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inquiryProduct Description Product website: http://www.finerchem.com Product Name 3,5-Dimethoxybenzyl alcohol CAS No.
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inquiry3,5-Dimethoxybenzyl alcohol Basic information Product Name: 3,5-Dimethoxybenzyl alcohol Synonyms: RARECHEM AL BD 0065;3,5-DIMETHOXYBENZYL ALCOHOL;(3,5-DIMETHOXYPHENYL)METHANOL;3,5-DIMETH
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inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryProducts: 3,5-Dimethoxybenzyl alcohol Cas No.: 705-76-0 Molecular Formula: C9H12O3 Molecular Weight: 168.19 Molecular Structure:
Cas:705-76-0
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inquiryProduct name: 3,5-Dimethoxybenzyl Alcohol CAS No.:705-76-0 Molecule Formula:C9H12O3 Molecule Weight:168.19 Purity: 98.0% Package: 25kg/drum Description:White or off-white powder Manufacture Standards:Enterprise Standard TESTING I
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryConditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 20℃; for 0.166667h; | 100% |
With sodium tetrahydroborate In methanol at 20℃; for 1h; | 100% |
With sodium tetrahydroborate In ethanol at 20℃; for 0.5h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; 4-methyltetrahydropyran at 0 - 20℃; for 1h; Inert atmosphere; Green chemistry; | 100% |
With lithium aluminium tetrahydride In tetrahydrofuran | 99% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 1.33333h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol; 1,2-dimethoxyethane for 3h; Heating; | 99% |
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 1h; | 99% |
With lithium aluminium tetrahydride In diethyl ether Heating; | 98% |
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate In methanol at 0 - 20℃; for 0.666667h; chemoselective reaction; | 98% |
3,5-dimethoxy((triethylsilyloxy)methyl)benzene
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate In methanol at 0 - 20℃; for 0.25h; chemoselective reaction; | 91% |
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate In methanol at 0 - 20℃; for 1h; chemoselective reaction; | 89% |
formaldehyd
3,5-dimethoxyphenylboronic acid
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 1-(2-bromophenyl)-3-(2,6-diisopropylphenyl)-4,5-dihydroimidazolinium chloride In tetrahydrofuran; water at 100℃; for 2h; Inert atmosphere; Sealed tube; | 86% |
ethyl 3,5-dimethoxybenzoate
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 3h; Reduction; Heating; | 84% |
With lithium aluminium tetrahydride In diethyl ether for 1h; Heating; | |
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; |
(1,1-dimethylethyl)diphenylsilyl 3,5-dimethoxybenzyl ether
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate In methanol at 0 - 20℃; for 3h; chemoselective reaction; | 84% |
3,5-dimethoxyphenyl trifluoromethanesulfonate
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With sodium carbonate; bis(dibenzylideneacetone)-palladium(0); ruphos In 1,4-dioxane; water for 10h; Suzuki-Miyaura cross-coupling; Inert atmosphere; Reflux; | 80.9% |
Conditions | Yield |
---|---|
With sodium carbonate; bis(dibenzylideneacetone)-palladium(0); ruphos In 1,4-dioxane; water for 48h; Suzuki-Miyaura cross-coupling; Inert atmosphere; Reflux; | 80.9% |
3,5-dimethoxybenzaldehdye
A
3,5-dimethoxybenzyl alcohol
B
3,5-dimethoxybenzoic acid
Conditions | Yield |
---|---|
With potassium hydroxide at 100℃; for 0.0833333h; solvent-free Cannizzaro reaction; | A 41% B 49% |
With potassium hydroxide auf dem Dampfbad; |
3,5-dimethoxybenzamide
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With sodium amalgam; ethanol |
methanol
3,5-dimethoxybenzyltrimethylammonium iodide
A
3,5-dimethoxybenzyl alcohol
B
1,3-dimethoxy-5-methylbenzene
C
trimethylammonium iodide
D
dimethylamine hydriodide
Conditions | Yield |
---|---|
With water at 30℃; for 2h; Irradiation; | A 42 % Chromat. B 31 % Chromat. C 70 % Chromat. D 30 % Chromat. |
Conditions | Yield |
---|---|
With water at 30℃; for 2h; Irradiation; |
Conditions | Yield |
---|---|
With water at 30℃; for 2h; Irradiation; |
carbon dioxide
2-bromo-3,5-dimethoxybenzyl alcohol
A
5,7-dimethoxyphthalide
B
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
3-(3,5-Dimethoxy-benzyl)-3H-purin-6-ylamine
A
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
In water Mechanism; Product distribution; Quantum yield; Irradiation; other meta-substituted N-arylmethyladenines and also other solvents investigated; |
Conditions | Yield |
---|---|
In water at 30℃; for 2h; Mechanism; Irradiation; >/= 260 nm; |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; potassium carbonate 1.) acetone; 2.) THF; Multistep reaction; |
3,5-dimethoxybenzyl acetate
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With potassium hydroxide |
3,5-dimethoxybenzyl acetate
A
3,5-dimethoxybenzyl alcohol
B
1,3-dimethoxy-5-ethylbenzene
Conditions | Yield |
---|---|
In water Irradiation; Title compound not separated from byproducts; | A 92 % Spectr. B 0.2 % Spectr. |
3,5-dimethoxybenzaldehdye
O-(4-methoxyphenyl)-N,N-diethylthiocarbamate
A
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium 1) cyclohexane, THF, -78 deg C, 2 h; 2) cyclohexane, THF, -78 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
In acetonitrile at 30℃; Kinetics; Further Variations:; wavelength of UV-light; photolysis; UV-irradiation; |
Conditions | Yield |
---|---|
In acetonitrile at 30℃; Kinetics; photolysis; UV-irradiation; |
ethane-1,2-dithiol
2-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxy-6-methoxy-benzaldehyde
A
3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With zinc(II) chloride In dichloromethane |
A
N-Nitrosodiethylamine
B
3,5-dimethoxybenzyl alcohol
C
3,5-dimethoxybenzaldehdye
D
3,5-dimethoxybenzaldoxime
Conditions | Yield |
---|---|
With water In acetonitrile Product distribution; Quantum yield; Further Variations:; Reagents; Solvents; UV-irradiation; | A 74 % Chromat. B 9 % Chromat. C 5 % Chromat. D 37 % Chromat. |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: NaOH 2: SOCl2 3: 92 percent / LiAlH4 / diethyl ether View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetone / 4 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 2.17 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetone / 4 h / Reflux 2: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C View Scheme |
Conditions | Yield |
---|---|
With phosphorus tribromide In benzene at 20℃; | 100% |
With phosphorus tribromide In 1,4-dioxane at 40℃; for 1h; Inert atmosphere; | 99% |
Stage #1: 3,5-dimethoxybenzyl alcohol With triphenylphosphine In dichloromethane at 20℃; for 0.166667h; Appel reaction; Stage #2: With carbon tetrabromide In dichloromethane at -78 - -50℃; Appel reaction; | 98% |
di(succinimido) carbonate
3,5-dimethoxybenzyl alcohol
3,5-dimethoxybenzyl-N-succinimidyl carbonate
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 20℃; for 0.333333h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With trichlorophosphate at 0 - 75℃; for 2h; Vilsmeier-Haack Formylation; | 100% |
Conditions | Yield |
---|---|
With silica-supported Jones reagent In dichloromethane for 0.00269444h; | 99.5% |
With 1,2-dimethyl-3-[6-(methylsulfinyl)hexyl]-1H-imidazolium triflate; oxalyl dichloride; triethylamine In dichloromethane; acetonitrile at -78 - 20℃; Swern oxidation; | 97% |
With Dess-Martin periodane In dichloromethane at 0℃; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With silica-supported Jones reagent In dichloromethane for 0.035h; | 99.3% |
With C15H27Br2CoN3; potassium hydroxide In toluene at 140℃; for 16h; Cannizzaro Reaction; Inert atmosphere; Sealed tube; | 86% |
With potassium phosphate; carbon dioxide; CrH6Mo6O24(3-)*3H3N*3H(1+) In dimethyl sulfoxide at 80℃; under 750.075 Torr; for 24h; Green chemistry; | 82% |
3,5-dimethoxybenzyl alcohol
2-iodo-3,5-bis(methoxy)benzenemethanol
Conditions | Yield |
---|---|
With iodine; silver trifluoroacetate | 99% |
With N-iodo-succinimide In N,N-dimethyl-formamide at 0 - 40℃; for 3h; | 99% |
With iodine; silver trifluoroacetate In chloroform for 0.25h; | 94% |
3,5-dimethoxybenzyl alcohol
acetic anhydride
3,5-dimethoxybenzyl acetate
Conditions | Yield |
---|---|
With tin(IV) tetraphenylporphyrin perchlorate at 20℃; for 0.0833333h; | 99% |
ruthenium trichloride In acetonitrile at 20℃; for 0.416667h; | 95% |
With pyridine | 93% |
With pyridine at 20℃; for 3h; Acetylation; | 86% |
In pyridine |
3,5-dimethoxybenzyl alcohol
2-bromo-3,5-dimethoxybenzyl alcohol
Conditions | Yield |
---|---|
With N-Bromosuccinimide In tetrachloromethane at 70℃; for 0.666667h; | 98% |
With N-Bromosuccinimide In chloroform at 45℃; | 96% |
With N-Bromosuccinimide In dichloromethane at 0 - 25℃; for 12.5h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; benzyl chloride In tetrahydrofuran at 65 - 70℃; for 20h; Inert atmosphere; Schlenk technique; | 98% |
With bismuth(lll) trifluoromethanesulfonate; dichloro bis(acetonitrile) palladium(II); oxygen; potassium carbonate at 60℃; for 3h; Schlenk technique; | 91% |
With palladium 10% on activated carbon; oxygen; sodium carbonate at 120℃; under 15001.5 Torr; for 1.5h; Microwave irradiation; Green chemistry; | 36% |
Conditions | Yield |
---|---|
With pyridine; thionyl chloride In diethyl ether at 20℃; Cooling with ice; | 97% |
With trichlorophosphate In methanol for 2h; Time; Reflux; | 96.7% |
With trichlorophosphate for 2h; Time; Reflux; | 96.7% |
3,5-dimethoxybenzyl alcohol
propargyl bromide
1,3-dimethoxy-5-{[(prop-2-yn-1-yl)oxy]methyl}benzene
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 10h; | 97% |
3,5-dimethoxybenzyl alcohol
Methyltriphenylphosphonium bromide
3,5-dimethoxystyrene
Conditions | Yield |
---|---|
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 1h; Stage #2: 3,5-dimethoxybenzyl alcohol In tetrahydrofuran at 0 - 20℃; for 2h; | 96% |
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; hexane at 0℃; Wittig type reaction; Stage #2: 3,5-dimethoxybenzyl alcohol With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride In tetrahydrofuran; hexane for 8h; Wittig type reaction; Inert atmosphere; Reflux; | 40% |
Conditions | Yield |
---|---|
With pyridine; dmap; 4-methyltetrahydropyran at 20℃; for 0.5h; Inert atmosphere; Green chemistry; | 96% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane | 93% |
With pyridine In benzene Ambient temperature; |
3,5-dimethoxybenzyl alcohol
N,N-dimethyl-formamide
2-(chloromethyl)-4,6-dimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 25℃; for 0.333333h; Stage #2: 3,5-dimethoxybenzyl alcohol at 25 - 75℃; for 2h; Further stages.; | 93% |
With trichlorophosphate at 75℃; for 2h; Formylation; substitution; | 93% |
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 0 - 20℃; for 0.5h; Vilsmeier-Haack Formylation; Inert atmosphere; Stage #2: 3,5-dimethoxybenzyl alcohol at 0 - 75℃; for 2h; Vilsmeier-Haack Formylation; Inert atmosphere; regioselective reaction; | 93% |
3,5-dimethoxybenzyl alcohol
2-(chloromethyl)-4,6-dimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With trichlorophosphate In N,N-dimethyl-formamide | 93% |
3,5-dimethoxybenzyl alcohol
3,4-dichlorbenzoic acid
3,5-dimethoxybenzyl 3,4-dichlorobenzoate
Conditions | Yield |
---|---|
With C18H20N2O4; Nb-TPP In tetrahydrofuran at 0 - 20℃; Mitsunobu reaction; | 93% |
3,5-dimethoxybenzyl alcohol
aniline
(E)-N-(3,5-dimethoxybenzylidene)aniline
Conditions | Yield |
---|---|
With CuO*Fe3O4; sodium hydroxide In toluene at 100℃; for 96h; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With dmap; triethylamine at 0 - 20℃; for 2h; | 93% |
3,5-dimethoxybenzyl alcohol
2-hydroxymethyl-6-methoxy-1,4-benzoquinone
Conditions | Yield |
---|---|
With C33H33N5O8Ru; dihydrogen peroxide In ethyl acetate at 20℃; for 15h; Schlenk technique; Green chemistry; chemoselective reaction; | 93% |
3,5-dimethoxybenzyl alcohol
3,5-dimethoxy-benzonitrile
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; TEMPOL; ammonia; copper(l) chloride In water; acetonitrile at 20℃; for 24h; | 93% |
With ammonia; oxygen In 1,4-dioxane for 2h; Reflux; | 90% |
With ammonia; oxygen In ethanol; water for 2h; Reflux; | 90% |
3,5-dimethoxybenzyl alcohol
benzoyl chloride
3,5-dimethoxybenzyl benzoate
Conditions | Yield |
---|---|
With pyridine | 92% |
3,5-dimethoxybenzyl alcohol
tert-butylchlorodiphenylsilane
(1,1-dimethylethyl)diphenylsilyl 3,5-dimethoxybenzyl ether
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 5h; | 92% |
With 4-methylpyridine-1-oxide In dichloromethane at 20℃; Molecular sieve; | 92% |
3,5-dimethoxybenzyl alcohol
exo-7-oxabicyclo[2.2.1]hept-4-ene-2,3-dicarboximide
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 18h; Inert atmosphere; | 92% |
3,5-dimethoxybenzyl alcohol
anthranilic acid amide
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; potassium hydroxide In toluene at 100℃; for 12h; | 92% |
Conditions | Yield |
---|---|
With C30H43ClCoN2P3(1+)*Cl(1-); potassium triethylborohydride; potassium hydroxide In toluene at 140℃; for 24h; Inert atmosphere; Glovebox; Sealed tube; | 92% |
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