DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:592-20-1
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Cas:592-20-1
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Type:Manufacturers
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Min.Order:5 Kiloliter
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Type:Manufacturers
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Type:Trading Company
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:592-20-1
Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: ACETOXYACETONE CAS: 592-20-1 MF: C5H8O3 MW: 116.12 EINECS: 209-746-3 Mol File: 592-20-1.mol ACETOXYACETONE Structure ACETOXYACETONE Chemical Properties Melting point 74.0-75.5 °C Boiling point 174-176 &de
ACETOXYACETONECAS:592-20-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
Cas:592-20-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:592-20-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Name: ACETOXYACETONE Synonyms: Acetoxy-2-propanone (stabilized with Mg6Al2(OH)16CO3.4H2O);Acetic acid acetonyl ester;Acetoxyacetone,95%;Acetol Acetate Acetoxyacetone;(stabilized with Mg6Al2(OH)16CO3.4H2O);Acetoxy-2-propanone ;Acetic acid-
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryAcetic acid-2-oxo-propyl ester CAS: 592-20-1 Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard Shelf life 2 years Storage should be stored i
Cas:592-20-1
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:592-20-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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Min.Order:0 Metric Ton
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Min.Order:0
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:592-20-1
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Type:Lab/Research institutions
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Cas:592-20-1
Min.Order:1 Kilogram
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Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:592-20-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:592-20-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
We produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphineoxide)dioxouranium(VI) perchlorate In dichloromethane-d2 at 22℃; for 2.5h; | 99% |
Conditions | Yield |
---|---|
With 18-crown-6 ether In tetrahydrofuran for 2h; Heating; | 92% |
at 140 - 150℃; | |
In N,N-dimethyl-formamide at 100℃; for 21h; | |
In N,N-dimethyl-formamide at 100℃; for 21h; |
Conditions | Yield |
---|---|
In benzene for 2h; Inert atmosphere; Reflux; regioselective reaction; | 91% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetrabutylammomium bromide In acetone at 120℃; under 33753.4 Torr; for 0.5h; Inert atmosphere; Microwave irradiation; | 88% |
3,3-dimethyldioxirane
pentan-3-one
A
Acetol acetate
B
1-methyl-2-oxobutyl acetate
Conditions | Yield |
---|---|
In acetone Heating; Yields of byproduct given; | A n/a B 64.6% |
3,3-dimethyldioxirane
cyclohexanone
A
Acetol acetate
B
2-acetoxycyclohexanone
Conditions | Yield |
---|---|
In acetone Heating; | A n/a B 57.6% |
methanol
Acetyl(1-chlor-1-methylethyl)peroxid
A
Acetol acetate
B
Acetyl(1-methoxy-1-methylethyl)peroxid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In chloroform-d1 at 0℃; for 20h; Yields of byproduct given; | A n/a B 57% |
3,3-dimethyldioxirane
cyclopentanone
A
Acetol acetate
B
2-acetoxycyclopentanone
Conditions | Yield |
---|---|
In acetone Heating; | A n/a B 54.3% |
3,3-dimethyldioxirane
butanone
A
3-acetoxy-2-butanone
B
Acetol acetate
C
1-acetoxybutan-3-one
D
2-oxobutyl acetate
Conditions | Yield |
---|---|
In acetone Heating; Yields of byproduct given; | A 52.3% B n/a C n/a D n/a |
In acetone Heating; Yield given. Yields of byproduct given; |
ethylbenzene
3,3-dimethyldioxirane
A
Acetol acetate
B
1-Phenylethanol
C
1-phenylethyl acetate
D
acetophenone
Conditions | Yield |
---|---|
In acetone for 48h; Ambient temperature; Further byproducts given; | A n/a B 36% C 14 % Chromat. D 50% |
3-methyl-butan-2-one
3,3-dimethyldioxirane
A
Acetol acetate
B
3-Acetoxy-3-methyl-2-butanon
C
1-(acetyloxy)-3-methyl-2-butanone
Conditions | Yield |
---|---|
In acetone Heating; Yields of byproduct given; | A n/a B 43.6% C n/a |
In acetone Heating; Yield given. Yields of byproduct given; |
3,3-dimethyldioxirane
A
methanol
B
acetic acid methyl ester
C
Acetol acetate
Conditions | Yield |
---|---|
With di-isopropyl ether In acetone at 22℃; for 6h; Product distribution; Mechanism; | A 12.1% B 38.4% C 11.8% |
3,3-dimethyldioxirane
2-Pentanone
A
Acetol acetate
B
4-(acetyloxy)-2-pentanone
C
1-(acetyloxy)-2-pentanone
D
(-)-1-Ethyl-2-oxopropyl acetate
Conditions | Yield |
---|---|
In acetone Heating; Yields of byproduct given; | A n/a B n/a C n/a D 35.9% |
In acetone Heating; Yield given. Yields of byproduct given; |
3,3-dimethyldioxirane
2,4-dimethylpentan-3-one
A
Acetol acetate
B
2-acetoxy-2,4-dimethyl-pentan-3-one
Conditions | Yield |
---|---|
In acetone Heating; Yields of byproduct given; | A n/a B 32% |
methanol
Allyl acetate
A
1,1,3-trimethoxypropane
B
3-acetoxypropanal
C
Acetol acetate
D
3-acetoxy-1,1-dimethoxy-propane
Conditions | Yield |
---|---|
With disodium hydrogenphosphate Product distribution; hexamethylphosphoric triamide; | A 16% B 3% C 11% D 28% |
Conditions | Yield |
---|---|
Heating; | 26.1% |
Mechanism; Heating; other substrates, other ketones, or mixtures of ketones; | 26.1% |
2,5-dimethoxy-2,5-dimethyl-1,4-dioxane
acetic anhydride
A
acetic acid methyl ester
B
Acetol acetate
2,5-dimethoxy-2,5-dimethyl-1,4-dioxane
acetyl chloride
A
acetic acid methyl ester
B
Acetol acetate
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
at 140 - 150℃; |
Conditions | Yield |
---|---|
at 55 - 65℃; in Gegenwart eines durch Erhitzen von HgO mit (C2H5)2O+BF3 und wenig Trichloressigsaeure in Methanol dargestellten Katalysators; | |
at 55 - 65℃; in Gegenwart eines aus HgO, Borfluorid-aetherat, Methanol und Trichloressigsaeure hergestellten Katalysators; | |
With boron trifluoride diethyl etherate; mercury(II) oxide |
Conditions | Yield |
---|---|
at 140 - 150℃; |
Conditions | Yield |
---|---|
With lead(IV) acetate; acetic acid |
Conditions | Yield |
---|---|
In acetic acid Heating; |
Conditions | Yield |
---|---|
(i) LDA, Et2O, (ii) air, (iii) /BRN= 385737/; Multistep reaction; |
manganese triacetate
acetone
Acetol acetate
Conditions | Yield |
---|---|
In acetic anhydride; acetic acid |
3,3-dimethyl-butan-2-one
3,3-dimethyldioxirane
A
Acetol acetate
B
4-(acetyloxy)-3,3-dimethyl-2-butanone
C
acetic acid 3,3-dimethyl-2-oxobutyl ester
Conditions | Yield |
---|---|
In acetone Heating; Yield given. Yields of byproduct given; |
Acetol acetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 15h; | 100% |
Acetol acetate
methyl 2,6-di-O-benzyl-3,4-di-O-trimethylsilyl-α-D-galactopyranoside
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; trimethylsilyl trifluoromethanesulfonate In diethyl ether at -20℃; for 48h; | 97% |
Acetol acetate
(2R,3S,4R,5R)-3,4-Bis-benzyloxy-2-((R)-1,2-bis-trimethylsilanyloxy-ethyl)-5-methoxy-tetrahydro-furan
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; trimethylsilyl trifluoromethanesulfonate In diethyl ether at -20℃; for 48h; | 96% |
Conditions | Yield |
---|---|
Stage #1: Acetol acetate; C22H36O8Si2 In dichloromethane at 20℃; for 1h; Molecular sieve; Stage #2: With trifluorormethanesulfonic acid; trimethylsilyl trifluoromethanesulfonate In dichloromethane at -50℃; for 16h; | 90% |
Acetol acetate
(S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol
(S,S)-2-(acetoxymethyl)-2-methyl-4,5-bis(p-toluenesulfonyloxymethyl)-1,3-dioxolane
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In chloroform Ambient temperature; | 89% |
Conditions | Yield |
---|---|
Stage #1: Acetol acetate With tert-butylamine In neat (no solvent) at 20℃; for 0.25h; Stage #2: With phenylphosphonate In neat (no solvent) at 20℃; for 0.25h; Stage #3: Dimethyl phosphite In neat (no solvent) at 50℃; for 2h; | 89% |
Acetol acetate
p-Toluic acid
N-isocyaniminotriphenylphosphorane
benzylamine
2-(benzylamino)-2-[5-(4-methylphenyl)-1,3,4-oxadiazol-2-yl]propyl acetate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3.25h; | 88% |
Acetol acetate
N-isocyaniminotriphenylphosphorane
m-Toluic acid
2-hydroxy-2-[5-(3-methylphenyl)-1,3,4-oxadiazol-2-yl]propyl acetate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 88% |
In water at 20℃; for 1h; Green chemistry; | 85% |
3,5-dimethylbenzoic acid
Acetol acetate
N-isocyaniminotriphenylphosphorane
benzylamine
2-(benzylamino)-2-[5-(3,5-dimethylphenyl)-1,3,4-oxadiazol-2-yl]propyl acetate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3.25h; | 87% |
Acetol acetate
p-Toluic acid
N-isocyaniminotriphenylphosphorane
2-hydroxy-2-[5-(4-methylphenyl)-1,3,4-oxadiazol-2-yl]propyl acetate
Conditions | Yield |
---|---|
In water at 20℃; for 1h; Green chemistry; | 86% |
In dichloromethane at 20℃; for 1h; | 83% |
Acetol acetate
Conditions | Yield |
---|---|
With titanium tetrachloride; triethylamine In dichloromethane at -78℃; for 2h; | 83% |
Acetol acetate
anthranilic acid amide
2-acetoxymethyl-2-methyl-2,3-dihydroquinazolin-4(1H)-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 5h; Reflux; | 80% |
3-bromobenzo[b]thiophene-2-carbaldehyde
Acetol acetate
C
(R)-4-(3-bromobenzo[b]thiophen-2-yl)-4-hydroxy-2-oxobutyl acetate
Conditions | Yield |
---|---|
With 5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole at 0℃; for 12h; Aldol reaction; optical yield given as %ee; regioselective reaction; | A n/a B n/a C 80% |
benzothiophene-2-carboxaldehyde
Acetol acetate
C
(R)-4-(1-benzothiophen-2-yl)-4-hydroxy-2-oxobutyl acetate
Conditions | Yield |
---|---|
With 5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole at 0℃; for 12h; Aldol reaction; optical yield given as %ee; regioselective reaction; | A n/a B n/a C 78% |
3-methylbenzo[b]thiophene-2-carboxaldehyde
Acetol acetate
B
(R)-4-hydroxy-4-(3-methylbenzo[b]thiophen-2-yl)-2-oxobutyl acetate
Conditions | Yield |
---|---|
With 5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole at 0℃; for 12h; Aldol reaction; optical yield given as %ee; regioselective reaction; | A n/a B 78% |
Conditions | Yield |
---|---|
With pyridine; titanium tetrachloride In tetrahydrofuran; dichloromethane at 0 - 20℃; for 3h; Knoevenagel Condensation; | 74% |
Conditions | Yield |
---|---|
Stage #1: Acetol acetate; 2-(3,4-dimethoxyphenyl)-ethylamine In neat (no solvent) at 20℃; for 0.25h; Stage #2: With phenylphosphonate In neat (no solvent) at 20℃; for 0.25h; Stage #3: Dimethyl phosphite In neat (no solvent) at 50℃; for 3h; | 73% |
Acetol acetate
heptanoic acid phenyl ester
Conditions | Yield |
---|---|
With titanium tetrachloride; triethylamine In dichloromethane at -78℃; for 2h; | 72% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene Heating; | 71% |
Acetol acetate
Conditions | Yield |
---|---|
With titanium tetrachloride; triethylamine In dichloromethane at -78℃; for 2h; | 70% |
Conditions | Yield |
---|---|
Stage #1: Acetol acetate; 1-amino-2-propene In neat (no solvent) at 20℃; for 0.25h; Stage #2: With phenylphosphonate In neat (no solvent) at 20℃; for 0.25h; Stage #3: Dimethyl phosphite In neat (no solvent) at 50℃; for 2h; | 69% |
Acetol acetate
ethylene glycol
methyl (2-methyl-1,3-dioxolan-2-yl)acetate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene | 68% |
benzothiophene-3-carboxaldehyde
Acetol acetate
A
(R)-4-(benzo[b]thiophen-3-yl)-4-hydroxy-2-oxobutyl acetate
Conditions | Yield |
---|---|
With 5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole at 0℃; for 12h; Aldol reaction; optical yield given as %ee; regioselective reaction; | A 65% B n/a C n/a |
Hippuric Acid
Acetol acetate
A
E-2-phenyl-4(2-acetoxy-1-methylethylidene)-2-oxazoline-5-one
B
Z-2-phenyl-4(2-acetoxy-1-methylethylidene)-2-oxazoline-5-one
Conditions | Yield |
---|---|
With lead acetate; acetic anhydride In tetrahydrofuran for 16h; Heating; | A 63% B 1.9% |
With lead acetate; acetic anhydride In tetrahydrofuran |
Conditions | Yield |
---|---|
Stage #1: Acetol acetate; cyclohexylmethylamine In neat (no solvent) at 20℃; for 0.25h; Stage #2: With phenylphosphonate In neat (no solvent) at 20℃; for 0.25h; Stage #3: Dimethyl phosphite In neat (no solvent) at 50℃; for 1h; | 62% |
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