As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:77-74-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryEstablished in 2010, located in Hangzhou Qinglan science park, lingruichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. In our R&D centre, we have a staff of skilled and experie
Cas:77-74-7
Min.Order:1 Gram
Negotiable
Type:Other
inquiryItems Standard Result Appearance Transparent liquid Transparent liquid Assay, % ≥99%
Cas:77-74-7
Min.Order:1 Kilogram
FOB Price: $100.0 / 200.0
Type:Manufacturers
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:77-74-7
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:77-74-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryProduct Name: 3-Methyl-3-pentanol Synonyms: 3-methyl-3-pentano;3-Methyl-pentanol-(3);3-Pentanol,3-methyl-;Diethylmetylcarbinol;Methyl-3 pentanol-3;Methyldiaethylcarbinol;3-METHYL-3-PENTANOL;3-METHYLPENTAN-3-OL CAS: 77-74-7
Cas:77-74-7
Min.Order:1 Kilogram
FOB Price: $8900.0
Type:Lab/Research institutions
inquiryAppearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao
Cas:77-74-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:77-74-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:77-74-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:77-74-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:77-74-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryhigh qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Cas:77-74-7
Min.Order:0
Negotiable
Type:Manufacturers
inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:77-74-7
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Top purity 3-methyl-3-pentanol with high quality cas:77-74-7 Application:Top purity 3-methyl-3-pentanol with high quality cas:77-74-7
Cas:77-74-7
Min.Order:0
Negotiable
Type:Other
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
Cas:77-74-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryTop purity 3-methyl-3-pentanol with high quality cas:77-74-7Appearance:Transparent liquid Storage:Rom tep. Package:25kg net/paper drum Application:used Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport
Cas:77-74-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:77-74-7
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryiodomethyl (2S-cis)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate 4,4-dioxide Basic information Product Name: iodomethyl (2S-cis)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-
Cas:77-74-7
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryWhy Choose Us: 1.Own chemical factory 2.Abundant professional production experience 3.Sample is free of charge and in stock with fast delivery 4.Price,quality&service,we care that all your cares 5.Prompt reply keep in touch to sa
Cas:77-74-7
Min.Order:1 Kilogram
FOB Price: $330.0 / 355.0
Type:Trading Company
inquiryQingdao Sigma Chemical Ltd is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additives, herbal extracts, agrochemicals and fine chemicals etc. Our Labo
Cas:77-74-7
Min.Order:1 Gram
FOB Price: $1.0
Type:Trading Company
inquiryBaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art
Aopharm is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in modes of
With about ten years experiences in the field of pharmaceutical chemicals, Yierdechem has established solid business cooperation relationships with many large companys worldwide.As a leading supplier of API and pharmaceutical intermediates, holds its
Conditions | Yield |
---|---|
With oxygen In benzene at 60℃; under 760.051 Torr; for 1h; Catalytic behavior; Reagent/catalyst; Solvent; | 99% |
With 4-nitroperbenzoic acid In chloroform at 60℃; Rate constant; proportion of velocity of the hydroxylation of tert- and sec. C-H-bonds; | 84% |
With 4-nitroperbenzoic acid In chloroform at 60℃; | 84% |
With lithium aluminium tetrahydride; O(3P) Yield given. Multistep reaction; | |
With tris(μ-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate; dihydrogen peroxide; acetic acid In acetonitrile at 20℃; for 2h; Product distribution; Mechanism; bond selectivity; |
3-(2-Methoxy-ethoxymethoxy)-3-methyl-pentane
3-methylpentan-3-ol
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In butanone for 8h; Heating; | 99% |
Conditions | Yield |
---|---|
With hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760.051 Torr; for 0.0666667h; Product distribution; Kinetics; Further Variations:; Catalysts; reaction time; | A 97% B 3% |
With sodium hydroxide; copper bei der elektrolytischen Reduktion; | |
With quinoline; hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760.051 Torr; Kinetics; Product distribution; Further Variations:; Catalysts; Solvents; | |
With sodium bromate; acetic acid; hydrazine In water at 20 - 60℃; for 5h; | |
With hydrogen In toluene at 139.84℃; under 67506.8 Torr; Reagent/catalyst; Flow reactor; |
3-(methoxymethoxy)-3-methylpentane
3-methylpentan-3-ol
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In butanone for 3h; Heating; | 96% |
Conditions | Yield |
---|---|
With oxygen In dichloromethane at 25℃; under 760.051 Torr; for 2h; | A 90% B 7% |
Conditions | Yield |
---|---|
With iodosylbenzene In dichloromethane at 25℃; for 2h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; | A 77% B 9% |
3-methylpentane
A
3-methylpentan-3-ol
B
3-methyl-pentan-2-one
C
3-Methyl-2,4-pentanedione
Conditions | Yield |
---|---|
With iodosylbenzene In dichloromethane at 25℃; for 2h; Catalytic behavior; Solvent; Reagent/catalyst; Inert atmosphere; | A 61% B 7% C 28% |
3-methylpentane
A
3-methylpentan-2-ol
B
3-methylpentan-3-ol
C
3-methyl-pentan-2-one
Conditions | Yield |
---|---|
With iodosylbenzene In dichloromethane at 25℃; for 3h; Solvent; Inert atmosphere; | A 10% B 60% C 18% |
3-methylpentane
A
3-methylpentan-2-ol
B
3-methyl-1-pentanol
C
3-methylpentan-3-ol
D
3-methyl-pentan-2-one
Conditions | Yield |
---|---|
With iodosylbenzene In dichloromethane at 25℃; for 2h; Inert atmosphere; | A 14% B 12% C 57% D 13% |
With iodosylbenzene In dichloromethane at 25℃; for 2h; Inert atmosphere; | A 11% B 24% C 52% D 6% |
Conditions | Yield |
---|---|
With O(3P) Product distribution; | A 52% B n/a |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; air; cobalt(II) acetate In benzonitrile at 100℃; under 7600 Torr; for 8h; Oxidation; | A 13% B 24% |
Conditions | Yield |
---|---|
With water at 50℃; for 16h; | 6.9% |
Multi-step reaction with 2 steps 1: HI 2: diluted KOH-solution View Scheme |
ethylmagnesium iodide
diethyl ether
benzhydryl acetate
A
ethane
B
3-methylpentan-3-ol
C
benzhydryl ether
Conditions | Yield |
---|---|
Behandeln des Reaktionsprodukts mit Wasser; |
Conditions | Yield |
---|---|
With diethyl ether man zerlegt das Reaktionsprodukt mit angesaeuertem Wasser; |
diethyl ether
acetoxytrichlorosilane
ethylmagnesium bromide
A
3-methylpentan-3-ol
B
triethylsilane
3-iodo-3-methylpentane
3-methylpentan-3-ol
Conditions | Yield |
---|---|
With potassium hydroxide |
2-iodo-3-methyl-pentane
3-methylpentan-3-ol
Conditions | Yield |
---|---|
With zinc in eisessigalkoholischer Loesung; | |
Multi-step reaction with 3 steps 1: glacial acetic acid; zinc 2: HI 3: diluted KOH-solution View Scheme |
Conditions | Yield |
---|---|
With diethyl ether unter Eiskuehlung; |
Conditions | Yield |
---|---|
analog verlaeuft die Reaktion mit Chloressigsaeureaethylester, β-Jod-propionsaeure-aethylester, Buttersaeureester, Isovaleriansaeureester; | |
analog verlaeuft die Reaktion mit n-Capronsaeureester und Pelargonsaeureester; |
Acetol acetate
ethylmagnesium bromide
A
3-methylpentan-3-ol
B
acetic acid-(2-hydroxy-2-methyl-butyl ester)
Acetol acetate
A
3-methylpentan-3-ol
B
acetic acid-(2-hydroxy-2-methyl-butyl ester)
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
With diethyl ether; benzene |
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
nachfolgendes Hydrolysieren mit Eiswasser und wenig Salzsaeure; |
Conditions | Yield |
---|---|
With diethyl ether und Behandlung des Reaktionsgemisches mit Eiswasser und wenig Salzsaeure; |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; dimethyl sulfoxide for 0.166667h; | 94% |
With hydrogenchloride at 15 - 20℃; | 56% |
With hydrogenchloride; copper(II) sulfate |
3-methylpentan-3-ol
methanesulfonic acid 3-(naphthalen-2-oxy)-1-propyl ester
B
2-(3-fluoro-n-propoxy)naphthalene
Conditions | Yield |
---|---|
With cesium fluoride at 80℃; for 6h; | A 3 % Spectr. B 94% |
3-methylpentan-3-ol
Conditions | Yield |
---|---|
In benzene byproducts: HN(Si(CH3)3)2; under dry N2; soln. of alcohol and Zn-compd. refluxed for 10h, pptn.; filtered, washed (benzene), dried; elem. anal.; | 93% |
Conditions | Yield |
---|---|
In diethyl ether Et2MeCOH was added dropwise to soln. In(N-t-Bu(SiMe3))3 in ether at room temp. and stirred for 2 days; volatile components were distilled in vacuo, residue was extracted withhexane, filtered, evapd., and sublimated at 135-150°C and 1E-2 mmHg; elem. anal.; | 92% |
3-methylpentan-3-ol
2-Bromoacetyl bromide
1-ethyl-1-methylpropyl bromoacetate
Conditions | Yield |
---|---|
In dichloromethane; N,N-dimethyl-aniline | 89% |
With N,N-dimethyl-aniline In dichloromethane at 20℃; for 2h; | 89% |
3-methylpentan-3-ol
3-azido-3-methylpentane
Conditions | Yield |
---|---|
With sodium azide; trifluoroacetic acid In chloroform at -5 - 0℃; Inert atmosphere; | 87% |
With trimethylsilylazide; boron trifluoride diethyl etherate In benzene for 24h; Ambient temperature; |
3-methylpentan-3-ol
(ethylimido)tris(diethylamido)tantalum
(ethylimido)tri(1-ethyl-1-methylpropyloxo)-tantalum
Conditions | Yield |
---|---|
In toluene at 20℃; for 12h; | 87% |
Conditions | Yield |
---|---|
With sulfuric acid In dichloromethane at 20℃; Cooling with ice; | 87% |
Conditions | Yield |
---|---|
With triethylamine In toluene byproducts: triethylamine hydrochloride; oxalyl dichloride added to Ni complex in toluene (protected from moisture), gently heated with stirring for 15 min, treated with alcohol, refluxed for 30 min, treated with excess Et3N, refluxed for 30 min; filtered, evapd.(vac.), washed (water), dried, chromy.(Alumina-toluene/acetone 50:1), concd., crystd., elem. anal.; | 85% |
Conditions | Yield |
---|---|
Stage #1: 3-methylpentan-3-ol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Inert atmosphere; Stage #2: bromoacetic acid In tetrahydrofuran; mineral oil Inert atmosphere; Reflux; | 82% |
3-methylpentan-3-ol
O-<2-(Trimethylsilyl)ethyl>glycolic acid
2-[2-(trimethylsilyl)ethyl]-acetic acid 1-ethyl-1-methylpropyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; | 81% |
3-methylpentan-3-ol
2-methoxyacetic acid
2-methoxyacetic acid 1-ethyl-1-methylpropyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; | 80% |
Conditions | Yield |
---|---|
With tantalum pentachloride In dichloromethane for 0.166667h; Ambient temperature; | 76% |
3-methylpentan-3-ol
1-bromo-2-fluoro-4-nitrobenzene
Conditions | Yield |
---|---|
With potassium hydride In tetrahydrofuran at 20℃; for 2h; | 76% |
Conditions | Yield |
---|---|
Stage #1: 3-methylpentan-3-ol With hydrogen bromide; acetic acid; thiourea In water for 3h; Inert atmosphere; Reflux; Stage #2: With sodium hydroxide In water at 20℃; Stage #3: With sulfuric acid at 10℃; pH=2 - 3; | 73% |
3-methylpentan-3-ol
Conditions | Yield |
---|---|
With iodobenzene; silver(I) acetate; palladium diacetate In 1,2-dichloro-ethane at 120℃; for 24h; Schlenk technique; Sealed tube; | 72% |
3-methylpentan-3-ol
tantalum pentachloride
tert-butylamine
(tert-butylimido)tris(1-ethyl-1-methylpropyloxo)tantalum
Conditions | Yield |
---|---|
Stage #1: 3-methylpentan-3-ol; tert-butylamine With n-butyllithium In hexane at 20℃; for 12h; Stage #2: tantalum pentachloride In hexane at 20℃; for 24h; | 71% |
Conditions | Yield |
---|---|
With aluminum oxide for 1h; Ambient temperature; | 70% |
3-methylpentan-3-ol
benzyloxyacetic acid
2-(phenylmethoxy)acetic acid 1-ethyl-1-methylpropyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; | 68% |
3-methylpentan-3-ol
Glycine ethyl ester isocyanate
ethyl {[(1-ethyl-1-methylpropyloxy)carbonyl]amino}acetate
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; dichloromethane; water at 20℃; | 67% |
Stage #1: Glycine ethyl ester isocyanate With hydrogenchloride In 1,4-dioxane; dichloromethane; water at 20℃; for 0.0833333h; Stage #2: 3-methylpentan-3-ol In 1,4-dioxane; dichloromethane; water | 67% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; palladium diacetate; trifluoroacetic acid In cyclohexane at 100℃; for 0.5h; | 66% |
Conditions | Yield |
---|---|
Stage #1: 3-methylpentan-3-ol; potassium cyanide With sulfuric acid; acetic acid at 20℃; for 23.42h; Ritter Reaction; Stage #2: With sodium hydroxide; water at 0℃; pH=9; | 64% |
3-methylpentan-3-ol
niobium pentachloride
isopropylamine
(isopropylimido)tris(1-ethyl-1-methylpropyl-oxo)niobium
Conditions | Yield |
---|---|
Stage #1: 3-methylpentan-3-ol; isopropylamine With n-butyllithium In hexane at 20℃; for 12h; Stage #2: niobium pentachloride In hexane at 20℃; for 14h; | 64% |
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