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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need CMO

Miglustat manufacturer/supplier

Cas:72599-27-0

Min.Order:1 Gram

Negotiable

Type:Manufacturers

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Content Natural Extract Miglustat HACCP manufacturer

Cas:72599-27-0

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Miglustat

Cas:72599-27-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

Miglustat/ LIDE PHARMA- Factory supply / Best price

Cas:72599-27-0

Min.Order:1 Gram

FOB Price: $10.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 72599-27-0 with competitive price

Cas:72599-27-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

72599-27-0 N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

3,4,5-Piperidinetriol,1-butyl-2-(hydroxymethyl)-, (2R,3R,4R,5S)- 72599-27-0

Cas:72599-27-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

N-BUTYLDEOXYNOJIRIMYCIN CAS:72599-27-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i

N-BUTYLDEOXYNOJIRIMYCIN CAS:72599-27-0

Cas:72599-27-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

3,4,5-Piperidinetriol,1-butyl-2-(hydroxymethyl)-, (2R,3R,4R,5S)-

Cas:72599-27-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Miglustat

Cas:72599-27-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater

N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:18 Metric Ton

FOB Price: $18.0 / 20.0

Type:Lab/Research institutions

inquiry

Sinoway Industrial Co., Ltd.

Why is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c

99% up GMP DMF Miglustat powder 72599-27-0

Cas:72599-27-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Taizhou Crene Biotechnology co.ltd

Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

OGT918 miglustat 72599-27-0

Cas:72599-27-0

Min.Order:300 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

NewCan Biotech Limited

NewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed

Miglustat

Cas:72599-27-0

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

buy-Miglustat

Cas:72599-27-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Kunsui Technology Co., Ltd.

1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m

High Purity API miglustat OGT918 Powder CAS 72599-27-0

Cas:72599-27-0

Min.Order:1 Kilogram

FOB Price: $8.2 / 8.8

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so

Miglustat 72599-27-0

Cas:72599-27-0

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Reliable Quality N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualified

N-BUTYLDEOXYNOJIRIMYCIN supplier Factory

Cas:72599-27-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

N-BUTYLDEOXYNOJIRIMYCIN,72599-27-0

Cas:72599-27-0

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermediat

Miglustat

Cas:72599-27-0

Min.Order:1 Kilogram

FOB Price: $777.0 / 888.0

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

N-BUTYLDEOXYNOJIRIMYCIN,72599-27-0

Cas:72599-27-0

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

N-BUTYLDEOXYNOJIRIMYCIN,72599-27-0

Cas:72599-27-0

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

3,4,5-Piperidinetriol,1-butyl-2-(hydroxymethyl)-, (2R,3R,4R,5S)-

Cas:72599-27-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

N-BUTYLDEOXYNOJIRIMYCIN

Cas:72599-27-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high quality,low priceAppearance:white powder Storage:cool, dark Package:Drum & Bag Application:pharam Transportation:by sea or air

Miglustat

Cas:72599-27-0

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

miglustat hydrochloride
210110-90-0

miglustat hydrochloride

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene99.5%
N-butyl 2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol
227932-82-3

N-butyl 2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
With ammonia; lithium In tetrahydrofuran at -78℃; for 2.5h;91%
With boron trichloride In hexane; dichloromethane at -78℃;83%
With 10 wt% Pd(OH)2 on carbon; hydrogen In ethanol; chloroform at 20℃; for 20h;
With hydrogenchloride; 16% Pd/C; hydrogen In methanol; water under 3000.3 Torr; for 4h;50 g
With hydrogenchloride; 16% Pd/C; hydrogen In methanol; water under 3000.3 Torr; for 4h;50 g
1-bromo-butane
109-65-9

1-bromo-butane

1,5-dideoxy-1,5-imino-D-glucitol
19130-96-2

1,5-dideoxy-1,5-imino-D-glucitol

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 80 - 90℃; for 24h;76%
With sodium hydrogencarbonate In 1,4-dioxane; methanol for 48h; Heating;
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 24h;
1,5-dideoxy-1,5-imino-D-glucitol
19130-96-2

1,5-dideoxy-1,5-imino-D-glucitol

butyraldehyde
123-72-8

butyraldehyde

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In ethanol; water at 20℃; under 2585.81 Torr;60%
palladium In methanol
palladium In methanol
D-xylo-hexos-5-ulose
19684-22-1

D-xylo-hexos-5-ulose

N-butylamine
109-73-9

N-butylamine

A

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

B

(3R,4R,5S)-6-Butylamino-hexane-1,2,3,4,5-pentaol

(3R,4R,5S)-6-Butylamino-hexane-1,2,3,4,5-pentaol

Conditions
ConditionsYield
With sodium cyanoborohydride; acetic acid In methanol 1.) -78 deg C, 2 h, 2.) r.t., 20 h;A 55%
B 10%
C24H33NO4

C24H33NO4

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Stage #1: C24H33NO4 With trimethylsilyl iodide In dichloromethane at 20℃; for 0.25h;
Stage #2: With methanol In dichloromethane
33%
2,3,4,6-tetra-O-benzyl-D-glucopyranose
6564-72-3

2,3,4,6-tetra-O-benzyl-D-glucopyranose

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 100 percent / LiAlH4 / tetrahydrofuran / Ambient temperature
2: 1.) TFAA, DMSO, 2.) Et3N / 1.) CH2Cl2, -78 deg C, 1.5 h, 2.) CH2Cl2, -78 deg C to r.t., 30 min
3: 77 percent / NaBH3CN, molecular sieves 3 Angstroem / methanol / 0.5 h / Ambient temperature
4: 91 percent / Li, NH3 / tetrahydrofuran / 2.5 h / -78 °C
View Scheme
2,3,4,6-tetra-O-benzyl-D-glucitol
78136-16-0, 14233-48-8

2,3,4,6-tetra-O-benzyl-D-glucitol

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) TFAA, DMSO, 2.) Et3N / 1.) CH2Cl2, -78 deg C, 1.5 h, 2.) CH2Cl2, -78 deg C to r.t., 30 min
2: 77 percent / NaBH3CN, molecular sieves 3 Angstroem / methanol / 0.5 h / Ambient temperature
3: 91 percent / Li, NH3 / tetrahydrofuran / 2.5 h / -78 °C
View Scheme
Multi-step reaction with 6 steps
1: pyridine / dichloromethane / 20 °C / Inert atmosphere
2: triphenylphosphine; diethylazodicarboxylate / toluene / 20 °C / Inert atmosphere
3: sodium methylate / methanol / 5 h / 20 °C
4: pyridine / 5 h / 20 °C
5: 96 h / 55 °C
6: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; chloroform / 20 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 4 h / 50 °C / Inert atmosphere
2: sodium cyanoborohydride; sodium sulfate; acetic acid / dichloromethane; methanol / 15 h / 20 °C / pH 6 / Inert atmosphere
3: hydrogenchloride; 16% Pd/C; hydrogen / methanol; water / 4 h / 3000.3 Torr
View Scheme
(2R,3R,4S)-2,3,4,6-tetrakis(benzyloxy)-5-oxohexanal
214041-43-7

(2R,3R,4S)-2,3,4,6-tetrakis(benzyloxy)-5-oxohexanal

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / NaBH3CN, molecular sieves 3 Angstroem / methanol / 0.5 h / Ambient temperature
2: 91 percent / Li, NH3 / tetrahydrofuran / 2.5 h / -78 °C
View Scheme
1,2-O-isopropylidene-α-D-xylo-hexafuranos-5-ulose
19684-32-3

1,2-O-isopropylidene-α-D-xylo-hexafuranos-5-ulose

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 70 percent / Dowex 50W-X8 / H2O / 36 h / 25 °C
2: 55 percent / HOAc, NaBH3CN / methanol / 1.) -78 deg C, 2 h, 2.) r.t., 20 h
View Scheme
1,2-O-isopropylidene-α-D-glucofuranose
18549-40-1

1,2-O-isopropylidene-α-D-glucofuranose

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) dibutylin oxide hemihydrate, 2.) Br2 / 1.) MeOH, reflux, 1.5 h, 2.) CH2Cl2, 0 deg C, 10 min
2: 70 percent / Dowex 50W-X8 / H2O / 36 h / 25 °C
3: 55 percent / HOAc, NaBH3CN / methanol / 1.) -78 deg C, 2 h, 2.) r.t., 20 h
View Scheme
2,2-dimethylpropanoic anhydride
1538-75-6

2,2-dimethylpropanoic anhydride

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

(2S,3R,4S,5S)-2,3,4,6-tetrakis(benzyloxy)hexane-1,5-diyldimethanesulfonate

(2S,3R,4S,5S)-2,3,4,6-tetrakis(benzyloxy)hexane-1,5-diyldimethanesulfonate

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 96 h / 55 °C
2: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; chloroform / 20 h / 20 °C
View Scheme
(2S,3R,4R,5R)-2,3,4,6-tetrakis(benzyloxy)-5-hydroxyhexyl pivalate
1316108-84-5

(2S,3R,4R,5R)-2,3,4,6-tetrakis(benzyloxy)-5-hydroxyhexyl pivalate

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: triphenylphosphine; diethylazodicarboxylate / toluene / 20 °C / Inert atmosphere
2: sodium methylate / methanol / 5 h / 20 °C
3: pyridine / 5 h / 20 °C
4: 96 h / 55 °C
5: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; chloroform / 20 h / 20 °C
View Scheme
(2R,3R,4R,5S)-1,3,4,5-tetrakis(benzyloxy)-6-(pivaloyloxy)hexan-2-yl benzoate
1316108-89-0

(2R,3R,4R,5S)-1,3,4,5-tetrakis(benzyloxy)-6-(pivaloyloxy)hexan-2-yl benzoate

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium methylate / methanol / 5 h / 20 °C
2: pyridine / 5 h / 20 °C
3: 96 h / 55 °C
4: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; chloroform / 20 h / 20 °C
View Scheme
Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: sodium tetrahydroborate / ethanol / 12 h / Inert atmosphere
2: pyridine / dichloromethane / 20 °C / Inert atmosphere
3: triphenylphosphine; diethylazodicarboxylate / toluene / 20 °C / Inert atmosphere
4: sodium methylate / methanol / 5 h / 20 °C
5: pyridine / 5 h / 20 °C
6: 96 h / 55 °C
7: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; chloroform / 20 h / 20 °C
View Scheme
Multi-step reaction with 7 steps
1: acetic anhydride; dimethyl sulfoxide / 20 °C
2: ammonia / methanol / 3 h / 0 °C
3: acetic anhydride; dimethyl sulfoxide / 6 h / 20 °C
4: sodium cyanoborohydride; formic acid / acetonitrile / 3 h / Reflux
5: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
6: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
7: boron trichloride / dichloromethane; hexane / -78 °C
View Scheme
(2S,3R,4R,5S)-2,3,4,6-tetrakis(benzyloxy)hexane-1,5-diol
78136-16-0

(2S,3R,4R,5S)-2,3,4,6-tetrakis(benzyloxy)hexane-1,5-diol

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine / 5 h / 20 °C
2: 96 h / 55 °C
3: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; chloroform / 20 h / 20 °C
View Scheme
6-deoxy-6-butylaminosorbose

6-deoxy-6-butylaminosorbose

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
With 4% Pd/C; hydrogen In water at 20℃; under 3345.86 Torr; for 2.33333h; pH=5;
2,3,4,6-tetra-O-benzyl-D-xylo-hex-5-ulosononitrile
139189-61-0

2,3,4,6-tetra-O-benzyl-D-xylo-hex-5-ulosononitrile

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: palladium hydroxide, 20 wt% on carbon; hydrogen / tert-butyl alcohol; methanol / 25 °C / 7757.43 - 8791.75 Torr
1.2: 0.5 h
1.3: 4654.46 - 5171.62 Torr
2.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 - 90 °C
View Scheme
methyl-alpha-D-glucopyranoside
97-30-3

methyl-alpha-D-glucopyranoside

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 9 steps
1: sodium hydride / N,N-dimethyl-formamide / 8 h / 0 - 20 °C
2: acetic acid; sulfuric acid / Reflux
3: acetic anhydride; dimethyl sulfoxide / 20 °C
4: ammonia / methanol / 3 h / 0 °C
5: acetic anhydride; dimethyl sulfoxide / 6 h / 20 °C
6: sodium cyanoborohydride; formic acid / acetonitrile / 3 h / Reflux
7: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
8: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
9: boron trichloride / dichloromethane; hexane / -78 °C
View Scheme
2,3,4,6-tetra-O-benzyl-5-dehydro-5-oxo-D-gluconamide
76670-94-5

2,3,4,6-tetra-O-benzyl-5-dehydro-5-oxo-D-gluconamide

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium cyanoborohydride; formic acid / acetonitrile / 3 h / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
3: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
4: boron trichloride / dichloromethane; hexane / -78 °C
View Scheme
Conditions
ConditionsYield
Multi-step reaction with 8 steps
1: acetic acid; sulfuric acid / Reflux
2: acetic anhydride; dimethyl sulfoxide / 20 °C
3: ammonia / methanol / 3 h / 0 °C
4: acetic anhydride; dimethyl sulfoxide / 6 h / 20 °C
5: sodium cyanoborohydride; formic acid / acetonitrile / 3 h / Reflux
6: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
7: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
8: boron trichloride / dichloromethane; hexane / -78 °C
View Scheme
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one
13096-62-3

(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: ammonia / methanol / 3 h / 0 °C
2: acetic anhydride; dimethyl sulfoxide / 6 h / 20 °C
3: sodium cyanoborohydride; formic acid / acetonitrile / 3 h / Reflux
4: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
5: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
6: boron trichloride / dichloromethane; hexane / -78 °C
View Scheme
2,3,4,6-tetra-O-benzyl-D-gluconamide
76670-93-4

2,3,4,6-tetra-O-benzyl-D-gluconamide

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: acetic anhydride; dimethyl sulfoxide / 6 h / 20 °C
2: sodium cyanoborohydride; formic acid / acetonitrile / 3 h / Reflux
3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
4: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
5: boron trichloride / dichloromethane; hexane / -78 °C
View Scheme
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)piperidin-2-one
77174-08-4

(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)piperidin-2-one

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
2: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
3: boron trichloride / dichloromethane; hexane / -78 °C
View Scheme
2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol
69567-11-9, 76738-52-8, 126836-30-4

2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium on carbon; hydrogen; hydrogenchloride / ethanol; water / 24 h / 3000.3 Torr / pH 2
2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 70 °C / Inert atmosphere
View Scheme
3,4-di-O-benzyl-D-mannitol
36199-02-7

3,4-di-O-benzyl-D-mannitol

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 0 °C
2: triethylamine / dichloromethane
3: hydrogenchloride; methanol
4: sodium hydroxide / water
5: methanol / 0.08 h / 90 °C / Microwave irradiation; Sealed tube
6: trimethylsilyl iodide / dichloromethane / 0.25 h / 20 °C
View Scheme
(2R,3R,4R,5R)-3,4-Bis-benzyloxy-1,6-bis-(tert-butyl-dimethyl-silanyloxy)-hexane-2,5-diol
172147-87-4

(2R,3R,4R,5R)-3,4-Bis-benzyloxy-1,6-bis-(tert-butyl-dimethyl-silanyloxy)-hexane-2,5-diol

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane
2: hydrogenchloride; methanol
3: sodium hydroxide / water
4: methanol / 0.08 h / 90 °C / Microwave irradiation; Sealed tube
5: trimethylsilyl iodide / dichloromethane / 0.25 h / 20 °C
View Scheme
Methanesulfonic acid (1R,2S,3S,4R)-2,3-bis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-4-methanesulfonyloxy-pentyl ester
172147-86-3

Methanesulfonic acid (1R,2S,3S,4R)-2,3-bis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-4-methanesulfonyloxy-pentyl ester

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrogenchloride; methanol
2: sodium hydroxide / water
3: methanol / 0.08 h / 90 °C / Microwave irradiation; Sealed tube
4: trimethylsilyl iodide / dichloromethane / 0.25 h / 20 °C
View Scheme
N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

1,5-(Butylimino)-1,5-dideoxy-D-glucitol, 6-acetate
131262-99-2

1,5-(Butylimino)-1,5-dideoxy-D-glucitol, 6-acetate

Conditions
ConditionsYield
With acetic anhydride In pyridine; water
With acetic anhydride In pyridine; water
With acetic anhydride In pyridine; water
With acetic anhydride In pyridine; water
dimethyoxytoluene

dimethyoxytoluene

p-toluenesulfonic acid monohydrate
6192-52-5

p-toluenesulfonic acid monohydrate

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

1,5-(Butylimino)-1,5-dideoxy-4R, 6-0-(phenylmethylene)-D-glucitol

1,5-(Butylimino)-1,5-dideoxy-4R, 6-0-(phenylmethylene)-D-glucitol

Conditions
ConditionsYield
In N-methyl-acetamide
4-methylvaleroyl chloride
38136-29-7

4-methylvaleroyl chloride

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

1,5-(Butylimino)-1,5-dideoxy-D-glucitol, tetra(4-methylpentanoate)
143698-23-1

1,5-(Butylimino)-1,5-dideoxy-D-glucitol, tetra(4-methylpentanoate)

Conditions
ConditionsYield
In tetrahydrofuran; pyridine; water; ethyl acetate
1,2-dimethoxy-3-methylbenzene
4463-33-6

1,2-dimethoxy-3-methylbenzene

p-toluenesulfonic acid monohydrate
6192-52-5

p-toluenesulfonic acid monohydrate

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

1,5-(Butylimino)-1,5-dideoxy-4R, 6-0-(phenylmethylene)-D-glucitol

1,5-(Butylimino)-1,5-dideoxy-4R, 6-0-(phenylmethylene)-D-glucitol

Conditions
ConditionsYield
In N-methyl-acetamide
In N-methyl-acetamide
In N-methyl-acetamide
4,4,4-trifluorobutanoyl chloride
406-91-7

4,4,4-trifluorobutanoyl chloride

N-butyldeoxynojirimycin
72599-27-0

N-butyldeoxynojirimycin

1,5-(Butylimino)-1,5-dideoxy-D-glucitol tetra(4,4,4-trifluorobutanoate)

1,5-(Butylimino)-1,5-dideoxy-D-glucitol tetra(4,4,4-trifluorobutanoate)

Conditions
ConditionsYield
In tetrahydrofuran; pyridine; water

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