CAS No.723-97-7,1-Methoxy-9H-carbazole-3-carbaldehyde Suppliers

Dayang Chem (Hangzhou) Co.,Ltd.

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Qingdao Beluga Import and Export Co., LTD

1-Methoxy-9H-carbazole-3-carbaldehyde CAS:723-97-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qual

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Shandong Hanjiang Chemical Co., Ltd.

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

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Zibo Hangyu Biotechnology Development Co., Ltd

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Henan Tianfu Chemical Co., Ltd.

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Antimex Chemical Limied

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Hangzhou Fandachem Co.,Ltd

Murrayanine cas 723-97-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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Henan Kanbei Chemical Co.,LTD

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1-Methoxy-9H-carbazole-3-carbaldehyde

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Shanghai Chinqesen Biotechnology Co., Ltd.

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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Henan Wising Chem Co., Ltd

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Nanjing Raymon Biotech Co., Ltd.

MurrayanineAppearance:Pls see the Details Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:

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Chemical Co.Ltd

MurrayanineAppearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them from sunsh

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Synthetic route

: 3909-78-2
koenoline

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With manganese(IV) oxide In acetone at 20℃; for 12h;	98%
With manganese(IV) oxide In tetrachloromethane at 20℃; for 12h;	81%
for 144h; Ambient temperature;	10%
With manganese(IV) oxide In tetrachloromethane for 6h; Ambient temperature; Yield given;

: 4532-33-6
1-methoxy-3-methylcarbazole

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In tetrahydrofuran; methanol; water at 20℃; for 0.5h;	95%
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In benzene for 4h; Ambient temperature;	70%

: 1384959-52-7
1-bromo-9H-carbazole-3-carbaldehyde

: 124-41-4
sodium methylate

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With methanol; copper(l) iodide In N,N-dimethyl-formamide at 120℃; for 5h; Inert atmosphere;	88%

: 954378-08-6
4-[(2-bromophenyl)amino]-3-methoxybenzaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With sodium carbonate; lithium chloride; tetrakis(triphenylphosphine) palladium(0) In acetonitrile for 48h; Heating;	85%

: 808114-06-9
3-methoxy-4-(phenylamino)benzaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With acetic acid; palladium diacetate at 160℃; for 12h;	73%
With copper diacetate; palladium diacetate; acetic acid at 110 - 130℃; Reagent/catalyst; Inert atmosphere;	68%
Stage #1: 3-methoxy-4-(phenylamino)benzaldehyde With palladium diacetate; potassium carbonate; Trimethylacetic acid at 115℃; for 12h; Stage #2: With sodium hydrogencarbonate	20%

: 39538-68-6
2-methoxy-4-methylaniline

(η5-cyclohexadienyl)tricarbonyliron tetrafluoroborate: (η5-cyclohexadienyl)tricarbonyliron tetrafluoroborate

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With manganese(IV) oxide 1.) MeCN, 25 deg C, 2.) toluene, 25 deg C; Multistep reaction;

: 39538-68-6
2-methoxy-4-methylaniline

tricarbonyl<(1-5-η)-cyclohexadienylium>iron tetrafluoroborate: tricarbonyl<(1-5-η)-cyclohexadienylium>iron tetrafluoroborate

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With manganese(IV) oxide 1) CH3CN, 46 h, RT, 2) toluene, RT 24 h and 2 d; Yield given. Multistep reaction;

: 41608-64-4
methyl 3-methoxy-4-aminobenzoate

tricarbonyl<(1-5-η)-cyclohexadienylium>iron tetrafluoroborate: tricarbonyl<(1-5-η)-cyclohexadienylium>iron tetrafluoroborate

: 723-97-7
murrayanine

Conditions

Conditions	Yield
With manganese(IV) oxide; diisobutylaluminium hydride Yield given. Multistep reaction;

: 954378-09-7
3-(2-bromophenyl)-2,3,4,5,6,7-hexahydro-2-oxobenzoxazol-6-carboxaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 65 percent / DDQ / benzene / 24 h / Heating 2: KOH / ethanol; H2O / 18 h / 20 °C 3: 0.24 g / K2CO3 / acetone / 12 h / Heating 4: 85 percent / Na2CO3; LiCl / [Pd(PPh3)4] / acetonitrile / 48 h / Heating View Scheme

: 954378-10-0
3-(2-bromophenyl)-2,3-dihydro-2-oxobenzoxazol-6-carboxaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: KOH / ethanol; H2O / 18 h / 20 °C 2: 0.24 g / K2CO3 / acetone / 12 h / Heating 3: 85 percent / Na2CO3; LiCl / [Pd(PPh3)4] / acetonitrile / 48 h / Heating View Scheme

: C13H10BrNO2

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 0.24 g / K2CO3 / acetone / 12 h / Heating 2: 85 percent / Na2CO3; LiCl / [Pd(PPh3)4] / acetonitrile / 48 h / Heating View Scheme

: 189953-32-0
3-(2-Bromo-phenyl)-4,5-dimethylene-oxazolidin-2-one

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: 90 percent / BF3*Et2O / CH2Cl2 / 0.42 h / -78 °C 2: 65 percent / DDQ / benzene / 24 h / Heating 3: KOH / ethanol; H2O / 18 h / 20 °C 4: 0.24 g / K2CO3 / acetone / 12 h / Heating 5: 85 percent / Na2CO3; LiCl / [Pd(PPh3)4] / acetonitrile / 48 h / Heating View Scheme

: 153897-88-2
4,5-dimethylene-3-phenyl-1,3-oxazolidin-2-one

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: BF3*Et2O / CH2Cl2 / 2.5 h / 160 °C 2: 69 percent / DDQ / benzene / 24 h / Heating 3: 81 percent / aq. NaOH / ethanol / 1 h / 20 °C 4: 95 percent / K2CO3 / acetone / 3 h / 60 °C 5: 73 percent / glacial acetic acid / Pd(OAc)2 / 12 h / 160 °C View Scheme
Multi-step reaction with 5 steps 1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / -78 °C 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 12 h / 60 °C 3: sodium hydroxide / ethanol; water / 0.75 h / 60 °C 4: potassium carbonate / acetone / 0.75 h / 60 °C 5: palladium diacetate; acetic acid; copper diacetate / 110 - 130 °C / Inert atmosphere View Scheme

: 808114-01-4
3-hydroxy-4-(phenylamino)benzaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 95 percent / K2CO3 / acetone / 3 h / 60 °C 2: 73 percent / glacial acetic acid / Pd(OAc)2 / 12 h / 160 °C View Scheme
Multi-step reaction with 2 steps 1: potassium carbonate / acetone / 0.75 h / 60 °C 2: palladium diacetate; acetic acid; copper diacetate / 110 - 130 °C / Inert atmosphere View Scheme

: 808114-05-8
2,3-dihydro-2-oxo-3-phenylbenzo[d]oxazole-6-carbaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 81 percent / aq. NaOH / ethanol / 1 h / 20 °C 2: 95 percent / K2CO3 / acetone / 3 h / 60 °C 3: 73 percent / glacial acetic acid / Pd(OAc)2 / 12 h / 160 °C View Scheme
Multi-step reaction with 3 steps 1: sodium hydroxide / ethanol; water / 0.75 h / 60 °C 2: potassium carbonate / acetone / 0.75 h / 60 °C 3: palladium diacetate; acetic acid; copper diacetate / 110 - 130 °C / Inert atmosphere View Scheme

: 808113-99-7
2,3,4,5,6,7-hexahydro-2-oxo-3-phenylbenzo[d]oxazole-6-carbaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 69 percent / DDQ / benzene / 24 h / Heating 2: 81 percent / aq. NaOH / ethanol / 1 h / 20 °C 3: 95 percent / K2CO3 / acetone / 3 h / 60 °C 4: 73 percent / glacial acetic acid / Pd(OAc)2 / 12 h / 160 °C View Scheme
Multi-step reaction with 4 steps 1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 12 h / 60 °C 2: sodium hydroxide / ethanol; water / 0.75 h / 60 °C 3: potassium carbonate / acetone / 0.75 h / 60 °C 4: palladium diacetate; acetic acid; copper diacetate / 110 - 130 °C / Inert atmosphere View Scheme

: 23523-94-6
1-methoxy-3-methoxycarbonyl-9H-carbazole

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 90 percent / DIBAH / diethyl ether; hexane / 3.5 h / -78 °C 2: MnO2 / CCl4 / 6 h / Ambient temperature View Scheme
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 70 °C 2: manganese(IV) oxide / acetone / 12 h / 20 °C View Scheme
Multi-step reaction with 2 steps 1: diisobutylaluminium hydride / toluene; diethyl ether / 2 h / -78 °C / Inert atmosphere 2: manganese(IV) oxide / tetrachloromethane / 12 h / 20 °C View Scheme

: 182261-83-2
methyl 1-hydroxy-9H-carbazole-3-carboxylate

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: K2CO3 / acetone / 7 h / Heating 2: 90 percent / DIBAH / diethyl ether; hexane / 3.5 h / -78 °C 3: MnO2 / CCl4 / 6 h / Ambient temperature View Scheme
Multi-step reaction with 3 steps 1: methanol; diethyl ether / 12 h / 0 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 70 °C 3: manganese(IV) oxide / acetone / 12 h / 20 °C View Scheme

: 38512-82-2
3-methoxy-4-nitrotoluene

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 96 percent / hydrogen / 10percent Pd/C / ethanol / 912 Torr 2: 2) MnO2 / 1) CH3CN, 46 h, RT, 2) toluene, RT 24 h and 2 d View Scheme
Multi-step reaction with 2 steps 1: H2 / Pd/C / ethanol 2: 2.) MnO2 / 1.) MeCN, 25 deg C, 2.) toluene, 25 deg C View Scheme

: 1375487-97-0
4-hydroxy-9H-carbazole-3-carbaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere 2: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere 3: tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride / N,N-dimethyl-formamide / 0.75 h / 100 °C / Inert atmosphere 4: methanol; copper(l) iodide / N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere View Scheme

Yield

Multi-step reaction with 4 steps
1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride / N,N-dimethyl-formamide / 0.75 h / 100 °C / Inert atmosphere
4: methanol; copper(l) iodide / N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere
View Scheme

: 1375487-99-2
1-bromo-4-hydroxy-9H-carbazole-3-carbaldehyde

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride / N,N-dimethyl-formamide / 0.75 h / 100 °C / Inert atmosphere 3: methanol; copper(l) iodide / N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere View Scheme

: 1384959-51-6
1-bromo-3-formyl-9H-carbazol-4-yl trifluoromethanesulfonate

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride / N,N-dimethyl-formamide / 0.75 h / 100 °C / Inert atmosphere 2: methanol; copper(l) iodide / N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere View Scheme

: 52602-39-8
9H-carbazol-4-ol

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: trichlorophosphate / 10 - 20 °C / Inert atmosphere 1.2: 20 - 35 °C / Inert atmosphere 1.3: 20 - 30 °C / Inert atmosphere 2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere 3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere 4.1: tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride / N,N-dimethyl-formamide / 0.75 h / 100 °C / Inert atmosphere 5.1: methanol; copper(l) iodide / N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere View Scheme

Yield

Multi-step reaction with 5 steps
1.1: trichlorophosphate / 10 - 20 °C / Inert atmosphere
1.2: 20 - 35 °C / Inert atmosphere
1.3: 20 - 30 °C / Inert atmosphere
2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
4.1: tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride / N,N-dimethyl-formamide / 0.75 h / 100 °C / Inert atmosphere
5.1: methanol; copper(l) iodide / N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere
View Scheme

: 121-33-5
vanillin

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: pyridine / dichloromethane / 0.25 h / 20 °C 1.2: 1 h / -20 °C 2.1: caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 12 h / 96 °C 3.1: potassium carbonate; palladium diacetate; Trimethylacetic acid / 12 h / 115 °C View Scheme

: 194018-68-3
vanillin triflate

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 12 h / 96 °C 2: potassium carbonate; palladium diacetate; Trimethylacetic acid / 12 h / 115 °C View Scheme

: 808114-08-1
(2-methoxy-4-methylphenyl)phenylamine

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: potassium carbonate; Trimethylacetic acid; palladium diacetate / 12 h / 110 °C 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; methanol; tetrahydrofuran / 0.5 h / 20 °C View Scheme

: 39538-68-6
2-methoxy-4-methylaniline

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: C19H19N5O; copper(l) iodide; potassium carbonate / water / 24 h / 100 °C / Green chemistry 2: potassium carbonate; Trimethylacetic acid; palladium diacetate / 12 h / 110 °C 3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; methanol; tetrahydrofuran / 0.5 h / 20 °C View Scheme

: 591-50-4
iodobenzene

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: C19H19N5O; copper(l) iodide; potassium carbonate / water / 24 h / 100 °C / Green chemistry 2: potassium carbonate; Trimethylacetic acid; palladium diacetate / 12 h / 110 °C 3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; methanol; tetrahydrofuran / 0.5 h / 20 °C View Scheme

: 5-methoxy-2'-nitrobiphenyl-3-carboxylic acid methyl ester

: 723-97-7
murrayanine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: triphenylphosphine / 1,2-dichloro-benzene / 10 h / Reflux 2: diisobutylaluminium hydride / toluene; diethyl ether / 2 h / -78 °C / Inert atmosphere 3: manganese(IV) oxide / tetrachloromethane / 12 h / 20 °C View Scheme

: 723-97-7
murrayanine

: 3,3'-dihydroxy-1,1'-dimethoxy-4,4'-bis(9,9'H-carbazole)

Conditions

Conditions	Yield
With potassium hydrogensulfate; dihydrogen peroxide In methanol at 20℃; for 1h; Dakin Phenol Oxidation; Inert atmosphere;	93%

: 723-97-7
murrayanine

: 3909-78-2
koenoline

Conditions

Conditions	Yield
With potassium borohydride In methanol at 25℃; for 17h;	90%
With sodium tetrahydroborate In methanol at 0 - 20℃; for 0.75h;	90%
With potassium borohydride In methanol at 25℃; Yield given;
With sodium tetrahydroborate In methanol for 24h;	20 mg
With methanol; sodium tetrahydroborate at 20℃; for 24h;

: 723-97-7
murrayanine

: 1-hydroxy-9H-carbazole-3-carbaldehyde

Conditions

Conditions	Yield
With boron tribromide In dichloromethane 1.) 0 deg C, 3 h, 2.) r.t., overnight;	90%
Stage #1: murrayanine With aluminum (III) chloride In benzene for 6h; Reflux; Stage #2: With hydrogenchloride In water

: 723-97-7
murrayanine

: 1-methoxy-9H-carbazol-3-yl formate

Conditions

Conditions	Yield
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 0.333333h; Baeyer-Villiger Ketone Oxidation; Inert atmosphere;	65%

: 723-97-7
murrayanine

A: 4532-33-6
1-methoxy-3-methylcarbazole

B: 3909-78-2
koenoline

Conditions

Conditions	Yield
With amalgamated zinc In ethanol Heating;

: 723-97-7
murrayanine

: koenoline acetate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 20 mg / NaBH4 / methanol / 24 h 2: 3 mg / pyridine / 120 h View Scheme

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Antimex Chemical Limied

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