Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:678-45-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:678-45-5
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:678-45-5
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryDODECAFLUOROSUBERIC ACID CAS:678-45-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:678-45-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:678-45-5
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:678-45-5
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:678-45-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:678-45-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
Cas:678-45-5
Min.Order:1 Kilogram
FOB Price: $200.0
Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:678-45-5
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:678-45-5
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Type:Lab/Research institutions
inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate
Cas:678-45-5
Min.Order:0
Negotiable
Type:Trading Company
inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to light yellow crystal powder Storage:Room temperature with sealed well Package:according to the clients requirement Appl
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Cas:678-45-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
Cas:678-45-5
Min.Order:0
Negotiable
Type:Trading Company
inquiryUnited Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Cas:678-45-5
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Type:Lab/Research institutions
inquiryMolecular Formula C8H2F12O4.2(H2O) Molecular Weight 426.11 CAS Registry Number 678-45-5 NamePerfluorosuberic acid dihydrate …
Cas:678-45-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the Dodecafluorosuberic acid, CAS:678-45-5 with the most competitive price and the best q
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; sodium formate In N,N-dimethyl-formamide at 50℃; for 12h; | 89% |
Multi-step reaction with 2 steps 1: 55 percent / Na2S2O4, NaHCO3 / acetonitrile; H2O / 5 h / 70 °C 2: 17 percent / (NH4)2S2O8 / dimethylformamide / 4 h / 40 °C View Scheme | |
Multi-step reaction with 2 steps 1: 55 percent / Na2S2O4, NaHCO3 / acetonitrile; H2O / 5 h / 70 °C 2: 38 percent / (NH4)2S2O8 / dimethylformamide / 4 h / 40 °C View Scheme |
(n-perfluoro hexyl) 1,6-di(magnesiumbromide)
carbon dioxide
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
In tetrahydrofuran reaction at -70°C, 22 hours;; | 81% |
In tetrahydrofuran reaction at -70°C, 22 hours;; | 81% |
(E)-2,2,3,3,4,4,5,5,6,6,7,7,8,9-Tetradecafluoro-dec-8-en-1-ol
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
With potassium permanganate In acetic acid Heating; | 60% |
sodium perfluoroctane-1,8-disulfinate
allyl bromide
A
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
B
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-hexadecafluoro-1,13-tetradecadiene
Conditions | Yield |
---|---|
With ammonium peroxydisulfate In N,N-dimethyl-formamide at 40℃; for 4h; | A 17% B 55% |
sodium perfluoroctane-1,8-disulfinate
propargyl bromide
A
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
B
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-hexadecafluoro-1,2,12,13-tetradecatetraene
Conditions | Yield |
---|---|
With ammonium peroxydisulfate In N,N-dimethyl-formamide at 40℃; for 4h; | A 38% B 43% |
octadecafluoro-deca-1,9-diene
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
With potassium permanganate In acetone |
1H,1H,9H-hexadecafluoro-1-nonanol
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 77 percent / NaH, LiBr / diethyl ether / -20 °C 2: 60 percent / KMnO4 / acetic acid / Heating View Scheme |
1,2-dichloro-1H,2H,6H-undecafluoro-6-iodo-hexane
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Zn, Ac2O / CH2Cl2 2: Zn, Ac2O / acetic acid 3: aq. KMnO4 / acetone View Scheme |
1,2,9,10-tetrachloro-1H,2H,9H,10H-octadecafluoro-decane
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Zn, Ac2O / acetic acid 2: aq. KMnO4 / acetone View Scheme |
3,5-bis(3,4-diethyl-5-formyl-1H-pyrrol-2-ylmethyl)-1H-pyrazole
3,3',4,4'-tetraaminobiphenyl
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
Stage #1: 3,5-bis(3,4-diethyl-5-formyl-1H-pyrrol-2-ylmethyl)-1H-pyrazole; 3,3',4,4'-tetraaminobiphenyl In methanol at 50℃; for 0.25h; Inert atmosphere; Stage #2: 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid In methanol for 31h; Inert atmosphere; Reflux; | 94% |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioyl dichloride
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide for 4h; Inert atmosphere; Reflux; | 86% |
With thionyl chloride; N,N-dimethyl-formamide for 4h; Inert atmosphere; Reflux; | 86% |
With thionyl chloride; N,N-dimethyl-formamide for 4h; Inert atmosphere; Reflux; | 86% |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
dodecafluoro-1,6-diiodohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: KI / 270 - 375 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: (esterification) View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: KI / 270 - 375 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide (4-[1-phenyl-1H-[1,2,3]triazol-4-yl]phenyl)amide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide pyren-1-ylamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide (4-phenylthiazol-2-yl)amide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide [4-(1-phenyl-1H-[1,2,3]triazol-5-yl)phenyl]amide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide naphthalen-1-ylamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid biphenyl-3-ylamide hydroxyamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide naphthalen-2-ylamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid biphenyl-2-ylamide hydroxyamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid anthracen-2-ylamide hydroxyamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide phenanthren-9-ylamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid hydroxyamide phenyl amide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: thionyl chloride / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2.1: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3.1: triethylamine / tetrahydrofuran / 5.5 h / 5 - 20 °C / Inert atmosphere 3.2: 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: thionyl chloride / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2.1: 1,4-dioxane / 2 h / 100 °C / Inert atmosphere; Cooling 3.1: tetrahydrofuran / 0.5 h / Inert atmosphere; Cooling 3.2: 5 h / 5 - 20 °C 3.3: 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid anthracen-1-ylamide hydroxyamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice 4: hydroxylamine / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / N,N-dimethyl-formamide 2: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / Cooling with ice 3: triethylamine; hydroxylamine hydrochloride / tetrahydrofuran / 24 h / 20 °C View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice View Scheme |
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux 2: 2 h / 100 °C / Inert atmosphere; Cooling with ice 3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice View Scheme |
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