xylazine
Conditions | Yield |
---|---|
With hydrogenchloride In water at 80 - 95℃; Industrial scale; | 95% |
Conditions | Yield |
---|---|
With acetic anhydride In tetrahydrofuran; ethanol | 113.8 g (84%) |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide In water; acetone |
Conditions | Yield |
---|---|
With hydrogenchloride In water | 16.3 g (80%) |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydride / tetrahydrofuran; toluene / 0.5 h / Industrial scale 2: 50 - 80 °C / Industrial scale 3: hydrogenchloride / water / 80 - 95 °C / Industrial scale View Scheme |
ammonium hydroxide
chloroformic acid ethyl ester
xylazine
isopropyl alcohol
2,6-dimethylaniline
2,6-dimethylphenylisothiocyanate
Conditions | Yield |
---|---|
With carbon disulfide In propan-1-ol; water | 55.2% |
Conditions | Yield |
---|---|
With triethylamine at 4℃; |
benzoyl chloride
xylazine
N-(5,6-dihydro-4H-[1,3]thiazin-2-yl)-N-(2,6-dimethyl-phenyl)-benzamide
Conditions | Yield |
---|---|
With pyridine |
4-methoxy-benzoyl chloride
xylazine
N-(5,6-dihydro-4H-[1,3]thiazin-2-yl)-N-(2,6-dimethyl-phenyl)-4-methoxy-benzamide
Conditions | Yield |
---|---|
With pyridine |
ortho-toluoyl chloride
xylazine
N-(5,6-dihydro-4H-[1,3]thiazin-2-yl)-N-(2,6-dimethyl-phenyl)-2-methyl-benzamide
Conditions | Yield |
---|---|
With pyridine |
chloroformic acid ethyl ester
xylazine
A
(5,6-dihydro-4H-[1,3]thiazin-2-yl)-(2,6-dimethyl-phenyl)-carbamic acid ethyl ester
B
2-((Z)-2,6-dimethyl-phenylimino)-[1,3]thiazinane-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With pyridine |
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