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Cas:99-94-5
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inquiryProduct Description: Product Name p-Toluic acid CAS No. 99-94-5 Appearance White powder Assay ≥99% Capacity 3000mt/year Min.packing 100gram Appl
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Product description: product name p-toluic acid cas no. 99-94-5 appearance white powder assay ≥99% capacity 3000mt/year min.packing 100gram application ph
Items Standard Result Assay (Ursolic acid) 98%min 98.22% -----------------------------------------------------------------------------------------------------------
Cas:99-94-5
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inquiry1.5-Methylanthranilic acid 2.2941-78-8 3.assay no less than 98.5% 4.Competitive price 5. Usually have it in stock Appearance:white powder Storage:Warehouse ventilation, away from open flame, high temperature, and antioxidant Package:25kg/ba
p-Toluic acid Molecular Formula:: C8H8O2 Molecular Weight:: 136.15 Structural formula: EINECS NO: 204-284-9 Boiling Point: 274~275°C
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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Product Name: p-Toluic acid Synonyms: p-Tolylcarboxylic acid;4-Toluic acid ,99%;4-Carboxytoluene, p-Toluic acid;p-Toluic acid, 98% 100GR;p-carboxytoluene;p-toluic;p-Toluic acid ,99%;p-Toluic acid,4-Methylbenzoic acid CAS: 99-94-5 MF: C8H8O2 MW:
Cas:99-94-5
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inquiryEnglish Name: p-Toluic acid CAS: 99-94-5 Molecular formula: C8H8O2 Molecular weight: 1
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Cas:99-94-5
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inquiryProduct Name: p-Toluic acid CAS: 99-94-5 MF: C8H8O2 MW: 136.15 EINECS: 202-803-3 Mol File: 99-94-5.mol p-Toluic acid Structure p-Toluic acid Chemical Properties Melting point 177-180 °C (lit.) Boiling point 274-275 &de
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inquiryp-Toluic acid CAS:99-94-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
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Cas:99-94-5
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inquiryConditions | Yield |
---|---|
With oxygen; potassium hydroxide In methanol; water at 50℃; under 760.051 Torr; for 4h; | 100% |
With oxygen; potassium hydroxide In toluene at 100℃; under 760.051 Torr; for 12h; | 99% |
With periodic acid; pyridinium chlorochromate In acetonitrile | 98% |
Conditions | Yield |
---|---|
With phosphate-buffered silica gel supported KMnO4 In cyclohexane at 65℃; | 100% |
With periodic acid; tripropylammonium fluorochromate (VI) In acetonitrile at 0℃; for 1.5h; | 100% |
With [Cu2C6H4(CHNCH2CH2N(CH2C5H4N)2)2](2+)*2ClO4(1-)=C36H38Cu2N8(ClO4)2; oxygen In acetone at -90.16℃; | 100% |
methanol
1-pyrenylmethyl p-toluate
A
methyl 1-pyrenylmethyl ether
B
p-Toluic acid
Conditions | Yield |
---|---|
for 0.5h; Irradiation; | A 95% B 100% |
for 0.5h; Product distribution; Irradiation; recovery of carboxylic acids from their 1-pyrenylmethyl esters; | A 95% B 100% |
for 2h; Quantum yield; Irradiation; | A n/a B 80% |
Conditions | Yield |
---|---|
With potassium carbonate; palladium diacetate In water; N,N-dimethyl-formamide at 25℃; under 760 Torr; for 4h; | 100% |
With potassium hydroxide; amphiphilic resin-supported phosphine-palladium; water at 25℃; under 760 Torr; for 12h; Product distribution; Further Variations:; Reagents; hydroxycarbonylation; | 100% |
With dichloro bis(acetonitrile) palladium(II); sodium dodecyl-sulfate; potassium carbonate In water; toluene; butan-1-ol at 50℃; under 760 Torr; for 4h; | 92% |
p-Toluic acid
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran Product distribution; | 100% |
p-methylbenzyltri-n-butyl-stannane
p-Toluic acid
Conditions | Yield |
---|---|
With C2H2Cl2F3O2V; oxygen In tert-butyl alcohol at 50℃; for 36h; | 100% |
p-methylbenzaldehyde oxime
p-Toluic acid
Conditions | Yield |
---|---|
With poly(diselanediyl-1,2-phenylene); dihydrogen peroxide In tetrahydrofuran for 42h; Heating; | 100% |
With [hydroxy(tosyloxy)iodo]benzene; water In dimethyl sulfoxide at 20℃; for 24h; | 82% |
Conditions | Yield |
---|---|
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In 1,4-dioxane for 2h; Heating; | 100% |
p-Toluic acid
Conditions | Yield |
---|---|
With sodium hydroxide In water at 85℃; for 12h; | 100% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; water at 20℃; for 10h; Inert atmosphere; | 99% |
With N-hydroxy-tetrahydrophthalimide; oxygen; nitric acid at 50℃; under 750.075 - 1500.15 Torr; for 25h; Autoclave; Green chemistry; | 91.16% |
With MoO(O2)(8-quinolinolate)2; dihydrogen peroxide In acetonitrile for 6h; Oxidation; Heating; | 88% |
Conditions | Yield |
---|---|
With oxygen; copper(II) nitrate In acetonitrile at 120℃; under 4500.45 Torr; for 10h; | 99% |
With copper(II) nitrate trihydrate; oxygen In acetonitrile at 120℃; under 4500.45 Torr; for 10h; Autoclave; | 97% |
With sodium hydroxide; sodium bromite; sodium bromide In water for 6h; Ambient temperature; | 96% |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 100℃; under 2250.23 Torr; for 3h; Catalytic behavior; Inert atmosphere; | 99% |
With W-7 Raney-Nickel In ethanol for 5h; Heating; | 89% |
4,4'-dimethylbenzaldazine
p-Toluic acid
Conditions | Yield |
---|---|
With poly(diselanediyl-1,2-phenylene); dihydrogen peroxide In tetrahydrofuran for 60h; Heating; | 99% |
With [bis(acetoxy)iodo]benzene In tetrahydrofuran at 20℃; for 4h; Green chemistry; | 72% |
carbon dioxide
5,5-dimethyl-2-(4-methylphenyl)-1,3,2-dioxaborinane
p-Toluic acid
Conditions | Yield |
---|---|
Stage #1: carbon dioxide; 5,5-dimethyl-2-(4-methylphenyl)-1,3,2-dioxaborinane With [Ni(N,N'-bis[2,6-bis(diphenylmethyl)-4-methylphenyl]imidazole-2-ylidene)(allyl)Cl]; potassium tert-butylate In toluene at 100℃; under 760.051 Torr; for 15h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride In water; ethyl acetate; toluene at 20℃; | 99% |
Stage #1: carbon dioxide; 5,5-dimethyl-2-(4-methylphenyl)-1,3,2-dioxaborinane With potassium tert-butylate; silver(I) acetate; triphenylphosphine In tetrahydrofuran at 70℃; under 15201 Torr; for 16h; Inert atmosphere; Autoclave; Stage #2: With hydrogenchloride In tetrahydrofuran; water Inert atmosphere; | 83% |
1,2-di-p-tolylethane-1,2-diol
p-Toluic acid
Conditions | Yield |
---|---|
With oxygen; sodium methylate; silver trifluoromethanesulfonate In tetrahydrofuran; methanol at 37℃; under 760.051 Torr; for 12h; Sealed tube; | 99% |
Stage #1: 1,2-di-p-tolylethane-1,2-diol With 2,3,4,5,6-pentamethyliodobenzene; oxygen; isobutyraldehyde In 1,2-dichloro-ethane under 760.051 Torr; for 24h; Stage #2: With sodium chlorite; 2-methyl-but-2-ene In aq. phosphate buffer; 1,2-dichloro-ethane; tert-butyl alcohol at 25℃; for 14h; | 80% |
With oxygen In dichloromethane at 20℃; under 760.051 Torr; for 12h; Irradiation; | 78% |
Stage #1: 1,2-di-p-tolylethane-1,2-diol With oxygen; sodium t-butanolate In tetrahydrofuran at 20℃; under 760.051 Torr; for 5h; Stage #2: With hydrogenchloride In tetrahydrofuran; water pH=1; chemoselective reaction; | 60% |
para-xylene
A
terephthalic acid
B
4-methyl-benzaldehyde
C
4-Carboxybenzaldehyde
D
p-Toluic acid
Conditions | Yield |
---|---|
With hydrogen bromide; oxygen; acetic acid; cobalt(II) acetate; manganese(II) acetate In water at 190℃; under 16501.7 Torr; for 1h; Product distribution / selectivity; | A 98.1% B 0.2% C 0.4% D 0.4% |
With oxygen; acetic acid; palladium diacetate; antimony(III) acetate In water at 182 - 195℃; under 16501.7 - 20929.4 Torr; for 1 - 1.5h; Product distribution / selectivity; | A 50.3% B 7.2% C 6.4% D 6.2% |
With hydrogen bromide; oxygen; acetic acid; zirconium oxyacetate; cobalt(II) acetate In water at 190℃; under 16501.7 Torr; for 1h; Product distribution / selectivity; | A 4.9% B 3% C 1.9% D 36.9% |
Conditions | Yield |
---|---|
With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In N,N-dimethyl-formamide at 80℃; for 10h; Inert atmosphere; Sealed tube; | 98% |
With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In N,N-dimethyl-formamide at 100℃; for 20h; Inert atmosphere; Sealed tube; | 82% |
Conditions | Yield |
---|---|
With iron(III) sulfate; water In toluene at 110℃; for 1.5h; Ionic liquid; | 97% |
With iodine; aluminium In acetonitrile at 80℃; for 18h; | 96% |
With potassium hydroxide In methanol at 35℃; for 0.5h; | 90% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; dicobalt octacarbonyl In sodium hydroxide; benzene at 65℃; for 1h; Irradiation; | 97% |
With sodium hydroxide; tetrabutylammomium bromide; dicobalt octacarbonyl In water; benzene at 65℃; under 760 Torr; for 1.5h; Irradiation; | 97% |
With palladium diacetate; caesium carbonate; 1,2-bis[di(t-butyl)phosphinomethyl]benzene In water; N,N-dimethyl-formamide at 80℃; under 2068.65 Torr; Inert atmosphere; | 77% |
p-Toluic acid
Conditions | Yield |
---|---|
With Montmorillonite K-10 clay; methoxybenzene for 0.333333h; Dealkylation; Microwave irradiation; | 97% |
With methoxybenzene In toluene for 15h; Heating; | 10% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; methyltrioxorhenium(VII); magnesium sulfate In acetonitrile for 3h; Heating; | 97% |
With sodium hypochlorite In acetonitrile at 20℃; for 5h; | 85% |
With diphenyl diselenide; dihydrogen peroxide In water; acetonitrile at 20℃; for 24h; | 85% |
With graphitic carbon nitride; oxygen; acetic acid In water; acetonitrile at 100℃; under 2250.23 Torr; for 16h; Autoclave; Irradiation; Green chemistry; | 69 %Chromat. |
1-(4-methoxyphenyl)-2-(4-methylphenyl)ethanone
A
p-Toluic acid
B
4-methoxybenzoic acid
Conditions | Yield |
---|---|
With oxygen; potassium hydroxide at 20℃; Schlenk technique; chemoselective reaction; | A 93% B 97% |
Conditions | Yield |
---|---|
With 5% active carbon-supported ruthenium; water; oxygen; calcium oxide at 100℃; for 24h; Overall yield = 56.7 mg; | A 80% B 97% |
p-Toluic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water at 95℃; for 7h; Reagent/catalyst; | 97% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; nitric acid at 110℃; under 760.051 Torr; for 6h; Ionic liquid; | A 96% B 3% |
Stage #1: para-xylene With N-hydroxyphthalimide; cobalt(II) phthalocyanine; μ-oxo[manganese(III) tetraphenylporphine]2; oxygen at 120℃; under 3750.38 Torr; Stage #2: With N-hydroxyphthalimide; cobalt(II) phthalocyanine; μ-oxo[manganese(III) tetraphenylporphine]2; oxygen; acetic acid at 232℃; under 16501.7 Torr; for 1.5h; Temperature; Pressure; Reagent/catalyst; | A 90% B 9.7% |
With chromium(VI) oxide; periodic acid In acetonitrile at 20℃; for 1h; | A 6% B 86% |
Conditions | Yield |
---|---|
With sodium hydroxide In water; tert-butyl alcohol at 70℃; Ni-anode, 16 mA/cm2; | 96% |
With 4 Angstroem MS; methyl tri-n-octyl ammonium hydrogen sulfate; sodium tungstate at 90℃; for 18h; | 68% |
p-tolualdehyde p-toluenesulfonylhydrazone
p-Toluic acid
Conditions | Yield |
---|---|
With poly(diselanediyl-1,2-phenylene); dihydrogen peroxide In tetrahydrofuran for 18h; Heating; | 96% |
tert-butyl 4-methylbenzoate
p-Toluic acid
Conditions | Yield |
---|---|
With aluminium(III) iodide In acetonitrile at 80℃; for 18h; | 96% |
With 1,1,3,3-Tetramethyldisiloxane; pyrographite; palladium dichloride In 1,2-dimethoxyethane at 25 - 40℃; for 6h; | 95% |
With toluene-4-sulfonic acid for 0.0666667h; microwave irradiation; | 93% |
With (μ3,η2,η3,η5-acenaphthylene)Ru3(CO)7; Dimethylphenylsilane In 1,2-dimethoxyethane at 40℃; for 7h; Inert atmosphere; | 93% |
With high-silica Hβ-75 zeolite In water at 130℃; for 24h; Reagent/catalyst; | 88% |
methyl 3-(4-methylphenyl)-3-oxopropanedithioate
p-Toluic acid
Conditions | Yield |
---|---|
With sodium hydroxide In water at 100℃; for 10h; Reflux; chemoselective reaction; | 96% |
N-methoxy-4-methylbenzamide
p-Toluic acid
Conditions | Yield |
---|---|
With tert.-butylnitrite; water at 29℃; for 0.583333h; | 96% |
Conditions | Yield |
---|---|
With boron trifluoride at 65℃; for 0.333333h; | 100% |
With sulfuric acid for 4h; Reflux; | 100% |
With sulfuric acid Fischer-Speier esterification method; Reflux; | 100% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane for 6h; Reflux; | 100% |
With sodium bromate; sodium hydrogensulfite In water; ethyl acetate | 90% |
With dihydrogen peroxide; bromine In dichloromethane; water for 4h; Reflux; | 87% |
p-Toluic acid
4-methyl-3-sulfobenzoic acid
Conditions | Yield |
---|---|
With chlorosulfonic acid at 90℃; for 4h; | 100% |
With sulfuric acid at 160 - 170℃; for 4h; | 71% |
With sulfuric acid at 150 - 160℃; | |
With sulfuric acid at 150℃; | |
With sulfur trioxide |
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 2h; Reflux; | 100% |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 35℃; for 1h; | 100% |
Stage #1: p-Toluic acid With N,N-dimethyl-formamide In dichloromethane at 0℃; for 0.0833333h; Stage #2: With oxalyl dichloride In dichloromethane at 20℃; for 12h; | 100% |
p-Toluic acid
2,4,6-trimethylaniline
N-(2,4,6-trimethylphenyl)-4-methylbenzamide
Conditions | Yield |
---|---|
With diphosphorus tetraiodide In tetrachloromethane; dichloromethane Heating; | 100% |
2,2'-dimethoxy-1,1'-binaphthyl
p-Toluic acid
Conditions | Yield |
---|---|
With methanesulfonic acid; phosphorus pentoxide at 60℃; for 24h; Friedel-Crafts acylation; | 100% |
p-Toluic acid
(2S)-2-[(1,1-dimethylethoxycarbonyl)amino]-3-[(4-methylbenzoyl)amino]propionic acid benzyl ester
Conditions | Yield |
---|---|
Stage #1: 3-amino-(2S)-[(1,1-dimethylethoxycarbonyl)amino]-propionic acid benzyl ester With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In DMF (N,N-dimethyl-formamide) at 20℃; for 0.166667h; Stage #2: p-Toluic acid With 4-methyl-morpholine In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 3h; | 100% |
Stage #1: 3-amino-(2S)-[(1,1-dimethylethoxycarbonyl)amino]-propionic acid benzyl ester With N,N,N',N'-tetramethyl-O-(benzotriazol-1-yl)uronium tetrafluoroborate In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: p-Toluic acid With 4-methyl-morpholine In N,N-dimethyl-formamide at 0 - 20℃; for 3h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 5h; | |
With N'',N'''''-1,8-naphthalenediyl bis[N,N,N',N'-tetramethyl]guanidine In N,N-dimethyl-formamide at 20℃; Kinetics; | |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 10h; Inert atmosphere; Sealed tube; |
Conditions | Yield |
---|---|
With Candida antarctica lipase B immobilised in a macroporous DVB crosslinked polymer (Novozym 435) In cyclohexane at 80℃; for 24h; Enzymatic reaction; | 100% |
With 25 wtpercent H3PO4/ZrO2-TiO2 at 130℃; for 1.75h; Neat (no solvent); chemoselective reaction; | 80% |
Conditions | Yield |
---|---|
Stage #1: p-Toluic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate at 20℃; for 0.166667h; Stage #2: 4-benzylpyperidine at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With water In ethanol at 0 - 20℃; for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
With ammonium acetate; water; hydrogen bromide; oxygen; manganese(II) acetate; cobalt(II) diacetate tetrahydrate; 1-n-butyl-3-methylimidazolim bromide; acetic acid; 3-butyl-1-methylimidazolium acetate at 215℃; under 30753.1 Torr; for 3h; Inert atmosphere; | 99.1% |
With ammonium acetate; water; hydrogen bromide; oxygen; manganese(II) acetate; cobalt(II) diacetate tetrahydrate; 1-n-butyl-3-methylimidazolim bromide; acetic acid; 3-butyl-1-methylimidazolium acetate at 215℃; under 30753.1 Torr; for 3h; Inert atmosphere; | 99.1% |
With oxovanadium(IV) sulfate; hydrogen bromide; oxygen; acetic acid In water at 100℃; under 750.075 Torr; for 20h; | 97% |
Conditions | Yield |
---|---|
With borane-ammonia complex In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Reflux; | 99% |
With Bromotrichloromethane; 4-(diphenylphosphino)-benzyltrimethylammonium bromide; triethylamine In tetrahydrofuran at 60℃; for 6h; Inert atmosphere; | 98% |
Stage #1: p-Toluic acid With N-chlorobenzotriazole; triphenylphosphine In dichloromethane for 0.25h; Stage #2: benzylamine With triethylamine In dichloromethane at 20℃; for 0.75h; | 95% |
Conditions | Yield |
---|---|
With triphenylphosphine In tetrahydrofuran at 65℃; for 16h; Product distribution; Further Variations:; Solvents; Mitsunobu reaction; | 99% |
With trifluoromethylsulfonic anhydride; triethylamine; Triphenylphosphine oxide In 1,2-dichloro-ethane at 25℃; for 0.25h; | 88% |
Conditions | Yield |
---|---|
With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 5h; | 99% |
Stage #1: p-Toluic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate at 20℃; for 0.166667h; Stage #2: aniline at 20℃; for 1h; | 97% |
With (3-{[(cyclohexylimino)methylidene]amino}propyl)oxy linked polystyrene resin In dichloromethane; N,N-dimethyl-formamide for 0.0833333h; Flow reactor; | 96% |
p-Toluic acid
<α,α-2H2>-4-methylbenzyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium deuteride In tetrahydrofuran for 24h; Heating; | 99% |
With lithium aluminium deuteride In diethyl ether at 20℃; for 3h; | 90% |
Conditions | Yield |
---|---|
Stage #1: p-Toluic acid With sulfuric acid In ethanol for 6h; Reflux; Stage #2: With hydrazine hydrate; sodium hydrogencarbonate; acetic acid Reflux; | 99% |
With acetic acid; acetic acid hydrazide for 0.1h; Microwave irradiation; | 85% |
With hydrazine hydrate for 0.0472222h; Microwave irradiation; | 85% |
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