1.high purity 2.consistent quality 3.competitive price 4.fast shipping Binbo Biological Products Co. Ltd., is a professional high-tech enterprise which engaged in Biological products and raw materials. Binbo is engaged in R&D with perfect eq
Cas:19130-96-2
Min.Order:1 Kilogram
FOB Price: $1.0 / 5.0
Type:Lab/Research institutions
inquiryKnown for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica
Product Name: Mulberry Leaf Extract Botanical Name: Folium Mori, Ramulus Mori Part Used: Leaf Specification Water Soluble Spray-dried Powder 1-DNJ 1%, 2%, 5%, 10%, 20% HPLC Active Ingredient: 1-Deoxynojirimycin C
Cas:19130-96-2
Min.Order:1 Kilogram
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Type:Trading Company
inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:19130-96-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryItems Standard Result Appearance White crystalline powder Conform NMR Conform
Cas:19130-96-2
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Trading Company
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:19130-96-2
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryHigh quality 1-Deoxynojirimycin Product name:1-Deoxynojirimycin Appearance: white powder Purity:98% Shelf life:2 years Quality: TOP Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:Foil bag or drum Application:App
We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need CMO
Cas:19130-96-2
Min.Order:1 Gram
Negotiable
Type:Manufacturers
inquiryHigh Quality Mulberry Leaf Extract 5% 1-Deoxynojirimycin Powder Xi'an Quanao Biotech Co., Ltd. is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additive
Cas:19130-96-2
Min.Order:100 Kilogram
FOB Price: $95.0 / 100.0
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:19130-96-2
Min.Order:1
Negotiable
Type:Other
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:19130-96-2
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:19130-96-2
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryHigh purity, all the standards are around 99%; NRM, HPLC, Lc-MS/MS methods valued and certified, ensure the accurate purity; All the standards attached COA and MSDS; More than 80 kinds of mycotoxin standards can be provided; Accurate stock; Comp
Cas:19130-96-2
Min.Order:1 Milligram
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Type:Trading Company
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:19130-96-2
Min.Order:5 Kiloliter
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Type:Manufacturers
inquiryCHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
Cas:19130-96-2
Min.Order:1 Gram
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Type:Trading Company
inquiryName:DNJ The alias:1-deoxynojirimycin CAS NO:19130-96-2 Molecular formula:C6H13NO4 Molecular weight:163.17 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security withou
Cas:19130-96-2
Min.Order:25 Kilogram
FOB Price: $1.0 / 2.0
Type:Other
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:19130-96-2
Min.Order:1 Kilogram
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Type:Trading Company
inquiryName: Deoxynojirimycin CAS:19130-96-2 MF: C6H13NO4 Appearance:Green powder Storage: Store in cool and dry place, away from sun light. Package:25KG Application:Mulberry leaf p.e used to free radical scavenging activities; Mulberry leaf p.e with the
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o
Cas:19130-96-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Min.Order:1 Kilogram
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Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:19130-96-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:19130-96-2
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Type:Trading Company
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry pla
Cas:19130-96-2
Min.Order:100 Gram
Negotiable
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:19130-96-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:19130-96-2
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Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:19130-96-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryPRODUCT DETAILS
Cas:19130-96-2
Min.Order:500 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Negotiable
Type:Trading Company
inquiry2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride; 20% palladium hydroxide-activated charcoal; hydrogen In methanol; water for 14h; | 100% |
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In ethanol; water at 20℃; under 3000.3 Torr; for 20h; pH=Ca. 2; | 93% |
Stage #1: 2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol With hydrogenchloride In ethanol for 0.25h; pH=Ca. 2; Inert atmosphere; Stage #2: With palladium 10% on activated carbon; hydrogen In ethanol under 3000.3 Torr; for 20h; Inert atmosphere; | 93% |
N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; palladium In acetic acid for 15h; | 100% |
With hydrogen; acetic acid; palladium for 18h; | 100% |
With palladium 10% on activated carbon; hydrogen In acetic acid at 20℃; for 19h; | 98% |
(2R,4aR,7S,8R,8aR)-tert-butyl 8-hydroxy-7-(methoxymethyl)-2-phenyltetrahydro-4H-[1,3]dioxino[5,4-b]pyridine-5(4aH)-carboxylate
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 18h; Reflux; Inert atmosphere; | 100% |
N-Benzhydryl-1-deoxynojirimycin
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; palladium dihydroxide In methanol under 3102.9 Torr; for 24h; | 99% |
With hydrogen; palladium dihydroxide | 90% |
With hydrogen; palladium on activated charcoal In methanol | 50% |
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In tetrahydrofuran; water at 20℃; under 760.051 Torr; for 48h; | 98% |
With hydrogen; palladium dihydroxide In methanol for 24h; |
nojirimycin
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide In ethanol; water under 750.06 Torr; for 18h; Ambient temperature; | 97% |
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 12h; Heating; | 94% |
(2R,3R,4R,5S)-(3,4-dibenzyloxy-N-tert-butoxycarbonyl-5-hydroxy-2-piperidinyl)methanol
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethanol at 20℃; for 48h; | 92% |
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; palladium dihydroxide In acetic acid; tert-butyl alcohol under 3750.3 Torr; for 48h; Ambient temperature; | 91% |
N-bentyl-2,3,4,6-tetra-O-benzyl-1-deoxynojirimycin
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With 10 wt% Pd(OH)2 on carbon; hydrogen In ethanol; chloroform at 20℃; for 20h; | 91% |
(2R,3R,4S,5S)-4,5-(isopropylenedioxy)-3-(methoxymethoxy)-2-<(methoxymethoxy)methyl>piperidine
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 1h; Heating; | 90% |
(3aS,6R,7R,7aS)-6-(tert-Butyl-dimethyl-silanyloxymethyl)-2,2-dimethyl-hexahydro-[1,3]dioxolo[4,5-c]pyridin-7-ol
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With trifluoroacetic acid Ambient temperature; | 90% |
N-benzyl-1-deoxynojirimycin
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol | 89% |
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With 10 wt% Pd(OH)2 on carbon; hydrogen; potassium carbonate In water under 2585.81 Torr; | 80% |
Nojirimycin bisulfite
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With barium dihydroxide; hydrogen; nickel In water | 75% |
((2S,3R,4S)-2,3,4,6-Tetrahydroxy-5-oxo-hexyl)-carbamic acid benzyl ester
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; potassium carbonate; palladium on activated charcoal In methanol; water at 60℃; under 60004.8 Torr; for 2h; | 75% |
With palladium 10% on activated carbon; hydrogen In methanol; water at 20℃; under 2585.81 Torr; for 24h; | 717 mg |
(2R,3R,4R,5S)-3-benzyloxy-2-benzyloxymethyl-4,5-isopropylidenedioxypiperidine
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride; palladium 10% on activated carbon; water; hydrogen In methanol; ethyl acetate at 20℃; for 48h; | 75% |
6-Amino-6-desoxy-L-sorbofuranose-hydrochlorid
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With platinum(IV) oxide; hydrogen at 20℃; under 3750.38 Torr; for 16h; Inert atmosphere; | 70% |
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With 20 % Pd(OH)2/C; ammonium acetate; hydrogen In methanol; water at 20℃; for 24h; | 68% |
(+)-(3aR,5RS,6R,6aS)-3a,5,6,6a-tetrahydro-5,6-dihydroxyfuro<2,3-d>isoxazole-3-methanol
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 25℃; under 750.06 Torr; for 15h; | 65% |
5-azido-5-deoxy-D-glucofuranose
A
1,5-dideoxy-1,5-imino-D-glucitol
B
1-deoxynojirimycin hydrochloride
Conditions | Yield |
---|---|
Stage #1: 5-azido-5-deoxy-D-glucofuranose With palladium 10% on activated carbon; hydrogen In water at 20℃; under 2068.65 - 2585.81 Torr; Stage #2: With hydrogenchloride In water pH=2; | A 16% B 56% |
A
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium dihydroxide | A 55% B 21% |
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal In 1,4-dioxane; water for 24h; Ambient temperature; | 54% |
5-amino-5-deoxy-D-glucose-1-sulfonic acid
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With barium hydroxide octahydrate; hydrogen; Raney-Ni (W-4) In water under 760 Torr; for 8h; Ambient temperature; | 53% |
(2R,3R,4S,5S)-5-(Benzyloxy)-2-(hydroxymethyl)piperidine-3,4-diol
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; | 53% |
(1R,3aR,7aR,8R)-6,6-dimethylhexahydro-1,5,7-trioxa-3-azacyclopropa[a]naphthalene-3-carboxylic acid tert-butyl ester
A
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
Stage #1: (1R,3aR,7aR,8R)-6,6-dimethylhexahydro-1,5,7-trioxa-3-azacyclopropa[a]naphthalene-3-carboxylic acid tert-butyl ester With potassium hydroxide In 1,4-dioxane; water Heating; Stage #2: With hydrogenchloride In methanol; water at 60℃; for 1h; Stage #3: With DOWEX-1X2 (OH(1-) form) In water Further stages.; | A 33% B 51% |
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; palladium dihydroxide In ethanol under 25857.4 Torr; for 24h; | 19% |
3,6-di-O-benzyl-5-azido-5-deoxy-α/β-D-glucofuranose
A
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
With hydrogen; palladium hydroxide - carbon In methanol; water; acetic acid under 3800 Torr; for 48h; Ambient temperature; Yield given; | A n/a B 5% |
With hydrogen; palladium hydroxide - carbon In methanol; water; acetic acid under 3800 Torr; for 48h; Ambient temperature; Yields of byproduct given; | A n/a B 5% |
dihydroxyacetone phosphate
(RS)-3-azido-2-hydroxypropanal
A
1,5-dideoxy-1,5-imino-D-glucitol
Conditions | Yield |
---|---|
Multistep reaction; |
1,5-dideoxy-1,5-imino-D-glucitol
C12H15N5O3
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid In methanol at 20℃; for 14h; | 100% |
1,5-dideoxy-1,5-imino-D-glucitol
1-deoxynojirimycin hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In water | 100% |
With hydrogenchloride In water at 10℃; pH=2; Molecular sieve; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 24h; Inert atmosphere; | 99% |
1,5-dideoxy-1,5-imino-D-glucitol
C13H18O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(6-(m-tolyloxy)hexyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H18O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 98% |
1,5-dideoxy-1,5-imino-D-glucitol
C12H16O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(3-(2-propoxyphenyl)propyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C12H16O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen for 24h; | 97% |
1,5-dideoxy-1,5-imino-D-glucitol
C12H16O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(3-(3-propoxyphenyl)propyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C12H16O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 97% |
1,5-dideoxy-1,5-imino-D-glucitol
C12H16O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(3-(4-propoxyphenyl)propyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C12H16O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 97% |
1,5-dideoxy-1,5-imino-D-glucitol
3-bromoprop-1-ene-2-phosphonic acid diethyl ester
[1-((2R,3R,4R,5S)-3,4,5-Trihydroxy-2-hydroxymethyl-piperidin-1-ylmethyl)-vinyl]-phosphonic acid diethyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In acetone at 25℃; for 3h; | 96% |
1,5-dideoxy-1,5-imino-D-glucitol
C12H15FO2
(2R,3R,4R,5S)-1-(6-(2-fluorophenoxy)hexyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C12H15FO2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon In ethanol for 24h; | 96% |
1,5-dideoxy-1,5-imino-D-glucitol
6-(3-fluorophenoxy)hexanal
(2R,3R,4R,5S)-1-(6-(3-fluorophenoxy)hexyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: 6-(3-fluorophenoxy)hexanal With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 96% |
1,5-dideoxy-1,5-imino-D-glucitol
C12H15FO2
(2R,3R,4R,5S)-1-(6-(4-fluorophenoxy)hexyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C12H15FO2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 96% |
1,5-dideoxy-1,5-imino-D-glucitol
C13H15F3O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(6-(4-(trifluoromethyl)phenoxy)hexyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H15F3O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 96% |
1,5-dideoxy-1,5-imino-D-glucitol
C15H20O2
(2R,3R,4R,5S)-1-(3-(3-(cyclohexyloxy)phenyl)propyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C15H20O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 20h; | 96% |
1,5-dideoxy-1,5-imino-D-glucitol
C16H24O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(6-(2-isopropyl-5-methylphenoxy)hexyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C16H24O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 95% |
1,5-dideoxy-1,5-imino-D-glucitol
C15H20O2
(2R,3R,4R,5S)-1-(3-(4-(cyclohexyloxy)phenyl)propyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C15H20O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 95% |
1,5-dideoxy-1,5-imino-D-glucitol
C13H15F3O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(6-(3-(trifluoromethyl)phenoxy)hexyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H15F3O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 94% |
1,5-dideoxy-1,5-imino-D-glucitol
C13H15F3O3
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(6-(4-(trifluoromethoxy)phenoxy)hexyl) piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H15F3O3 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 94% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol; water under 2585.7 Torr; for 36h; | 93% |
With formic acid In water for 20h; Heating; Yield given; | |
With formic acid at 80℃; for 3h; |
1,5-dideoxy-1,5-imino-D-glucitol
C13H15F3O2
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(6-(2-(trifluoromethyl)phenoxy)hexyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H15F3O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 93% |
With sodium cyanoborohydride In methanol |
1,5-dideoxy-1,5-imino-D-glucitol
C13H18O3
(2R,3R,4R,5S)-2-(hydroxymethyl)-1-(6-(4-methoxyphenoxy)hexyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H18O3 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 93% |
1,5-dideoxy-1,5-imino-D-glucitol
C13H26O2
(2R,3R,4R,5S)-1-(6-(heptan-4-yloxy)hexyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H26O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon In ethanol for 24h; | 93% |
1,5-dideoxy-1,5-imino-D-glucitol
C14H26O2
(2R,3R,4R,5S)-1-(6-((2-ethylcyclohexyl)oxy)hexyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C14H26O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 93% |
1,5-dideoxy-1,5-imino-D-glucitol
C13H24O2
(2R,3R,4R,5S)-1-(6-(cycloheptyloxy)hexyl)-2-(hydroxymethyl)piperidine-3,4,5-triol
Conditions | Yield |
---|---|
Stage #1: 1,5-dideoxy-1,5-imino-D-glucitol With acetic acid at 20℃; Stage #2: C13H24O2 With acetic acid In ethanol at 20℃; for 1h; Inert atmosphere; Stage #3: With palladium 10% on activated carbon; hydrogen In ethanol for 24h; | 93% |
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