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inquiryAppearance:White crystalline powder Storage:R.T Package:25kg/drum Application:Used in health foods and beverages Transportation:Express/Sea/Air Port:Any port in China
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inquiryProduct name: 10-Hydroxydec-2-Enoic Acid CAS No.:765-01-5 Molecule Formula:C11H22O3 Molecule Weight:202.29 Purity: 98.0% Package: 25kg/drum Description:White or almost white crystalline powder Manufacture Standards:Enterprise Standard
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inquiryRoyal jelly acid is an organic acid separated from royal jelly by Chinese medical scientists. It is one of the important components of royal jelly and a special unsaturated organic acid. Many properties of royal jelly, such as smell and pH value, a
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10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
Stage #1: C10H17BrO2 With sodium hydroxide In ethanol at 20℃; for 3h; Stage #2: With hydrogenchloride In water pH=4; Time; | 97% |
C12H22O3
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
Stage #1: C12H22O3 With sodium carbonate In tetrahydrofuran; water at 65℃; for 3h; Stage #2: With hydrogenchloride; water In tetrahydrofuran pH=2; | 71% |
With sodium carbonate In tetrahydrofuran at 65℃; for 3h; |
Conditions | Yield |
---|---|
(i) aq. H2SO4, MeOH, (ii) /BRN= 1751370/, Py; Multistep reaction; |
10-hydroxy 8-decenoic acid ethyl ester
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 0.5h; Heating; Yield given; |
8-hydroxyoctanal
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. potassium carbonate / 1 h 2: potassium hydroxide / aq. ethanol / 0.5 h / Heating View Scheme |
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aq. hydrochloric acid / acetone / 2 h / 0 °C 2: aq. potassium carbonate / 1 h 3: potassium hydroxide / aq. ethanol / 0.5 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: LiAlH4 / diethyl ether 3: (i) aq. H2SO4, MeOH, (ii) /BRN= 1751370/, Py View Scheme |
8,8-diethoxy-octanoic acid ethyl ester
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LiAlH4 / diethyl ether 2: (i) aq. H2SO4, MeOH, (ii) /BRN= 1751370/, Py View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: diisobutylaluminium hydride / toluene / 2 h / -78 °C / Inert atmosphere 2: potassium carbonate / ethanol / 18 h / 40 °C 3: sodium carbonate / tetrahydrofuran / 3 h / 65 °C View Scheme |
N-(methyl)-N-(p-toluenesulfonyl)ethynylamine
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 98% |
With copper(l) chloride In dichloromethane at 20℃; for 4h; | 91% |
Conditions | Yield |
---|---|
In methanol at -10 - -5℃; for 2h; Inert atmosphere; | 50% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 6.5h; | 39% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C 2: [Ir(1,5-cyclooctadiene)2]triflate; (R)-(+)-(4,4'-bi-1,3-benzodioxole)-5,5'-diylbis(di(3,5-dimethylphenyl)phosphine) / tetrahydrofuran / 12 h / 40 °C / Inert atmosphere; Glovebox View Scheme |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; |
Conditions | Yield |
---|---|
With thionyl chloride; triethylamine In dichloromethane Inert atmosphere; |
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
for 0.166667h; Inert atmosphere; | 7.05 g |
10-hydroxy-2-decenoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 20 °C 2: toluene-4-sulfonic acid / dichloromethane / 20 °C View Scheme |
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