CAS No.7340-90-1,5-TERT-BUTYL-2-METHYLTHIOPHENOL Suppliers

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Benzenethiol, 5-(1,1-dimethylethyl)-2-methyl-

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7340-90-1

2-methyl-5-tert-butyl-benzenethiolate

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Synthetic route

: 34493-12-4
1,2-bis(5-(tert-butyl)-2-methylphenyl)disulfane

: 7340-90-1
2-methyl-5-tert-butylthiophenol

Conditions

Conditions	Yield
With sodium tetrahydroborate

: 10022-13-6, 31505-44-9, 81704-02-1, 116347-84-3, 131234-07-6, 144300-04-9, 79733-86-1
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1011529-31-9
(2-methyl-5-tert-butylphenyl) 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-α-D-glucopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane	98%

: 138811-45-7
1,2,3,5,6-penta-O-benzoyl-D-galactofuranose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1269500-75-5
(2-methyl-5-tert-butylphenyl) 2,3,5,6-tetra-O-benzoyl-1-thio-β-D-galactofuranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 1.5h; Inert atmosphere;	97%

: 109-09-1
2-chloropyridine

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 2-(2-methyl-5-tert-butylphenylthio)pyridine

Conditions

Conditions	Yield
With bis(η3-allyl-μ-chloropalladium(II)); 1,1',3,3'-tetrakis(diphenylphosphino)ferrocene; sodium t-butanolate In toluene for 17h; Catalytic behavior; Inert atmosphere; Schlenk technique; Heating;	95%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 604-69-3
β-D-glucose pentaacetate

: 1334540-33-8
(2-methyl-5-tert-butylphenyl) 2,3,4,6-tetra-O-acetyl-1-S-β-D-thioglucopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane Inert atmosphere;	94%
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere;	92%
With boron trifluoride diethyl etherate In dichloromethane	85%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 220612-64-6
((2R,3S,4S,5R,6S)-6-(((1S,2S,3R,4S,6R)-4,6-bis((tert-butoxycarbonyl)amino)-3-(((2R,3R,5S,6R)-3-((tert-butoxycarbonyl)methyl)-5-hydroxytetrahydro-2Hpyran-2-yl)oxy)-2-hydroxycyclohexyl)oxy)-4-((tert-butoxycarbonyl)amino)-3,5-dihydroxytetrahydro-2H-pyran-2-yl)methyl 2,4,6-triisopropylbenzenesulfonate

: 1392113-84-6
C54H91N5O18S

Conditions

Conditions	Yield
With caesium carbonate In N,N-dimethyl-formamide at 20℃;	94%

: 7139-63-1
1,3,4,6-tetra-O-acetyl-2-(trifluoroacetamido)-2-deoxy-β-D-glucopyranoside

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 866823-12-3
5-tert-butyl-2-methylphenyl 3,4,6-tri-O-acetyl-2-(trifluoroacetamido)-2-deoxy-1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; Inert atmosphere;	93%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 4163-65-9
per-O-acetyl-α-D-mannopyranose

: 1379519-57-9
(2-methyl-5-tert-butylphenyl) 2,3,4,6-tetra-O-acetyl-1-thia-α-D-mannopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at -78 - 20℃; Inert atmosphere;	93%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 4163-60-4
β-D-galactose peracetate

: (2-methyl-5-tert-butylphenyl) 1-thio-β-D-galactopyranoside

Conditions

Conditions	Yield
Stage #1: 2-methyl-5-tert-butylthiophenol; β-D-galactose peracetate With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 1h; Stage #2: With sodium methylate In methanol for 0.5h;	93%

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1011529-31-9
(2-methyl-5-tert-butylphenyl) 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-α-D-glucopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 8h; Inert atmosphere;	92%

: C23H33NO14

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: C32H45NO12S

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 3h; Inert atmosphere;	91%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 7155-00-2
5-(tert-butyl)-2-methylbenzenesulfonamide

Conditions

Conditions	Yield
With [bis(acetoxy)iodo]benzene; ammonium carbamate In methanol at 25℃; for 24h; Inert atmosphere; chemoselective reaction;	90%

: C28H34Cl3F3N2O17

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: C37H48F3NO16S

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at -20 - -5℃; for 1.5h; Molecular sieve;	89.5%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 34493-12-4
1,2-bis(5-(tert-butyl)-2-methylphenyl)disulfane

Conditions

Conditions	Yield
With (bis(2,1-phenylene)bis(azanediyl)bis(methylene)diphenol)diselenide In acetonitrile at 20℃; for 7h;	89%
With phosphoric acid; oxygen; methyl 2-N-salicylidene-3-hydroxypropanoate; manganese(ll) chloride In acetone at 20℃; under 760.051 Torr;

: 39686-94-7, 56632-47-4, 65827-58-9, 99202-62-7, 99202-66-1, 103082-79-7, 103703-00-0, 103703-01-1, 118711-49-2, 127853-23-0, 139563-66-9
3-O-benzyl-1,2,4,6-tetra-O-acetyl-D-glucopyranose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: (2-methyl-5-tert-butylphenyl) 2,4,6-tri-O-acetyl-3-O-benzyl-1-thio-β-D-glucopyranose

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;	89%
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;	89%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 25589-81-5
2-Methyl-5-t-butylbenzolsulfosaeure

Conditions

Conditions	Yield
With sodium molybdate; dihydrogen peroxide; sodium dodecyl-sulfate In dichloromethane; water; butan-1-ol at 25℃; for 2h;	88%

: C68H69Cl3N4O33

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 945263-06-9
C77H83N3O32S

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at -10℃;	86%

: 7404-35-5, 17081-04-8, 20853-37-6, 24332-95-4, 27821-10-9, 27821-11-0, 33947-15-8, 34371-40-9, 34371-41-0, 35521-79-0, 36807-81-5, 36807-82-6, 50615-78-6, 51921-33-6, 62182-03-0, 64913-16-2, 70004-81-8, 84622-47-9, 87303-56-8, 108942-32-1, 108942-33-2, 109430-94-6, 143394-72-3, 30021-94-4
1,2,3,4-tetra-O-acetyl-L-rhamnopyranose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1185741-87-0
2-methyl-5-tert-butylphenyl 2,3,4-tri-O-acetyl-1-thio-α-L-rhamnopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; Inert atmosphere;	86%

: 446-52-6
2-Fluorobenzaldehyde

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: C18H20OS

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 150℃; for 3h;	84%

: 150885-36-2
Ethyl <2,4,5,7,8-penta-O-acetyl-3-deoxy-β-D-manno-octulopyranosid>onate

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: ethyl (5-tert-butyl-2-methylbenzenethio 4,5,7,8-tetra-O-acetyl-3-deoxy-D-manno-oct-2-ulopyranoside)onate

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere;	83%

: 75-03-6
ethyl iodide

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1-methyl-2-ethylsulfonyl-4-(1,1-dimethylethyl)benzene

Conditions

Conditions	Yield
Stage #1: 2-methyl-5-tert-butylthiophenol With methyllithium; N-(benzenesulfonyl)-3-phenyloxaziridine In tetrahydrofuran; N,N-dimethyl-formamide Stage #2: ethyl iodide In tetrahydrofuran; N,N-dimethyl-formamide Further stages.;	80%

: 1293911-28-0
3,4,6-tri-O-acetyl-1,2-dideoxy-2-iodo-1-[2-(trimethylsilyl)ethanesulfonamido]-α-D-mannopyranose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1293911-40-6
3,4,6-tri-O-acetyl-1,2-dideoxy-1-(5-tert-butyl-2-methyl)phenylthio-2-[2-(trimethylsilyl)ethanesulfonamido]-β-D-glucopyranoside

Conditions

Conditions	Yield
Stage #1: 2-methyl-5-tert-butylthiophenol With lithium hexamethyldisilazane In tetrahydrofuran; N,N-dimethyl-formamide at -30℃; Inert atmosphere; Stage #2: 3,4,6-tri-O-acetyl-1,2-dideoxy-2-iodo-1-[2-(trimethylsilyl)ethanesulfonamido]-α-D-mannopyranose In tetrahydrofuran; N,N-dimethyl-formamide at -30 - 20℃; for 0.333333h; diastereoselective reaction;	77%

: 3458-28-4
D-Mannose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1361016-58-1
(2-methyl-5-tert-butylphenyl) 1-thia-α-D-mannopyranoside

Conditions

Conditions	Yield
Stage #1: D-Mannose With pyridine; acetic anhydride at 20℃; Inert atmosphere; Stage #2: 2-methyl-5-tert-butylthiophenol With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere;	75%

: 55628-56-3, 68567-54-4, 77790-45-5, 77790-46-6, 81969-44-0, 99630-89-4, 125135-30-0, 137567-77-2, 65827-55-6
1,2-di-O-acetyl-3,4,6-tri-O-benzyl-α/β-D-mannopyranoside

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: (2-methyl-5-tert-butylphenyl) 2-O-acetyl-3,4,6-tri-O-benzyl-1-thio-D-mannopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In toluene at 20℃; for 2h; Inert atmosphere; optical yield given as %de;	75%

: O-{O-[(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)]-O-[(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)]-O-[(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->6)]-3-O-acetyl-α-D-mannopyranosyl}-trichloroacetimidate

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: C79H85N3O33S

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0℃;	69%

: 2,7-di-O-acetyl-3-O-levulinoyl-4-O-(para-bromobenzyl)-6-O-benzyl-L-glycero-D-manno-heptopyranosyl levulinoate

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 5-tert-butyl-2-methylphenyl 2,7-di-O-acetyl-3-O-levulinoyl-4-O-para-bromobenzyl-6-O-benzyl-1-thio-L-glycero-D-manno-heptopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere;	66%

: 1403362-05-9
2,7-di-O-acetyl-3-O-levulinoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranosyl levulinoate

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1403362-08-2
5-tert-butyl-2-methylphenyl 2,7-di-O-acetyl-3-O-levulinoyl-4-O-parabromobenzyl-6-O-benzyl-1-thio-L-glycero-D-manno-heptopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere;	66%

: 53270-12-5
1,2-O-(1-ethoxyethylene) 3,4,6-tri-O-benzyl-1-thio-α-D-glucopyranose

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1011529-36-4
(2-methyl-5-tert-butylphenyl) 2-O-acetyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
With mercury dibromide In toluene at 80℃;	64%

: 96996-90-6
1,2,3,4,6-penta-O-benzoyl-α,β-D-mannopyranoside

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1011529-30-8
(2-methyl-5-tert-butylphenyl) 2,3,4,6-tetra-O-benzoyl-1-thio-α-D-mannopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃;	56%

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 2592-58-7, 3006-48-2, 3006-49-3, 13526-09-5, 14679-57-3, 22415-91-4, 29884-70-6, 41545-55-5, 41545-56-6, 41569-33-9, 96996-90-6, 121570-85-2, 121570-86-3
1,2,3,4,6-penta-O-benzoyl-α-D-galactopyranoside

: (2-methyl-5-tert-butylphenyl) α-D-(2,3,4,6-tetra-O-benzoyl) thiogalactopyranoside

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃;	56%

: 103-30-0
(E)-1,2-diphenyl-ethene

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: S-(5-tert-butyl-2-methylphenyl)-S-(2-hydroxy-1,2-diphenylethyl)sulfoxide

Conditions

Conditions	Yield
With oxygen In hexane; ethyl acetate for 2.5h; Irradiation;	55%

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