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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:off-white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as prima
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(6-METHYL-2-P-TOLYL-IMIDAZO[1,2-A](PYRIDIN-3-YL))-ACETONITRILEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
Cas:768398-03-4
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inquiry(6-METHYL-2-P-TOLYL-IMIDAZO[1,2-A]PYRIDIN-3-YL)-ACETONITRILE Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like
Cas:768398-03-4
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inquiryCas:768398-03-4
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inquiry6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
cyanomethyl bromide
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With fac-tris(2-phenylpyridinato-N,C2')iridium(III); sodium hydrogencarbonate In dimethyl sulfoxide at 20℃; for 12h; Schlenk technique; Inert atmosphere; Irradiation; regioselective reaction; | 85% |
S-cyanomethyl O-ethyl carbonodithioate
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With tris[2-phenylpyridinato-C2,N]iridium(III); N,N-dimethyl-formamide at 24℃; Minisci Aromatic Substitution; Inert atmosphere; UV-irradiation; regioselective reaction; | 61% |
With dilauryl peroxide In 1,2-dichloro-ethane at 85℃; Microwave irradiation; regioselective reaction; | 51% |
diazoacetonitrile
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With iron(III) chloride In acetonitrile at 60℃; for 6h; Sealed tube; Green chemistry; | 50% |
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
acetonitrile
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With ferrocene; bis(1-methyl-1-phenylethyl)peroxide at 20 - 100℃; for 20h; Inert atmosphere; Sealed tube; | 48% |
sodium cyanide
Trimethyl-(6-methyl-2-p-tolyl-imidazo[1,2-a]pyridin-3-ylmethyl)-ammonium; iodide
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
Yield given; | |
In water at 82 - 84℃; for 12h; |
potassium cyanide
dimethyl-(6-methyl-2-p-tolylimidazo[1,2-a]pyridin-3-ylmethyl)-amine
A
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
B
2-(4-methylphenyl)-6-methylimidazo[1,2-α]pyridine-3-acetamide
Conditions | Yield |
---|---|
Stage #1: dimethyl-(6-methyl-2-p-tolylimidazo[1,2-a]pyridin-3-ylmethyl)-amine With methyl iodide In ethanol at 20℃; for 24h; Stage #2: potassium cyanide In ethanol; water for 4h; Heating; |
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 78 percent / acetic acid / H2O / 4 h / 50 - 55 °C 2.1: MeI / ethanol / 24 h / 20 °C 2.2: H2O; ethanol / 4 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 79 percent / AcOH View Scheme |
dimethyl-(6-methyl-2-p-tolylimidazo[1,2-a]pyridin-3-ylmethyl)-amine
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
C20H24N3O2(1+)*Cl(1-)
sodium cyanide
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
Stage #1: C20H24N3O2(1+)*Cl(1-) With sodium hydroxide; water pH=7.5 - 8; Stage #2: sodium cyanide In water at 50 - 55℃; for 3h; Product distribution / selectivity; |
(5-methyl-pyridin-2-yl)amine
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / ethanol / 6 h / 20 °C / Inert atmosphere 2: ferrocene; bis(1-methyl-1-phenylethyl)peroxide / 20 h / 20 - 100 °C / Inert atmosphere; Sealed tube View Scheme |
4-(bromoacetyl)toluene
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / ethanol / 6 h / 20 °C / Inert atmosphere 2: ferrocene; bis(1-methyl-1-phenylethyl)peroxide / 20 h / 20 - 100 °C / Inert atmosphere; Sealed tube View Scheme |
ethanol
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
ethyl 6-methyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine-3-acetate
Conditions | Yield |
---|---|
With sulfuric acid; water at 90℃; for 12h; | 95% |
With sulfuric acid at 90℃; for 12h; | 95% |
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
6-methyl-2-(4-methylphenyl)-imidazo<1,2-a>pyridine-3-acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water | 91% |
Stage #1: 6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine With sulfuric acid; water at 110℃; for 4 - 5h; Stage #2: With sodium hydroxide; water at 0℃; pH=9; Stage #3: With water; acetic acid pH=5.5; Product distribution / selectivity; | 72% |
Stage #1: 6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine With hydrogenchloride In water at 25 - 100℃; for 12h; Heating / reflux; Stage #2: With potassium hydroxide In water at 25 - 105℃; for 2 - 3h; Stage #3: With acetic acid In water at 30 - 40℃; | |
Stage #1: 6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine With sodium hydroxide; water at 55 - 98℃; for 16.5h; Heating / reflux; Stage #2: With acetic acid In water at 25℃; for 4h; pH=5.3; | |
With sulfuric acid at 110℃; Inert atmosphere; |
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
3-((2H-tetrazol-5-yl)methyl)-6-methyl-2-p-tolylimidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With indium(III) chloride; sodium azide In N,N-dimethyl-formamide for 0.166667h; Microwave irradiation; | 76% |
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / H2O, HCl View Scheme |
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
N,N,6-trimethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine-3-acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 91 percent / H2O, HCl View Scheme | |
Multi-step reaction with 2 steps 1.1: sulfuric acid / 110 °C / Inert atmosphere 2.1: phosphorus pentachloride / dichloromethane / Reflux; Inert atmosphere 2.2: 0 °C / Inert atmosphere View Scheme |
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