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inquiry2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
With zinc In ethanol at 0℃; | 86% |
Ethylene 2-(methacryloyloxy)ethyl phosphate
trimethylamine
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
In acetonitrile at 50℃; for 48h; Ring cleavage; Amination; | 37% |
In acetonitrile at -20 - 60℃; for 36h; | |
In acetonitrile at -20 - 60℃; for 16h; Sealed tube; | 3.1 g |
2-Bromoethyl 2-cyanoethyl-2-(methacryloyloxy)ethyl phosphate
trimethylamine
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
In acetonitrile at 75℃; for 24h; Amination; |
2-methyl-2-propenoic acid 2-hydroxyethyl ester
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: N,N-diisopropylamine tetrazolide / dichloromethane / 0.33 h 2: 4,5-dichloroimidazole / acetonitrile / 16 h / 20 °C 3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 20 °C 4: acetonitrile / 24 h / 75 °C View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / tetrahydrofuran / 4 h / -30 - -20 °C 2: acetonitrile / 16 h / -20 - 60 °C / Sealed tube View Scheme |
Ethylenedioxy-2-(methacryloyloxy)ethoxyphosphine
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: trimethylamine-N-oxide / acetonitrile / 0.67 h 2: acetonitrile / 48 h / 50 °C View Scheme |
2-Bromoethoxy-2-(cyanoethoxy)-2-(methacryloyloxy)ethoxyphosphine
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 20 °C 2: acetonitrile / 24 h / 75 °C View Scheme |
2-((2-cyanoethoxy)(diisopropylamino)phosphinoxy)ethyl methacrylate
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 4,5-dichloroimidazole / acetonitrile / 16 h / 20 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 20 °C 3: acetonitrile / 24 h / 75 °C View Scheme |
2-methyl-2-propenoic acid 2-hydroxyethyl ester
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
In acetonitrile |
2-methacryloyloxyethyl phosphorylcholine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: trichlorophosphate; triethylamine / acetonitrile / 2.5 h / -5 - 20 °C 2.1: triethylamine / 2 h / 0 - 20 °C 2.2: 1 h / 0 - 20 °C 3.1: zinc / ethanol / 0 °C View Scheme |
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