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inquiryItems Standard Result Assay 99.9%min 99.9% Hangzhou Dingyan Chem is a leading manufacturer and supplier of che
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inquiryfine chemical white to light yellow powder Idoxuridine CAS 54-42-2 MF C9H11IN2O5 mw 354.10 354.10 dentification: White crystalline powder
Manufacturer supply 5-Iodo-2'-deoxyuridine CAS 54-42-2 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives,
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:54-42-2
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Cas:54-42-2
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inquiryMolecular formula: C9H11IN2O5 Molecular weight: 354.10 CAS No.: 54-42-2 Identification: White crystalline powder Appearance:White powder Storage: Room T
Cas:54-42-2
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inquiryAppearance:white crystalline solid Storage:Room temperature Package:25kg/drum Application:Antiviral Transportation:Express/Sea/Air Port:Any port in china
Cas:54-42-2
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Idoxuridine CAS:54-42-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, s
Cas:54-42-2
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryNewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:54-42-2
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inquiryProName: High quality 5-Iodo-2'-Deoxyuridine su... CasNo: 54-42-2 Molecular Formula: C9H11IN2O5 Appearance: white-off solid or colorless liquid ( ... Application: Specialty chemical DeliveryTime: Instock PackAge: 25kgs/fiber drum or 200kg
Cas:54-42-2
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryConditions | Yield |
---|---|
With iodine; silver nitrate In methanol at 40℃; for 3h; | 100% |
With iodine; silver nitrate In methanol at 40℃; for 3h; | 100% |
With sodium azide; Iodine monochloride In acetonitrile at 25℃; for 24h; Product distribution; Mechanism; other uracil nucleosides; other halogenation agents; var. temp. and time; | 96% |
Conditions | Yield |
---|---|
With sodium methylate In methanol for 1h; Ambient temperature; | 90% |
With methanol; sodium methylate at 20℃; for 1h; |
5-trimethylstannyl-2'-deoxyuridine
5-Iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide; acetic acid; sodium iodide In chloroform for 0.00416667h; Irradiation; |
5-Iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
With ammonia In methanol at 30℃; for 16h; |
Conditions | Yield |
---|---|
at 37℃; for 6h; alginate gel-entrapped cells of auxotrophic thymine-dependent strain of E. coli, ammonium acetate buffer pH 5.8; |
Conditions | Yield |
---|---|
With thymidine phosphorylase from Escherichia coli In phosphate buffer at 35℃; for 2h; pH=7.0; Title compound not separated from byproducts; | A 88 % Chromat. B n/a |
3',5'-di-O-acetyl-2'-deoxyuridine
5-Iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 93 percent / LiI, ceric ammonium nitrate (CAN) / acetonitrile / 1 h / 80 °C / other conditions and reagents investigated 2: 90 percent / 0.1 M NaOMe / methanol / 1 h / Ambient temperature View Scheme |
C5-chloromercuri-2'-deoxyuridine
1,3,4,6-tetrachloro-3α,6α-diphenyl glycoluril
5-Iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
With sodium iodide In water |
Conditions | Yield |
---|---|
With thymidine phosphorylase from Escherichia coli (E.C. 2.4.2.4) immobilized on Sepabeads EC-EP In aq. phosphate buffer at 20℃; for 3h; pH=7.5; Reagent/catalyst; Enzymatic reaction; |
3',5'-di-O-acetyl-2'-deoxyuridine
A
5-Iodo-2'-deoxyuridine
E
2'-deoxy-4-thiouridine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium cerium (IV) nitrate; iodine / acetonitrile / 1 h / 80 °C 2: tetraphosphorus decasulfide / 1,4-dioxane / Reflux 3: sodium hydride / methanol / 0.17 h / 0 - 20 °C 4: aq. phosphate buffer; tert-butyl alcohol / Radiolysis View Scheme |
3',5'-O-diacetyl-5-iodo-2'-deoxyuridine
A
5-Iodo-2'-deoxyuridine
E
2'-deoxy-4-thiouridine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tetraphosphorus decasulfide / 1,4-dioxane / Reflux 2: sodium hydride / methanol / 0.17 h / 0 - 20 °C 3: aq. phosphate buffer; tert-butyl alcohol / Radiolysis View Scheme |
5-iodo-4-thio-2'-deoxyuridine
A
5-Iodo-2'-deoxyuridine
E
2'-deoxy-4-thiouridine
Conditions | Yield |
---|---|
In aq. phosphate buffer; tert-butyl alcohol Radiolysis; |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: pyridine / 24 h / 20 °C 2: ammonium cerium (IV) nitrate; iodine / acetonitrile / 1 h / 80 °C 3: tetraphosphorus decasulfide / 1,4-dioxane / Reflux 4: sodium hydride / methanol / 0.17 h / 0 - 20 °C 5: aq. phosphate buffer; tert-butyl alcohol / Radiolysis View Scheme |
Conditions | Yield |
---|---|
With recobinant purine nucleoside phosphorylase from Escherichia coli In aq. phosphate buffer pH=6.8; Heating; Enzymatic reaction; |
Conditions | Yield |
---|---|
With E-pyrimidine nucleoside phosphorylase-0002 In aq. buffer at 50℃; for 2h; pH=9; Equilibrium constant; Enzymatic reaction; |
5-Iodo-2'-deoxyuridine
acrylic acid methyl ester
methyl (E)-3-(1-((2R,4S,5R)-4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)acrylate
Conditions | Yield |
---|---|
With palladium diacetate; triethylamine; triphenylphosphine In 1,4-dioxane for 14h; Heating; | 100% |
Stage #1: 5-Iodo-2'-deoxyuridine With C26H32N8O6P2PdS2 In acetonitrile at 80℃; for 0.0833333h; Heck Reaction; Inert atmosphere; Stage #2: acrylic acid methyl ester With triethylamine In acetonitrile at 80℃; for 8h; Heck Reaction; Inert atmosphere; | 92% |
With palladium diacetate; triethylamine; triphenylphosphine In N,N-dimethyl-formamide at 100℃; for 1h; | 87% |
9-ethynyl-closo-1,7-dodecaborane
5-Iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In N,N-dimethyl-formamide at 80℃; Sonogashira Cross-Coupling; Inert atmosphere; | 100% |
5-Iodo-2'-deoxyuridine
tert-butyldimethylsilyl chloride
2'-deoxy-3',5'-bis(O-tert-butyldimethylsilyl)-5-iodouridine
Conditions | Yield |
---|---|
With 1H-imidazole In pyridine for 33h; | 99% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 3h; | 99.8% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 60h; | 99% |
4,4'-dimethoxytrityl chloride
5-Iodo-2'-deoxyuridine
2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-5-iodouridine
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 99% |
With pyridine; triethylamine at 20℃; for 1h; | 98% |
With pyridine In triethylamine at 20℃; for 5h; | 96% |
5-Iodo-2'-deoxyuridine
acetic anhydride
3',5'-O-diacetyl-5-iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
With pyridine at 20℃; for 16.5h; | 99% |
With pyridine at 20℃; | 98% |
With pyridine at 25℃; for 20h; | 97% |
3,3-bis-(trifluoromethyl)-4,4,4-trifluoro-1-butyne
5-Iodo-2'-deoxyuridine
5-(4,4,4-trifluoro-3,3-bis(trifluoromethyl)but-1-ynyl)-2'-deoxyuridine
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 22℃; for 96h; Sonogashira coupling; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With 3,3′,3″-phosphinetriyltribenzenesulfonate; palladium diacetate; triethylamine In water; acetonitrile at 80℃; for 1.5h; Solvent; Temperature; Reagent/catalyst; Inert atmosphere; | 98% |
With tri(3-sulfonatophenyl)phosphine trisodium salt; palladium diacetate; triethylamine In water; acetonitrile at 80℃; Heck reaction; Inert atmosphere; | 74% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); triethylamine; triphenylphosphine In N,N-dimethyl-formamide at 70℃; | 98% |
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane
5-Iodo-2'-deoxyuridine
5-iodo-3',5'-O-[(tetraisopropyl)disiloxane-1,3-diyl]-2'-deoxyuridine
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 12h; | 97% |
With pyridine at 20℃; | 97% |
With pyridine at 20℃; | 84% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 3h; silylation; |
5-Iodo-2'-deoxyuridine
phenylboronic acid
1-((2R,4S,5R)-4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)-5-phenylpyrimidine-2,4(1H,3H)-dione
Conditions | Yield |
---|---|
With palladium diacetate; sodium carbonate; triphenylphosphine In water; acetonitrile at 70 - 80℃; for 4h; Suzuki-Miyaura Coupling; Inert atmosphere; | 97% |
With palladium diacetate; sodium carbonate; triphenylphosphine In water; acetonitrile at 70 - 80℃; for 4h; Suzuki-Miyaura Coupling; Inert atmosphere; | 97% |
With C30H24Cl2N2O10Pd2S2(2-)*2Na(1+); triethylamine In water at 60℃; for 3h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 93% |
2-ethynylpyridine
5-Iodo-2'-deoxyuridine
5-(2-pyridylethynyl)-2'-deoxyuridine
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With tributyl-amine; palladium diacetate In N,N-dimethyl-formamide at 100℃; for 0.333333h; Heck reaction; Microwave irradiation; | 97% |
With tributyl-amine; palladium diacetate In 1,4-dioxane; N,N-dimethyl-formamide at 100℃; for 0.333333h; Microwave irradiation; | 97% |
5-Iodo-2'-deoxyuridine
5-(benzofuran-2-yl)-1-((2R,4S,5R)-4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)pyrimidine-2,4(1H,3H)-dione
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride In 1,4-dioxane at 90℃; Stille Cross Coupling; | 97% |
5-Iodo-2'-deoxyuridine
but-1-yn-4-yl thiobenzoate
5-(4-benzoylthio-1-butynyl)-2'-deoxyuridine
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide at 22 - 24℃; | 96% |
5-Iodo-2'-deoxyuridine
acetyl chloride
3',5'-O-diacetyl-5-iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
With acetic anhydride; acetic acid 1.) 0 deg C, 1 h, 2.) RT, 24 h; | 95% |
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 0.166667h; | 95% |
5-Iodo-2'-deoxyuridine
3-methyl-N-(prop-2-yn-1-yl)butanamide
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In N,N-dimethyl-formamide at 20℃; for 4h; | 95% |
5-Iodo-2'-deoxyuridine
diphenylphosphane
5-diphenylphosphine-2'-deoxyuridine
Conditions | Yield |
---|---|
With triethylamine; palladium diacetate In N,N-dimethyl-formamide at 60℃; for 0.5h; | 95% |
3-methoxyphenylboronic acid
5-Iodo-2'-deoxyuridine
5-(3-methoxyphenyl)-2'-deoxyuridine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); cesium fluoride In water; N,N-dimethyl-formamide at 60℃; Suzuki cross-coupling; Inert atmosphere; | 95% |
With [Pd(phthalimidate)2(1,3,5-triaza-7-phosphaadamantane)2]; triethylamine In water at 20 - 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; |
4-tert-Butylphenylacetylene
5-Iodo-2'-deoxyuridine
5-((4-tert-butylphenyl)ethynyl)-2'-deoxyuridine
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide at 40℃; for 25h; Sonogashira coupling; | 94% |
With copper(l) iodide; tetra-(n-butyl)ammonium iodide; triphenylphosphine; tetrakis(triphenylphosphine) palladium(0); triethylamine In N,N-dimethyl-formamide at 20℃; for 24h; Sonogashira coupling; | 76% |
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide |
5-Iodo-2'-deoxyuridine
2-(tributylstannyl)furan
5-furan-2-yl-1-(β-D-2-deoxyribofuranos-1-yl)uracil
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride In 1,4-dioxane at 90℃; for 2h; Stille coupling; | 94% |
bis-triphenylphosphine-palladium(II) chloride In 1,4-dioxane at 90℃; for 2h; Stille coupling; | 94% |
With bis-triphenylphosphine-palladium(II) chloride In 1,4-dioxane | 94% |
With bis-triphenylphosphine-palladium(II) chloride In 1,4-dioxane at 90℃; Stille Cross Coupling; |
5-Iodo-2'-deoxyuridine
1-Ethynyl-1-cyclohexanol
5-((1-hydroxycyclohexyl)ethynyl)-2'-deoxyuridine
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide at 50℃; for 7h; Sonogashira coupling; | 94% |
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide |
2-Methylphenylboronic acid
5-Iodo-2'-deoxyuridine
5-(2-methylphenyl)-2'-deoxyuridine
Conditions | Yield |
---|---|
With sodium tetrachloropalladate; trisodium tris(3-sulfophenyl)phosphine; potassium hydroxide In water at 100℃; for 24h; Suzuki-Miyaura coupling; Inert atmosphere; | 94% |
With sodium tetrachloropalladate(II); potassium hydroxide In water at 100℃; for 1h; Suzuki-Miyaura Coupling; Inert atmosphere; Microwave irradiation; | 30% |
With sodium tetrachloropalladate(II); potassium hydroxide In water at 100℃; for 24h; Concentration; Time; Suzuki-Miyaura Coupling; Inert atmosphere; Green chemistry; | 22% |
benzofuran-2-boronic acid
5-Iodo-2'-deoxyuridine
5-(benzofuran-2-yl)-1-((2R,4S,5R)-4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)pyrimidine-2,4(1H,3H)-dione
Conditions | Yield |
---|---|
With [Pd(succinimidate)2(1,3,5-triaza-7-phosphaadamantane)2]; triethylamine In water at 80℃; for 0.0833333h; Catalytic behavior; Concentration; Suzuki-Miyaura Coupling; Microwave irradiation; Inert atmosphere; | 94% |
With C30H24Cl2N2O10Pd2S2(2-)*2Na(1+); triethylamine In water at 60℃; for 3h; Solvent; Reagent/catalyst; Temperature; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 89% |
5-Iodo-2'-deoxyuridine
propionic acid anhydride
3′,5′-bis-O-propionyl-5-iodo-2′-deoxyuridine
Conditions | Yield |
---|---|
With pyridine at 60℃; for 8h; Inert atmosphere; | 93% |
With pyridine | 85% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 12h; Inert atmosphere; Reflux; | 92% |
With bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran for 24h; Inert atmosphere; Reflux; | 50% |
With bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran for 24h; Heating; | 47% |
5-Iodo-2'-deoxyuridine
trimethylsilylacetylene
1-(2-deoxy-β-D-ribofuranosyl)-5-[2-(trimethylsilyl)ethynyl]uracil
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide at 55℃; for 24h; Sonogashira coupling; | 92% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In acetonitrile at 50℃; for 3.5h; Schlenk technique; Inert atmosphere; | 85% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In acetonitrile for 3.5h; Inert atmosphere; Heating; | 82% |
Conditions | Yield |
---|---|
With palladium diacetate; sodium carbonate; tris-(m-sulfonatophenyl)phosphine In water; acetonitrile at 80℃; Suzuki coupling; | 92% |
With tetrakis(triphenylphosphine) palladium(0); cesium fluoride In water; N,N-dimethyl-formamide at 60℃; Suzuki cross-coupling; Inert atmosphere; | 78% |
With palladium diacetate; sodium carbonate; triphenylphosphine In water at 120℃; for 0.166667h; Suzuki-Miyaura Coupling; Inert atmosphere; Sealed tube; Microwave irradiation; | 74% |
With [Pd(phthalimidate)2(1,3,5-triaza-7-phosphaadamantane)2]; triethylamine In water at 20 - 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; |
methyl 3-ethynylbenzoate
5-Iodo-2'-deoxyuridine
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 55℃; for 12h; | 92% |
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