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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

3-Methyl-1-pentyn-3-ol Manufacturer/High quality/Best price/In stock

Cas:77-75-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Methylpentynol

Cas:77-75-8

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Sinotech Import&Export Corporation

Molecular Formula C6H10O Molecular Weight 98.15 CAS Registry Number 77-75-8 EINECS 201-055-5 3-Methyl-1-pentyn-3-ol Synonyms Methylpentynol Molecular Formula

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:77-75-8

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

3-methyl-1-pentyn-3-ol Melting point -30 °C Boiling point 121-122 °C (lit.) Density 0.866 g/mL at 25 °C (lit.) Vapor density 3 (vs air) Vapor pressure 6.5 mm Hg ( 20 °C) Refractive index n20/D 1.431(lit.) Flash point 8

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Meparfynol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Manufacturers

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Other

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory supply CAS 77-75-8 with competitive price

Cas:77-75-8

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1-Pentyn-3-ol,3-methyl-

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an

Methyl pentynol manufature

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

Meparfynol 77-75-8

Cas:77-75-8

Min.Order:0

Negotiable

Type:Trading Company

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#77-75-8;CAT#A839182

Cas:77-75-8

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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HENAN SUNLAKE ENTERPRISE CORPORATION

iodomethyl (2S-cis)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate 4,4-dioxide Basic information Product Name: iodomethyl (2S-cis)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-

3-Methyl-1-pentyn-3-ol 77-75-8 C6H10O

Cas:77-75-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Shanghai AngewChem Co., Ltd.

Shanghai AngewChemCo., Ltd. is an innovative enterprise on fine chemicals and pharmaceuticals. Based on Shanghai R&D center and Hunan chemical manufacturing plant, we offer chemical research, process development, and large-scale production. Com

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Shanlong Biotechnology (hebei) Co., Ltd.

Why Choose Us: 1.Own chemical factory 2.Abundant professional production experience 3.Sample is free of charge and in stock with fast delivery 4.Price,quality&service,we care that all your cares 5.Prompt reply keep in touch to sa

Methylpentynol Dormison Meparfynol cas 77-75-8

Cas:77-75-8

Min.Order:1 Kilogram

FOB Price: $125.0 / 155.0

Type:Trading Company

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Yinghao Pharm Co.,Ltd.

Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Cerametek Materials(ShenZhen)Co., Ltd.

sub/micron to mesh powders (near/spheres, whiskers, flake, fiber, porous) and grain/ball, thin/ thick metal / alloys pieces / parts, thin and thick (particle) film materials /target, and custom-made crystals, substrates/parts. In the industries and a

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Other

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Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

1-Pentyn-3-ol,3-methyl-

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Pure Chemistry Scientific Inc.

Meparfynol Application:814097

Meparfynol

Cas:77-75-8

Min.Order:1 Gram

FOB Price: $500.0

Type:Trading Company

inquiry

Nanjing Raymon Biotech Co., Ltd.

Meparfynol 77-75-8Appearance:solid or liquid Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shangha

Meparfynol 77-75-8

Cas:77-75-8

Min.Order:0

Negotiable

Type:Trading Company

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Skyrun Industrial Co.,Ltd

Price, Purity Application:reagent

CSR081605-63063

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zhejiang Chemline International Co., Ltd.

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Jinan Great Chemical Co.,Ltd.

Application:Pharmaceutical intermediates

3-Methyl-1-pentyn-3-ol

Cas:77-75-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

77-75-8

Cas:77-75-8

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

butanone
78-93-3

butanone

acetylene
74-86-2

acetylene

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran at 0℃;100%
With tetra(n-butyl)ammonium hydroxide In water; dimethyl sulfoxide at 5℃; for 1h; Favorskii-Babayan Synthesis;78%
With sodium amide
butanone
78-93-3

butanone

lithium acetylide
70277-75-7

lithium acetylide

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
In diethyl ether at -78℃; for 4h;66.1%
butanone
78-93-3

butanone

acetylenemagnesium bromide
4301-14-8

acetylenemagnesium bromide

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
In tetrahydrofuran Heating;52%
With tetrahydrofuran
Stage #1: butanone; acetylenemagnesium bromide In tetrahydrofuran at 0 - 20℃;
Stage #2: With ammonium chloride In tetrahydrofuran; water
In tetrahydrofuran at -10 - 20℃;
3,6-dimethyl-oct-4-yne-3,6-diol
78-66-0

3,6-dimethyl-oct-4-yne-3,6-diol

A

butanone
78-93-3

butanone

B

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
With potassium carbonate
With potassium carbonate
sodium acetylide
1066-26-8

sodium acetylide

butanone
78-93-3

butanone

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
With ammonia
3-chloro-3-methylpent-1-yne
14179-94-3

3-chloro-3-methylpent-1-yne

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
With water; calcium carbonate at 80 - 90℃;
ethylamine
75-04-7

ethylamine

1-bromo-3-methyl-1,2-pentadiene
10575-70-9

1-bromo-3-methyl-1,2-pentadiene

A

3-ethylamino-3-methyl-1-pentyne
14465-45-3

3-ethylamino-3-methyl-1-pentyne

B

(E,E)-N-ethyl-4-methyl-1-aza-1,3-hexadiene

(E,E)-N-ethyl-4-methyl-1-aza-1,3-hexadiene

C

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
With potassium hydroxide at 25℃; for 120h;A 91 % Chromat.
B n/a
C 7 % Chromat.
tert-butylamine
75-64-9

tert-butylamine

1-bromo-3-methyl-1,2-pentadiene
10575-70-9

1-bromo-3-methyl-1,2-pentadiene

A

3-t-butylamino-3-methyl-1-pentyne
1185-98-4

3-t-butylamino-3-methyl-1-pentyne

B

(E,E)-N-t-butyl-4-methyl-1-aza-1,3-hexadiene

(E,E)-N-t-butyl-4-methyl-1-aza-1,3-hexadiene

C

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
With potassium hydroxide at 100℃; for 5h; Yield given;A 57 % Chromat.
B n/a
C 23 % Chromat.
sodium amide

sodium amide

butanone
78-93-3

butanone

acetylene
74-86-2

acetylene

meparfynol
77-75-8

meparfynol

sodium amide

sodium amide

butanone
78-93-3

butanone

acetylene
74-86-2

acetylene

A

3,6-dimethyl-oct-4-yne-3,6-diol
78-66-0

3,6-dimethyl-oct-4-yne-3,6-diol

B

meparfynol
77-75-8

meparfynol

water
7732-18-5

water

3-chloro-3-methylpent-1-yne
14179-94-3

3-chloro-3-methylpent-1-yne

CaCO3

CaCO3

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
at 80 - 90℃;
butanone
78-93-3

butanone

potassium acetylenide

potassium acetylenide

meparfynol
77-75-8

meparfynol

3,6-dimethyl-oct-4-yne-3,6-diol
78-66-0

3,6-dimethyl-oct-4-yne-3,6-diol

K2CO3

K2CO3

A

butanone
78-93-3

butanone

B

acetylene
74-86-2

acetylene

C

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
at 170℃; mixtures of stereoisomer(ic)/s;
at 170℃; mixtures of stereoisomer(ic)/s;
3-Hydroxy-3-methyl-1-trimethylsilyl-pentin-(1)
17889-43-9

3-Hydroxy-3-methyl-1-trimethylsilyl-pentin-(1)

meparfynol
77-75-8

meparfynol

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran; methanol at 20℃; for 1h; Inert atmosphere;
3,4-dihydro-2H-pyran
110-87-2

3,4-dihydro-2H-pyran

meparfynol
77-75-8

meparfynol

2-(3-methylpent-1-yn-3-yloxy)tetrahydro-2H-pyran
28659-16-7

2-(3-methylpent-1-yn-3-yloxy)tetrahydro-2H-pyran

Conditions
ConditionsYield
With lithium hexafluorophosphate In hexane at 10 - 15℃; for 0.25h;100%
With toluene-4-sulfonic acid In dichloromethane at -20℃; for 1h;84%
With calcium chloride In dichloromethane at 25℃; for 2h;80%
acetic anhydride
108-24-7

acetic anhydride

meparfynol
77-75-8

meparfynol

3-acetoxy-3-ethylbutyne
1185-96-2

3-acetoxy-3-ethylbutyne

Conditions
ConditionsYield
tetrafluoroboric acid; silica gel at 20℃; for 2h;100%
indium(III) chloride at 20℃; for 0.5h;100%
With zirconium(IV) chloride at 20℃; for 1h;100%
meparfynol
77-75-8

meparfynol

(E)-3-methylpent-3-en-2-one
1567-73-3

(E)-3-methylpent-3-en-2-one

Conditions
ConditionsYield
With NH4NO3-exchanged zeolite HSZ-320 In chlorobenzene at 130℃; for 4h;100%
With sulfuric acid; acetic acid In chloroform for 1h; Heating;70%
With formic acid oder dessen Acetat;
phenyl isocyanate
103-71-9

phenyl isocyanate

meparfynol
77-75-8

meparfynol

3-methylpent-1-yn-3-yl phenylcarbamate
32496-85-8

3-methylpent-1-yn-3-yl phenylcarbamate

Conditions
ConditionsYield
With dmap; triethylamine In tetrahydrofuran at 20℃; for 90h;100%
carbon dioxide
124-38-9

carbon dioxide

meparfynol
77-75-8

meparfynol

4-ethyl-4-methyl-5-methylene-1,3-dioxolan-2-one
80956-52-1

4-ethyl-4-methyl-5-methylene-1,3-dioxolan-2-one

Conditions
ConditionsYield
With polystyrene-supported N-heterocyclic carbene-silver complex at 40℃; under 37503.8 Torr; for 24h; Autoclave;99%
With [(triphenylphosphine)2Ag]2CO3 In neat (no solvent) at 25℃; under 750.075 Torr; for 3h; Schlenk technique;99%
With 1,8-diazabicyclo[5.4.0]undec-7-ene at 30℃; under 7500.75 Torr; for 8h; Catalytic behavior; Autoclave; Green chemistry;98%
benzyl azide
622-79-7

benzyl azide

meparfynol
77-75-8

meparfynol

C13H17N3O
1354827-07-8

C13H17N3O

Conditions
ConditionsYield
With (η5-C5Me5)Ru(P(i-Pr)3)Cl In dichloromethane at 20℃; for 0.0166667h;99%
carbon dioxide
124-38-9

carbon dioxide

N-butylamine
109-73-9

N-butylamine

meparfynol
77-75-8

meparfynol

3-butyl-5-ethyl-5-methyl-4-methylene-oxazolidin-2-one
91356-08-0

3-butyl-5-ethyl-5-methyl-4-methylene-oxazolidin-2-one

Conditions
ConditionsYield
With copper(l) iodide at 30℃; under 750.075 Torr; for 12h; Schlenk technique; Ionic liquid;99%
With silver(I) tungstate; triphenylphosphine In neat (no solvent) at 50℃; under 3750.38 Torr; for 12h; Molecular sieve;89%
With triphenylphosphine In dimethyl sulfoxide at 50℃; under 750.075 Torr; for 12h;> 99 %Spectr.
5-chloro-2-iodoaniline
6828-35-9

5-chloro-2-iodoaniline

meparfynol
77-75-8

meparfynol

1-(2-amino-4-chlorophenyl)-3-methylpent-1-yn-3-ol

1-(2-amino-4-chlorophenyl)-3-methylpent-1-yn-3-ol

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 30℃; for 4h; Inert atmosphere;99%
carbon dioxide
124-38-9

carbon dioxide

meparfynol
77-75-8

meparfynol

C13H20O4

C13H20O4

Conditions
ConditionsYield
With C9H16N2*C5H5NO at 50℃; under 3750.38 Torr; for 18h;99%
meparfynol
77-75-8

meparfynol

3-hydroxy-3-methyl-1-pentene
918-85-4

3-hydroxy-3-methyl-1-pentene

Conditions
ConditionsYield
With quinoline; hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760.051 Torr;98%
With potassium hydroxide; hydrogen; Lindlar's catalyst In pentane for 4h;88%
With hydrogen; palladium on barium sulfate In pyridine for 2h; reduced pressure;67.3%
bis(triphenylphosphine)palladium(II) dichloride

bis(triphenylphosphine)palladium(II) dichloride

3-cyclopentyl-2-(4-iodo-phenyl)-propionic acid methyl ester
372080-84-7

3-cyclopentyl-2-(4-iodo-phenyl)-propionic acid methyl ester

meparfynol
77-75-8

meparfynol

3-cyclopentyl-2-[4-(3-hydroxy-3-methyl-pent-1-ynyl)-phenyl]-propionic acid methyl ester

3-cyclopentyl-2-[4-(3-hydroxy-3-methyl-pent-1-ynyl)-phenyl]-propionic acid methyl ester

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide98%
2-Methoxypropene
116-11-0

2-Methoxypropene

meparfynol
77-75-8

meparfynol

6-methyl-octa-4,5-dien-2-one
1043584-53-7

6-methyl-octa-4,5-dien-2-one

Conditions
ConditionsYield
With sulfonic acid resin T239 at 90℃; for 5h; Autoclave; Inert atmosphere;98%
sulfuric acid In methanol at 95 - 105℃; for 1.91667 - 20h; Product distribution / selectivity;95%
carbon dioxide
124-38-9

carbon dioxide

benzyl alcohol
100-51-6

benzyl alcohol

meparfynol
77-75-8

meparfynol

benzyl (3-methyl-2-oxopentan-3-yl) carbonate

benzyl (3-methyl-2-oxopentan-3-yl) carbonate

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc(II) chloride In acetonitrile at 80℃; under 7500.75 Torr; for 24h; Autoclave; Sealed tube; chemoselective reaction;98%
With tetrabutylammomium bromide; silver sulfadiazine at 80℃; under 750.075 Torr; for 18h; Schlenk technique;98%
With triphenylphosphine; silver carbonate In acetonitrile at 80℃; under 7500.75 Torr; for 18h; Autoclave;93%
With DBN In N,N-dimethyl-formamide at 50℃; under 7500.75 Torr; for 6h;90 %Spectr.
meparfynol
77-75-8

meparfynol

rac-3-hydroxy-3-methylpentanenitrile
14368-30-0

rac-3-hydroxy-3-methylpentanenitrile

Conditions
ConditionsYield
With C24H20N2O4Ru; hydrazine hydrate In toluene at 150℃; Inert atmosphere; Microwave irradiation;98%
t-butyldimethylsiyl triflate
69739-34-0

t-butyldimethylsiyl triflate

meparfynol
77-75-8

meparfynol

tert-butyldimethyl((3-methylpent-1-yn-3-yl)oxy)silane
128176-27-2

tert-butyldimethyl((3-methylpent-1-yn-3-yl)oxy)silane

Conditions
ConditionsYield
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 2h; Inert atmosphere;98%
meparfynol
77-75-8

meparfynol

A

3-hydroxy-3-methyl-1-pentene
918-85-4

3-hydroxy-3-methyl-1-pentene

B

3-methylpentan-3-ol
77-74-7

3-methylpentan-3-ol

Conditions
ConditionsYield
With hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760.051 Torr; for 0.0666667h; Product distribution; Kinetics; Further Variations:; Catalysts; reaction time;A 97%
B 3%
With sodium hydroxide; copper bei der elektrolytischen Reduktion;
With quinoline; hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760.051 Torr; Kinetics; Product distribution; Further Variations:; Catalysts; Solvents;
With sodium bromate; acetic acid; hydrazine In water at 20 - 60℃; for 5h;
With hydrogen In toluene at 139.84℃; under 67506.8 Torr; Reagent/catalyst; Flow reactor;
Phenylselenyl chloride
5707-04-0

Phenylselenyl chloride

meparfynol
77-75-8

meparfynol

E-1-phenylseleno-2-chloro-3-methyl-1-penten-3-ol
77955-92-1

E-1-phenylseleno-2-chloro-3-methyl-1-penten-3-ol

Conditions
ConditionsYield
In dichloromethane Ambient temperature;97%
pyrrolidine
123-75-1

pyrrolidine

carbon dioxide
124-38-9

carbon dioxide

meparfynol
77-75-8

meparfynol

3-methyl-2-oxopentan-3-yl pyrrolidine-1-carboxylate

3-methyl-2-oxopentan-3-yl pyrrolidine-1-carboxylate

Conditions
ConditionsYield
With silver(I) tungstate; triphenylphosphine In neat (no solvent) at 50℃; under 3750.38 Torr; for 12h;97%
With [2,2]bipyridinyl; copper at 100℃; under 28880 Torr; for 24h;90 % Chromat.
With silver(I) bromide In neat (no solvent) at 50℃; under 11251.1 Torr; for 5h; Schlenk technique;92 %Chromat.
With laccase and 2,2,6,6-tetra-methylpiperidine-1oxyl immobilized onto glycidyloxypropyl functionalized fibrous phosphosilicate nanoparticles In water at 50℃; under 1125.11 Torr; Schlenk technique; Green chemistry;94 %Chromat.
(2-iodo-9-isopropyl-9H-purin-6-yl)(4-methoxybenzyl)amine
267885-16-5

(2-iodo-9-isopropyl-9H-purin-6-yl)(4-methoxybenzyl)amine

meparfynol
77-75-8

meparfynol

OL 567

OL 567

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-butylamine In N,N-dimethyl-formamide at 80℃; Substitution;97%
2,5-diphenyl-3-iodoselenophene
950894-38-9

2,5-diphenyl-3-iodoselenophene

meparfynol
77-75-8

meparfynol

1-(2,5-diphenylselenophen-3-yl)-2-methylpent-1-yn-3-ol
1032198-08-5

1-(2,5-diphenylselenophen-3-yl)-2-methylpent-1-yn-3-ol

Conditions
ConditionsYield
With triethylamine; bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 20℃; for 12h; Sonogashira coupling;97%
meparfynol
77-75-8

meparfynol

1-bromo-3-methyl-pent-1-yn-3-ol
2028-52-6

1-bromo-3-methyl-pent-1-yn-3-ol

Conditions
ConditionsYield
With potassium hydroxide; potassium hypobromite In pentane for 0.5h; Ambient temperature;96%
With potassium hypobromite
With sodium hypobromide
phenyl isocyanate
103-71-9

phenyl isocyanate

meparfynol
77-75-8

meparfynol

5-ethyl-5-methyl-4-methylene-3-phenyloxazolidin-2-one
74470-78-3

5-ethyl-5-methyl-4-methylene-3-phenyloxazolidin-2-one

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 40℃; for 12h; Inert atmosphere;96%
With sodium methylate In cyclohexane
piperidine
110-89-4

piperidine

carbon dioxide
124-38-9

carbon dioxide

meparfynol
77-75-8

meparfynol

Piperidine-1-carboxylic acid 1-ethyl-1-methyl-2-oxo-propyl ester

Piperidine-1-carboxylic acid 1-ethyl-1-methyl-2-oxo-propyl ester

Conditions
ConditionsYield
With triphenylphosphine; silver carbonate In acetonitrile at 30℃; for 16h; Schlenk technique;96%
With [2,2]bipyridinyl; copper at 100℃; under 28880 Torr; for 24h;94 % Chromat.
With silver(I) bromide In neat (no solvent) at 50℃; under 11251.1 Torr; for 5h; Schlenk technique;88 %Chromat.
(2-iodo-9-isopropyl-9H-purin-6-yl)(3,4-dimethoxybenzyl)amine

(2-iodo-9-isopropyl-9H-purin-6-yl)(3,4-dimethoxybenzyl)amine

meparfynol
77-75-8

meparfynol

1-[6-(3,4-dimethoxy-benzylamino)-9-isopropyl-9H-purin-2-yl]-3-methyl-pent-1-yn-3-ol

1-[6-(3,4-dimethoxy-benzylamino)-9-isopropyl-9H-purin-2-yl]-3-methyl-pent-1-yn-3-ol

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-butylamine In N,N-dimethyl-formamide at 80℃; Substitution;96%
6-iodo-1-(triisopropylsilyl)indoline

6-iodo-1-(triisopropylsilyl)indoline

meparfynol
77-75-8

meparfynol

3-methyl-1-(1-(triisopropylsilyl)indolin-6-yl)pent-1-yn-3-ol

3-methyl-1-(1-(triisopropylsilyl)indolin-6-yl)pent-1-yn-3-ol

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 40℃; for 2h; Sonogashira Cross-Coupling; Inert atmosphere;96%
methanol
67-56-1

methanol

carbon monoxide
201230-82-2

carbon monoxide

meparfynol
77-75-8

meparfynol

Methyl 4-hydroxy-4-methylhex-2-ynoate
90199-69-2

Methyl 4-hydroxy-4-methylhex-2-ynoate

Conditions
ConditionsYield
With sodium acetate; copper dichloride; palladium dichloride at 12 - 13℃; for 1.5h;95.6%
With sodium acetate; copper dichloride; palladium dichloride38%
(2-iodo-9-isopropyl-9H-purin-6-yl)(phenyl)amine
267885-23-4

(2-iodo-9-isopropyl-9H-purin-6-yl)(phenyl)amine

meparfynol
77-75-8

meparfynol

1-(9-isopropyl-6-phenylamino-9H-purin-2-yl)-3-methyl-pent-1-yn-3-ol

1-(9-isopropyl-6-phenylamino-9H-purin-2-yl)-3-methyl-pent-1-yn-3-ol

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-butylamine In N,N-dimethyl-formamide at 80℃; Substitution;95%
(2-iodo-9-isopropyl-9H-purin-6-yl)(4-methoxyphenyl)amine

(2-iodo-9-isopropyl-9H-purin-6-yl)(4-methoxyphenyl)amine

meparfynol
77-75-8

meparfynol

1-[9-isopropyl-6-(4-methoxy-phenylamino)-9H-purin-2-yl]-3-methyl-pent-1-yn-3-ol

1-[9-isopropyl-6-(4-methoxy-phenylamino)-9H-purin-2-yl]-3-methyl-pent-1-yn-3-ol

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-butylamine In N,N-dimethyl-formamide at 80℃; Substitution;95%
1-iodo-1-hexyne
1119-67-1

1-iodo-1-hexyne

meparfynol
77-75-8

meparfynol

3-methyl-undeca-4,6-diyn-3-ol
333753-95-0

3-methyl-undeca-4,6-diyn-3-ol

Conditions
ConditionsYield
With pyrrolidine; copper(l) iodide95%

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