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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Uridine,2'-deoxy-5-(2-propenyl)- (9CI)

Cas:73-39-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Uridine,2'-deoxy-5-(2-propenyl)- (9CI)

Cas:73-39-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Uridine,2'-deoxy-5-(2-propenyl)- (9CI)

Cas:73-39-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Uridine,2'-deoxy-5-(2-propenyl)- (9CI)

Cas:73-39-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

5-(2-propenyl)-2'-deoxyuridine

Cas:73-39-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

NewCan Biotech Limited

NewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed

5-Allyl-2′-deoxyuridine

Cas:73-39-2

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to light yellow crystal powder Storage:Room temperature with sealed well Package:according to the clients requirement Appl

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

5-(2-propenyl)-2'-deoxyuridine

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Uridine,2'-deoxy-5-(2-propenyl)- (9CI)

Cas:73-39-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

Uridine, 5-allyl-2'-deoxy- Application:Uridine, 5-allyl-2'-deoxy-

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Fandachem Co.,Ltd

Uridine,2'-deoxy-5-(2-propenyl)- (9CI) cas 73-39-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Uridine,2'-deoxy-5-(2-propenyl)- (9CI) cas 73-39-2

Cas:73-39-2

Min.Order:0

Negotiable

Type:Other

inquiry

Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

73-39-2

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

5-(2-propenyl)-2'-deoxyuridine

Cas:73-39-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

73-39-2

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

Uridine, 5-allyl-2'-deoxy- Package:as needed Application:Veterinary medicine Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for large amount.

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Saiwante (shanghai) New Material Technology Co., Ltd.

Stable supply of goods and provision of high-quality services Application:As raw materials in the field of medicine and biology

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

5-(2-propenyl)-2'-deoxyuridine

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

shanxiyuhong

Keywords Competitive price/ Top quality of Uridine,2'-deoxy-5-(2-propenyl)- (9CI) global trader Offer Reliable quality of Uridine,2'-deoxy-5-(2-propenyl)- (9CI) Best price of 99%m in Uridine,2'-deoxy-5-(2-propenyl)- (9CI) Quick Det

Uridine,2'-deoxy-5-(2-propenyl)- (9CI)

Cas:73-39-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

73-39-2 CAS NO.73-39-2

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

Uridine,2'-deoxy-5-(2-propenyl)- (9CI)

Cas:73-39-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Jusheng Technology Co., Ltd.,

1,Best Quality: Our products have exported to Germany, Spain, UK, USA, Australia, Middle East, and so on other countries, and we have got very good feedback from our customers.so

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:10 Gram

FOB Price: $1.0 / 2.0

Type:Trading Company

inquiry

Taizhou volsen chemical Co., Ltd

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

Uridine, 5-allyl-2'-deoxy-

Cas:73-39-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Raymon Biotech Co., Ltd.

Uridine,2'-deoxy-5-(2-propenyl)- ((9CIAppearance:Pls see the Details Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By cour

Uridine,2'-deoxy-5-(2-propenyl)- ((9CI

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Minshang Biotechnology Co., Ltd

Uridine, 5-allyl-2'-deoxy- Application:Veterinary medicine

73-39-2

Cas:73-39-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

methanol
67-56-1

methanol

C5-chloromercuri-2'-deoxyuridine
65505-76-2

C5-chloromercuri-2'-deoxyuridine

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

(E)-5-<3-(2'-deoxyuridylin-5-yl)-1-propen-1-yl>-2'-deoxyuridine
76334-41-3

(E)-5-<3-(2'-deoxyuridylin-5-yl)-1-propen-1-yl>-2'-deoxyuridine

B

5-<3-(2'-deoxyuridin-5-yl)-1-methoxyprop-1-yl>-2'-deoxyuridine
76334-42-4

5-<3-(2'-deoxyuridin-5-yl)-1-methoxyprop-1-yl>-2'-deoxyuridine

C

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With lithium tetrachloropalladate(II) Yield given;A n/a
B n/a
C 84%
C5-chloromercuri-2'-deoxyuridine
65505-76-2

C5-chloromercuri-2'-deoxyuridine

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

(E)-5-<3-(2'-deoxyuridylin-5-yl)-1-propen-1-yl>-2'-deoxyuridine
76334-41-3

(E)-5-<3-(2'-deoxyuridylin-5-yl)-1-propen-1-yl>-2'-deoxyuridine

B

5-<3-(2'-deoxyuridin-5-yl)-1-methoxyprop-1-yl>-2'-deoxyuridine
76334-42-4

5-<3-(2'-deoxyuridin-5-yl)-1-methoxyprop-1-yl>-2'-deoxyuridine

C

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With lithium tetrachloropalladate(II) In methanolA n/a
B n/a
C 84%
C5-chloromercuri-2'-deoxyuridine
65505-76-2

C5-chloromercuri-2'-deoxyuridine

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With palladium dichloride In methanol for 20h;78%
lithium tetrachloropalladate(II) In methanol
5-Iodo-2'-deoxyuridine
54-42-2

5-Iodo-2'-deoxyuridine

allyl-trimethyl-silane
762-72-1

allyl-trimethyl-silane

A

2'-deoxyuridine
951-78-0

2'-deoxyuridine

B

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
In water; acetonitrile Irradiation;A 31%
B 49%
In water; acetonitrile for 10h; Ambient temperature; Irradiation;A 31%
B 49%
5-Iodo-2'-deoxyuridine
54-42-2

5-Iodo-2'-deoxyuridine

A

2'-deoxyuridine
951-78-0

2'-deoxyuridine

B

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With allyl-trimethyl-silane In water; acetonitrile Irradiation;A 31%
B 49%
With allyl-trimethyl-silane In water; acetonitrile for 10h; Ambient temperature; Irradiation;A 31%
B 49%
methanol
67-56-1

methanol

3-ethoxyprop-1-ene
557-31-3

3-ethoxyprop-1-ene

C5-chloromercuri-2'-deoxyuridine
65505-76-2

C5-chloromercuri-2'-deoxyuridine

A

5-(2,2-dimethoxy-1-methylethyl)-2'-deoxyuridine
76334-65-1

5-(2,2-dimethoxy-1-methylethyl)-2'-deoxyuridine

B

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With lithium tetrachloropalladate(II)A 15%
B 32%
3-ethoxyprop-1-ene
557-31-3

3-ethoxyprop-1-ene

C5-chloromercuri-2'-deoxyuridine
65505-76-2

C5-chloromercuri-2'-deoxyuridine

A

5-(2,2-dimethoxy-1-methylethyl)-2'-deoxyuridine
76334-65-1

5-(2,2-dimethoxy-1-methylethyl)-2'-deoxyuridine

B

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With lithium tetrachloropalladate(II) In methanolA 15%
B 32%
5-Iodo-2'-deoxyuridine
54-42-2

5-Iodo-2'-deoxyuridine

allyltributylstanane
24850-33-7

allyltributylstanane

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran for 24h; Heating; Yield given;
4,4'-dimethoxytrityl chloride
40615-36-9

4,4'-dimethoxytrityl chloride

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

5-allyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine
809290-35-5

5-allyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine

Conditions
ConditionsYield
Stage #1: C5-(allyl)-2'-deoxyuridine With pyridine; silver nitrate for 0.0833333h;
Stage #2: 4,4'-dimethoxytrityl chloride for 4h;
86%
With pyridine; silver nitrate
tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

3',5'-bis-O-(tert-butyldimethylsilyl)-C5-(allyl)-2'-deoxyuridine
151894-33-6

3',5'-bis-O-(tert-butyldimethylsilyl)-C5-(allyl)-2'-deoxyuridine

Conditions
ConditionsYield
With 1H-imidazole In N,N-dimethyl-formamide for 3h;78%
With 1H-imidazole In N,N-dimethyl-formamide Yield given;
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane
69304-37-6

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

5-Allyl-1-((2R,3aS,9aR)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-1H-pyrimidine-2,4-dione
194595-63-6

5-Allyl-1-((2R,3aS,9aR)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-1H-pyrimidine-2,4-dione

Conditions
ConditionsYield
In pyridine at 0℃;68%
tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

5-allyl-5'-O-tert-butyldimethylsilyl-2'-deoxyuridine
809290-37-7

5-allyl-5'-O-tert-butyldimethylsilyl-2'-deoxyuridine

Conditions
ConditionsYield
Stage #1: C5-(allyl)-2'-deoxyuridine With pyridine; silver nitrate for 0.0833333h;
Stage #2: tert-butyldimethylsilyl chloride for 10h;
42%
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

5-Propyl-2'-deoxyuridine
27826-74-0

5-Propyl-2'-deoxyuridine

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol under 1241.2 Torr; for 10h;
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

5-allyl-5'-O-(tert-butyldimethylsilyl)-2'-deoxyuridine-3'-O-{(N,N-diisopropyl)-(2-cyanoethyl)phosphoramidite}
809290-38-8

5-allyl-5'-O-(tert-butyldimethylsilyl)-2'-deoxyuridine-3'-O-{(N,N-diisopropyl)-(2-cyanoethyl)phosphoramidite}

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 42 percent / 10 h
2.1: 75 percent / 4,5-dicyanoimidazole / CH2Cl2; acetonitrile / 0.58 h / 20 °C
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C35H57N4O12PSi2
809290-46-8

C35H57N4O12PSi2

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 1.5 h / 20 °C
4.2: 64 percent / t-BuOOH / acetonitrile; toluene / 1.5 h
5.1: 58 percent / (1,3-dimesitylimidazolidin-2-ylidene)[(c-hexyl)3P]Cl2Ru=CHPh / CH2Cl2 / 2 h / Heating
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C37H58N5O12PSi2

C37H58N5O12PSi2

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 0.5 h
5.1: 0.142 g / t-BuOOH / acetonitrile; toluene / 2 h
6.1: 27 percent / (1,3-dimesitylimidazolidin-2-ylidene)[(c-hexyl)3P]Cl2Ru=CHPh / CH2Cl2 / 22 h / Heating
View Scheme
Multi-step reaction with 5 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 42 percent / 10 h
2.1: 75 percent / 4,5-dicyanoimidazole / CH2Cl2; acetonitrile / 0.58 h / 20 °C
3.1: 1H-tetrazole / acetonitrile / 0.5 h
4.1: 0.142 g / t-BuOOH / acetonitrile; toluene / 2 h
5.1: 27 percent / (1,3-dimesitylimidazolidin-2-ylidene)[(c-hexyl)3P]Cl2Ru=CHPh / CH2Cl2 / 22 h / Heating
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C39H62N5O11PSi2

C39H62N5O11PSi2

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 0.5 h
View Scheme
Multi-step reaction with 3 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 42 percent / 10 h
2.1: 75 percent / 4,5-dicyanoimidazole / CH2Cl2; acetonitrile / 0.58 h / 20 °C
3.1: 1H-tetrazole / acetonitrile / 0.5 h
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C39H62N5O12PSi2

C39H62N5O12PSi2

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / CH2Cl2; acetonitrile / 1 h
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C39H62N5O13PSi2

C39H62N5O13PSi2

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / CH2Cl2; acetonitrile / 1 h
5.1: 0.156 g / t-BuOOH / CH2Cl2; acetonitrile; toluene / 3 h / 0 - 20 °C
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C39H62N5O12PSi2
809290-45-7

C39H62N5O12PSi2

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 0.5 h
5.1: 0.142 g / t-BuOOH / acetonitrile; toluene / 2 h
View Scheme
Multi-step reaction with 4 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 42 percent / 10 h
2.1: 75 percent / 4,5-dicyanoimidazole / CH2Cl2; acetonitrile / 0.58 h / 20 °C
3.1: 1H-tetrazole / acetonitrile / 0.5 h
4.1: 0.142 g / t-BuOOH / acetonitrile; toluene / 2 h
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

5-allyl-3'-O-tert-butyldimethylsilyl-2'-deoxyuridine
492452-95-6

5-allyl-3'-O-tert-butyldimethylsilyl-2'-deoxyuridine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
View Scheme
Multi-step reaction with 3 steps
1: AgNO3; pyridine
2: AgNO3; pyridine
3: p-TsOH / CH2Cl2; methanol / 0 °C
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

5-allyl-3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine
809290-36-6

5-allyl-3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
View Scheme
Multi-step reaction with 2 steps
1: AgNO3; pyridine
2: AgNO3; pyridine
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

(2R,4S,5R)-4-Hydroxy-8-[(2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yloxy]-8-oxo-7,9,19-trioxa-1,16-diaza-8λ5-phospha-tricyclo[12.3.1.12,5]nonadec-14(18)-ene-15,17-dione
492453-06-2

(2R,4S,5R)-4-Hydroxy-8-[(2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yloxy]-8-oxo-7,9,19-trioxa-1,16-diaza-8λ5-phospha-tricyclo[12.3.1.12,5]nonadec-14(18)-ene-15,17-dione

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 1.5 h / 20 °C
4.2: 64 percent / t-BuOOH / acetonitrile; toluene / 1.5 h
5.1: (1,3-dimesitylimidazolidin-2-ylidene)[(c-hexyl)3P]Cl2Ru=CHPh / CH2Cl2 / 3.5 h / Heating
5.2: 63 percent / H2 / CH2Cl2 / 50 °C / 51714.8 Torr
6.1: 100 percent / trifluoroacetic acid / H2O / 3 h
View Scheme
Multi-step reaction with 7 steps
1.1: AgNO3; pyridine
2.1: AgNO3; pyridine
3.1: p-TsOH / CH2Cl2; methanol / 0 °C
4.1: 1H-tetrazole / acetonitrile
5.1: tert-BuOOH / acetonitrile
6.1: Grubbs' type catalyst / CH2Cl2 / 40 °C
6.2: 63 percent / H2 / Grubbs' type catalyst / CH2Cl2 / 50 °C / 51716.2 Torr
7.1: 100 percent / aq. TFA
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

Phosphoric acid (2R,3S,5R)-5-[5-((E)-4-amino-but-2-enyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-3-hydroxy-tetrahydro-furan-2-ylmethyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Phosphoric acid (2R,3S,5R)-5-[5-((E)-4-amino-but-2-enyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-3-hydroxy-tetrahydro-furan-2-ylmethyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 1.5 h / 20 °C
4.2: 64 percent / t-BuOOH / acetonitrile; toluene / 1.5 h
5.1: 58 percent / (1,3-dimesitylimidazolidin-2-ylidene)[(c-hexyl)3P]Cl2Ru=CHPh / CH2Cl2 / 2 h / Heating
6.1: NH3 / H2O / 24 h / 20 °C
View Scheme
Multi-step reaction with 7 steps
1: AgNO3; pyridine
2: AgNO3; pyridine
3: p-TsOH / CH2Cl2; methanol / 0 °C
4: 1H-tetrazole / acetonitrile
5: tert-BuOOH / acetonitrile
6: 58 percent / Grubbs' type catalyst / CH2Cl2 / 40 °C
7: 100 percent / aq. NH3 / 55 °C
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C35H59N4O12PSi2
492453-05-1

C35H59N4O12PSi2

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 1.5 h / 20 °C
4.2: 64 percent / t-BuOOH / acetonitrile; toluene / 1.5 h
5.1: (1,3-dimesitylimidazolidin-2-ylidene)[(c-hexyl)3P]Cl2Ru=CHPh / CH2Cl2 / 3.5 h / Heating
5.2: 63 percent / H2 / CH2Cl2 / 50 °C / 51714.8 Torr
View Scheme
Multi-step reaction with 6 steps
1.1: AgNO3; pyridine
2.1: AgNO3; pyridine
3.1: p-TsOH / CH2Cl2; methanol / 0 °C
4.1: 1H-tetrazole / acetonitrile
5.1: tert-BuOOH / acetonitrile
6.1: Grubbs' type catalyst / CH2Cl2 / 40 °C
6.2: 63 percent / H2 / Grubbs' type catalyst / CH2Cl2 / 50 °C / 51716.2 Torr
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C37H61N4O12PSi2
492452-96-7

C37H61N4O12PSi2

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: pyridine; AgNO3 / 0.08 h
1.2: 86 percent / 4 h
2.1: 86 percent / pyridine; AgNO3 / 0.08 h
3.1: 88 percent / p-toluenesulfonic acid monohydrate / methanol; CH2Cl2 / 0.58 h / 0 °C
4.1: 1H-tetrazole / acetonitrile / 1.5 h / 20 °C
4.2: 64 percent / t-BuOOH / acetonitrile; toluene / 1.5 h
View Scheme
Multi-step reaction with 5 steps
1: AgNO3; pyridine
2: AgNO3; pyridine
3: p-TsOH / CH2Cl2; methanol / 0 °C
4: 1H-tetrazole / acetonitrile
5: tert-BuOOH / acetonitrile
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C35H57N4O12PSi2
492452-99-0

C35H57N4O12PSi2

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: AgNO3; pyridine
2: AgNO3; pyridine
3: p-TsOH / CH2Cl2; methanol / 0 °C
4: 1H-tetrazole / acetonitrile
5: tert-BuOOH / acetonitrile
6: 58 percent / Grubbs' type catalyst / CH2Cl2 / 40 °C
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

C37H61N4O11PSi2

C37H61N4O11PSi2

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: AgNO3; pyridine
2: AgNO3; pyridine
3: p-TsOH / CH2Cl2; methanol / 0 °C
4: 1H-tetrazole / acetonitrile
View Scheme
C5-(allyl)-2'-deoxyuridine
73-39-2

C5-(allyl)-2'-deoxyuridine

[2,4-Dioxo-1-((2R,3aS,9aR)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-1,2,3,4-tetrahydro-pyrimidin-5-yl]-acetaldehyde
194595-69-2

[2,4-Dioxo-1-((2R,3aS,9aR)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-1,2,3,4-tetrahydro-pyrimidin-5-yl]-acetaldehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 68 percent / pyridine / 0 °C
2.1: K2OsO4*2H2O; N-methylmorpholino-N-oxide / acetone
2.2: NaIO4 / tetrahydrofuran; H2O
View Scheme

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