-6
Min.Order:0
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Type:Manufacturers
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua
Cas:657408-07-6
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:657408-07-6
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:657408-07-6
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:657408-07-6
Min.Order:100 Gram
Negotiable
Type:Other
inquirychlorodicyclohexylphosphane
2'-bromo-2,6-dimethoxybiphenyl
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Stage #1: 2'-bromo-2,6-dimethoxybiphenyl With n-butyllithium In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Cooling with acetone-dry ice; Stage #2: chlorodicyclohexylphosphane In tetrahydrofuran at 20 - 45℃; Inert atmosphere; | 88% |
Stage #1: 2'-bromo-2,6-dimethoxybiphenyl With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: chlorodicyclohexylphosphane In tetrahydrofuran; hexane at -78 - 20℃; | 3.32 g |
2-bromo-1-chlorobenzene
1,3-Dimethoxybenzene
chlorodicyclohexylphosphane
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Stage #1: 1,3-Dimethoxybenzene With n-butyllithium In tetrahydrofuran at 0 - 20℃; for 3.5h; Stage #2: 2-bromo-1-chlorobenzene In tetrahydrofuran at 0℃; for 0.5h; Stage #3: chlorodicyclohexylphosphane | 36% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
With 1,3-diphenyl-disiloxane In toluene at 110℃; Sealed tube; chemoselective reaction; | 87% |
2'-chloro-2,6-dimethoxy-1,1'-biphenyl
chlorodicyclohexylphosphane
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Stage #1: 2'-chloro-2,6-dimethoxy-1,1'-biphenyl With sec.-butyllithium In diethyl ether; cyclohexane at -78 - -45℃; Inert atmosphere; Stage #2: chlorodicyclohexylphosphane In diethyl ether; cyclohexane at -78℃; Inert atmosphere; | 48% |
2-bromo-1-chlorobenzene
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-BuLi / tetrahydrofuran; hexane / 5 h / 0 - 20 °C 1.2: 81 percent / tetrahydrofuran; hexane / 0.25 h / 0 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: 3.32 g / tetrahydrofuran; hexane / -78 - 20 °C View Scheme |
1,3-Dimethoxybenzene
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-BuLi / tetrahydrofuran; hexane / 5 h / 0 - 20 °C 1.2: 81 percent / tetrahydrofuran; hexane / 0.25 h / 0 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: 3.32 g / tetrahydrofuran; hexane / -78 - 20 °C View Scheme |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
(2,6-dimethoxyphenyl)boronic acid
1,2-dichloro-benzene
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 1,3,5,7-tetramethyl-8-phenyl-2,4,6-trioxa-8-phosphatricyclo[3.3.1.13,7]decane / toluene / 70 °C / Inert atmosphere 2.1: sec.-butyllithium / diethyl ether; cyclohexane / -78 - -45 °C / Inert atmosphere 2.2: -78 °C / Inert atmosphere View Scheme |
1,3-Dimethoxybenzene
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2,2,6,6-tetramethylpiperidinyl-lithium / diethyl ether; tetrahydrofuran / 36 h / -45 °C / Inert atmosphere; Sealed tube 2: diethyl ether / -78 °C / Inert atmosphere; Sealed tube View Scheme |
chlorobenzene
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2,2,6,6-tetramethylpiperidinyl-lithium / diethyl ether; tetrahydrofuran / 36 h / -45 °C / Inert atmosphere; Sealed tube 2: diethyl ether / -78 °C / Inert atmosphere; Sealed tube View Scheme |
2,6-dimethoxybiphenyl
chlorodicyclohexylphosphane
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In diethyl ether at -78℃; Inert atmosphere; Sealed tube; | 1.3 g |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
(tetrahydrothiophene)gold(I) chloride
chloro(dicyclohexyl(2',6'-dimethoxy-[1,1'-biphenyl]-2-yl)phosphine)gold(I)
Conditions | Yield |
---|---|
In dichloromethane for 1.75h; | 100% |
In dichloromethane at 20℃; for 1h; Darkness; |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Stage #1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane With sulfuric acid In dichloromethane at 0 - 40℃; for 24h; Stage #2: With sodium hydroxide In dichloromethane; water at 0℃; pH=~ 7.0; Cooling with ice; | 99% |
Stage #1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane With sulfuric acid In dichloromethane at 20℃; for 1h; Sealed tube; Stage #2: With sodium hydroxide In dichloromethane; water at 20℃; for 0.25h; pH=14; Sealed tube; Cooling with ice; regioselective reaction; | 85% |
Stage #1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane With sulfuric acid In dichloromethane at 0 - 40℃; for 24.7h; Inert atmosphere; Stage #2: With sodium hydroxide In dichloromethane; water at 0℃; pH=13; | 62% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; Schlenk technique; Inert atmosphere; | 99% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In tetrahydrofuran for 3h; Schlenk technique; Inert atmosphere; Glovebox; | 98% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.5h; Schlenk technique; Inert atmosphere; | 98% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; | 97.3% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
chloro(dicyclohexyl(2',6'-dimethoxy-[1,1'-biphenyl]-2-yl)phosphine)gold(I)
Conditions | Yield |
---|---|
Stage #1: hydrogen tetrachloroaurate(III) tetrahydrate With propyl sulfide In ethanol at 40℃; for 0.166667h; Stage #2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane In ethanol at 40℃; for 1h; | 97% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In acetone at 25℃; | 96% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
4-chloro-2-(dibenzo[b,d]furan-4-yl)pyridine
2-isopropenyl-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane
2-(dibenzo[b,d]furan-4-yl)-4-(prop-1-en-2-yl)pyridine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0) In water; ethyl acetate; toluene | 96% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
lithium bromide
Conditions | Yield |
---|---|
Stage #1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dihydrogen tetrachloropalladate(II) In acetone at 18 - 27℃; for 0.5h; Stage #2: lithium bromide In water; acetone | 96% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
Stage #1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane With sulfuric acid In dichloromethane for 1.5h; Sealed tube; Stage #2: With fuming sulphuric acid In dichloromethane at 0 - 20℃; for 0.533333h; Sealed tube; regioselective reaction; | 96% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Dihydroxy-isobutyl-boran
5,7-dichloro isoquinoline
5,7-diisobutylisoquinoline
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0) In hexane; water; toluene | 95% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
2-bromo-3-methylaniline
1-methylphenanthridin-6-amine
Conditions | Yield |
---|---|
With nitrogen In tetrahydrofuran; methanol; dichloromethane | 95% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
2-(2-chlorophenyl)ethanamine
chloro(2-dicyclohexylphosphino-2',6'-dimethoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II)
Conditions | Yield |
---|---|
In further solvent(s) treatment of palladium compd. with chlorobenzene deriv. and phosphine deriv. in methyl tert-butyl ether at 55°C; recrystn.; | 94% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
bis(1,5-cyclooctadiene)diiridium(I) dichloride
[IrCl(COD)(2-dicyclohexylphosphino-2',6'-dimethoxybiphenyl)]
Conditions | Yield |
---|---|
In toluene under Ar atm. using Schlenk techniques; mixt. of Ir complex and ligand in dry toluene was stirred at room temp. for 3 h; solvent evapd.; cold hexane added; suspn. filtered; washed (cold hexane); elem. anal.; | 94% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
3-bromo-9-phenyl-9H-carbazole
4-dibenzothiophene boronic acid
Conditions | Yield |
---|---|
94% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
(2'-amino-1,1'-biphenyl-2-yl)methanesulfonatopalladium(II) dimer
C26H35O2P*C13H13NO3PdS
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 93% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
bis[(trimethylsilyl)methyl](1,5-cyclooctadiene)palladium(II)
para-chlorotoluene
Conditions | Yield |
---|---|
In cyclohexane at 20℃; for 18h; Inert atmosphere; Glovebox; | 93% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; | 93% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In acetone at 18 - 27℃; for 1.16667h; | 93% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
N-phenyl-2-aminobiphenylpalladium methanesulfonate
C45H52NO5PPdS
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 92% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
bis(pentafluorophenyl)(1,5-cyclo-octadiene)palladium(II)
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 48h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; | 92% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.00166667h; Time; | 91% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
With dihydrogen peroxide In dichloromethane | 90% |
With oxygen In toluene at 20℃; Product distribution; Further Variations:; Reagents; Temperatures; | |
With dihydrogen peroxide In diethyl ether at 30℃; for 16h; |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Dihydroxy-isobutyl-boran
4,6-dichloro-1-(3,5-dimethylphenyl)isoquinoline
1-(3,5-dimethylphenyl)isoquinoline
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0) In dichloromethane; water; ethyl acetate; toluene | 90% |
Conditions | Yield |
---|---|
In acetone at 20℃; for 0.5h; | 90% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
Conditions | Yield |
---|---|
With sodium acetate In ethanol at 80℃; for 30h; Inert atmosphere; | 89% |
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane
dichloro bis(acetonitrile) palladium(II)
Pd(2-dicyclohexylphosphino-2’,6’-dimethoxybiphenyl)2Cl2
Conditions | Yield |
---|---|
In dichloromethane mixt. ligand and (CH3CN)2PdCl2 in CH2Cl2 was stirred; flash chromy. on silica; | 88% |
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