CAS No.72-63-9,Metandienone Suppliers,MSDS download

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Synthetic route

: 74-83-9
methyl bromide

: 897-06-3
Androsta-1,4-diene-3,17-dione

: 72-63-9
metandienone

Conditions

Conditions	Yield
Stage #1: methyl bromide With magnesium In tetrahydrofuran at 40 - 45℃; Stage #2: Androsta-1,4-diene-3,17-dione In toluene at 50 - 55℃;	94.6%
Stage #1: methyl bromide With magnesium In tetrahydrofuran at 40 - 45℃; Stage #2: Androsta-1,4-diene-3,17-dione In toluene at 50 - 55℃;	94.6%
Stage #1: methyl bromide With magnesium In tetrahydrofuran at 40 - 45℃; Stage #2: Androsta-1,4-diene-3,17-dione In toluene at 50 - 55℃; Stage #3: With hydrogenchloride In water at 50 - 55℃; pH=2 - 3;	93.8%

: 74-87-3
methylene chloride

: 897-06-3
Androsta-1,4-diene-3,17-dione

: 72-63-9
metandienone

Conditions

Conditions	Yield
Stage #1: methylene chloride With magnesium In tetrahydrofuran at 30 - 35℃; Stage #2: Androsta-1,4-diene-3,17-dione In tetrahydrofuran at 50 - 55℃;	92.5%
Stage #1: methylene chloride With magnesium In tetrahydrofuran at 30 - 35℃; Stage #2: Androsta-1,4-diene-3,17-dione In tetrahydrofuran at 50 - 55℃;	92.5%
Stage #1: methylene chloride With magnesium In tetrahydrofuran at 30 - 35℃; Stage #2: Androsta-1,4-diene-3,17-dione In tetrahydrofuran at 50 - 55℃; Stage #3: With hydrogenchloride In water at 50 - 55℃; pH=2 - 3;	92.5%

: 897-06-3
Androsta-1,4-diene-3,17-dione

: 74-88-4
methyl iodide

: 72-63-9
metandienone

Conditions

Conditions	Yield
Stage #1: methyl iodide With magnesium In diethyl ether at 30 - 35℃; Stage #2: Androsta-1,4-diene-3,17-dione In benzene at 50 - 55℃;	90.8%
Stage #1: methyl iodide With magnesium In diethyl ether at 30 - 35℃; Stage #2: Androsta-1,4-diene-3,17-dione In benzene at 50 - 55℃;	90.8%
Stage #1: methyl iodide With magnesium In diethyl ether at 30 - 35℃; Stage #2: Androsta-1,4-diene-3,17-dione In benzene at 50 - 55℃; Stage #3: With hydrogenchloride In water at 50 - 55℃; pH=2 - 3;	90.8%

: 58-18-4
17-methyltestosterone

: 72-63-9
metandienone

Conditions

Conditions	Yield
With tert-butyldimethylsilyl chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone In 1,4-dioxane at 0 - 20℃; for 48h;	78%
With selenium(IV) oxide
mit Hilfe von Didymella lycopersici;

: 5781-53-3
monomethyl oxalyl chloride

: 72-63-9
metandienone

: methyl ((8R,9S,10R,13S,14S,17S)-10,13,17-trimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl) oxalate

Conditions

Conditions	Yield
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 12h; Inert atmosphere;	95%

: 72-63-9
metandienone

: 64760-67-4
(8S,9S,10R,13S,14S)-10,13,17-trimethyl-7,8,9,11,12,13,14,15-octahydro-6H-cyclopenta[a]phenanthren-3(10H)-one

Conditions

Conditions	Yield
With Amberlyst-15 In dichloromethane at 20℃; for 6h;	90%

: 72-63-9
metandienone

A: 15α,17β-dihydroxy-17α-methyl-1,4-androstadien-3-one

B: 33526-41-9
6β,17β-dihydroxy-17α-methyl-1,4-androstadien-3-one

Conditions

Conditions	Yield
With Penicillium notatum KCH 904 In water; acetone at 27℃; for 264h; Enzymatic reaction;	A 83% B 9%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 72-63-9
metandienone

: C30H46N2O6

Conditions

Conditions	Yield
With cerium(III) chloride; tetrabutyl-ammonium chloride In acetonitrile for 48h; Inert atmosphere; Irradiation; diastereoselective reaction;	71%

: 72-63-9
metandienone

: 77702-25-1
17,17-dimethyl-18-norandrosta-1,4,13(14)-trien-3-one

Conditions

Conditions	Yield
With hydrogenchloride at 60℃; for 0.5h;	60%
With hydrogenchloride In methanol; water for 16h; Reflux;

: 72-63-9
metandienone

: androsta-3,5-dien-17β-ol, 17-methyl-

Conditions

Conditions	Yield
Stage #1: metandienone With C19H26ClIrN3O(1+)*Cl(1-) In water; acetonitrile at 80℃; for 0.166667h; Green chemistry; Stage #2: With formic acid In water; acetonitrile at 80℃; for 4h; Green chemistry;	35%

: 72-63-9
metandienone

: 58-18-4
17-methyltestosterone

Conditions

Conditions	Yield
With thallium(III) nitrate trihydrate In diethylene glycol dimethyl ether for 24h; Ambient temperature;	34%

: 72-63-9
metandienone

: 2616-64-0
UDP-glucuronic acid

A: 1062581-61-6
17β-methyl-5β-androst-1-ene-17α-ol-3α-O-glucuronide

B: 17α-methyl-5β-androstane-17β-ol-3α-O-glucuronide

Conditions

Conditions	Yield
With liver microsomes from Aroclor 1254-induced male Wistar rat In methanol; phosphate buffer at 37℃; pH=7.4;	A 25% B n/a

...Expand

: 72-63-9
metandienone

A: 1,17α-dimethyl-1,3,5(10)-estratriene-3,17β-diol

B: (3aα,8aα,8bβ)-dodecahydro-5aβ,6α-dimethyl-6β-hydroxy-2'-methyl-as-indacene-3(R)-spiro-(2',5'-cyclohexadienone)

Conditions

Conditions	Yield
With axenic culture of strain T76 Scenedesmus quadricauda	A 11% B 21%
With axenic culture of strain T76 of Scenedesmus quadricauda	A 11% B 21%

: 72-63-9
metandienone

: anti-17α-Methyl-17β-hydroxy-Δ1,4-androstadien-3-N-chlorimin

Conditions

Conditions	Yield
(i) MeNH2, MeOH, (ii) aq. Ca(OCl)2, NH3, NH4Cl; Multistep reaction;

: 110-86-1
pyridine

: 72-63-9
metandienone

: 143579-41-3
methandienone 17β-sulfate pyridinium salt

Conditions

Conditions	Yield
With chlorosulfonic acid 1.) -5 deg C, 2.) RT, 3 h; Yield given. Multistep reaction;

: 72-63-9
metandienone

: 119888-55-0
metanedienone-17-sulfate

Conditions

Conditions	Yield
With sulfur trioxide pyridine complex In N,N-dimethyl-formamide for 12h; Ambient temperature;	3.8 g

: 24589-78-4
N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide

: 72-63-9
metandienone

: 136693-32-8
(8R,9S,10R,13S,14S,17S)-10,13,17-Trimethyl-3,17-bis-trimethylsilanyloxy-8,9,10,11,12,13,14,15,16,17-decahydro-7H-cyclopenta[a]phenanthrene

Conditions

Conditions	Yield
With ammonium iodide In ethyl acetate for 1h; Heating;	97 % Chromat.
With ammonium iodide; 2-hydroxyethanethiol at 60℃; for 0.333333h;
With ammonium iodide; ethanethiol In acetonitrile at 80℃; for 0.5h;

: 72-63-9
metandienone

: 13712-20-4
3,5-Dioxo-17β-hydroxy-17α-methyl-10(5->4)-abeo-Δ1-androsten

Conditions

Conditions	Yield
(i) PhCO3H, CHCl3, (ii) (UV-irradiation), dioxane; Multistep reaction;

: 67-56-1
methanol

: 72-63-9
metandienone

: 94761-63-4
1-Hydroxy-4.17.17-trimethyl-7.8.9.11.12.15.16.17-octahydro-6H-cyclopentaphenanthren

Conditions

Conditions	Yield
With hydrogenchloride

: 67-56-1
methanol

: 72-63-9
metandienone

: 96671-98-6
13-Chlor-1-methoxy-4.17.17-trimethyl-13ξ-gonatrien-(A)

Conditions

Conditions	Yield
With hydrogenchloride

: 67-56-1
methanol

: 72-63-9
metandienone

: 77702-25-1
17,17-dimethyl-18-norandrosta-1,4,13(14)-trien-3-one

Conditions

Conditions	Yield
With hydrogenchloride

: 72-63-9
metandienone

: 2694-97-5
17β-Hydroxy-17α-methyl-Δ1.5-androstadien-3-on

Conditions

Conditions	Yield
With potassium tert-butylate In dimethyl sulfoxide

: 72-63-9
metandienone

A: 1,17α-dimethyl-1,3,5(10)-estratriene-3,17β-diol

B: (3S,3aS,5aS,6R,6aR,11aS,11bS)-3,6-Dihydroxy-3,3a,6-trimethyl-1,2,3,3a,4,5,5a,6,6a,7,10,11,11a,11b-tetradecahydro-indeno[5,4-f]azulen-8-one

C: C20H28O2

D: 5α,17β-dihydroxy-17α-methyl-androst-1-en-3-one

Conditions

Conditions	Yield
With water In 1,4-dioxane at 24℃; for 480h; Irradiation; green alga T76 Scenedesmus quadricauda; Yield given. Further byproducts given. Yields of byproduct given;

...Expand

: 72-63-9
metandienone

A: 1,17α-dimethyl-1,3,5(10)-estratriene-3,17β-diol

B: C20H28O2

C: 5β,17β-dihydroxy-17α-methyl-androst-1-en-3-one

D: 5α,17β-dihydroxy-17α-methyl-androst-1-en-3-one

Conditions

Conditions	Yield
In 1,4-dioxane at 24℃; for 480h; Irradiation; green alga T76 Scenedesmus quadricauda; Yield given. Further byproducts given. Yields of byproduct given;
With water In 1,4-dioxane at 24℃; for 480h; Irradiation; green alga T76 Scenedesmus quadricauda; Yield given. Further byproducts given. Yields of byproduct given;

...Expand

: 72-63-9
metandienone

A: 571-03-9
17β-hydroxy-17α-methylandrost-4-en-3β-ol

B: (3R,8R,9S,10R,13S,14S,17S)-10,13,17-Trimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,17-diol

Conditions

Conditions	Yield
With sodium tetrahydroborate In ethanol at 20℃; for 2h;

: 72-63-9
metandienone

: 33526-40-8
17α-17-hydroxy-17-methylandrosta-1,4-dien-3-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 3.8 g / sulfur trioxide pyridine complex / dimethylformamide / 12 h / Ambient temperature 2: H2O / 24 h View Scheme

: 72-63-9
metandienone

: 17-epimetandienone,bis-TMS

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 3.8 g / sulfur trioxide pyridine complex / dimethylformamide / 12 h / Ambient temperature 2: H2O / 24 h 3: trimethylsilylimidazole / 0.17 h / 60 °C 4: trimethyliodosilane / 0.25 h / 60 °C View Scheme

: 72-63-9
metandienone

: 73024-97-2
(8R,9S,10R,13S,14S,17R)-10,13,17-Trimethyl-17-trimethylsilanyloxy-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-3-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 3.8 g / sulfur trioxide pyridine complex / dimethylformamide / 12 h / Ambient temperature 2: H2O / 24 h 3: trimethylsilylimidazole / 0.17 h / 60 °C View Scheme

: 72-63-9
metandienone

: 2694-98-6
17α-Methyl-androsta-1,5-dien-3β,17β-diol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: KOtBu / dimethylsulfoxide 2: NaBH4 / methanol View Scheme

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Raw Materials

58-18-4

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