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inquiryItems Standard Result Appearance Off-White Crystal Conforms Purity Of HPLC 99.0% up
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name 4-Formylbenzoic acid CAS number 619-66-9 Assay ≥99% Appearance White powder Capacity 500mt/year Application Pharmaceutical/pesticides/fluor
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inquiry4-Formylbenzoic acid Manufacturer Factory CAS 619-66-9 4-Formylbenzoic acid Manufacturer High quality Best price In stock factory CAS 619-66-9 4-Formylbenzoic acid COA TDS price MSDS highly quality and immedaite delivery 4-Formylbenzoic
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inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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inquiryChemical Name 4-Carboxybenzaldehyde Synonyms CAS No. 619-66-9 EINECS No. 210-607-4 Molecular formula C8H6O3
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inquiry4-Formylbenzoic acid CAS:619-66-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryp-carboxybenzaldehydeAppearance:powder Storage:store in a cool dry place and keep away from strong Package:according to customers' requirements Application:in research Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or C
moderate price & quick delivery Appearance:Yellowish fine crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:A metabolite of
Product name: 4-Carboxybenzaldehyde CAS No.:619-66-9 Molecule Formula:C8H5O3 Molecule Weight:149.12 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TE
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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4-Formylbenzoic acid Chemical Properties Melting point 247 °C(lit.) Boiling point 231.65°C (rough estimate) density 1.2645 (rough estimate) refractive index 1.4500 (estimate) storage temp. -20 C Freezer pka 3.77(at 25℃)
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inquiryConditions | Yield |
---|---|
With copper acetylacetonate; oxygen; sodium hydroxide; 1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene In water at 50℃; under 760.051 Torr; for 12h; Sealed tube; | 99% |
With 4H3N*4H(1+)*CuMo6O18(OH)6(4-); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 12h; | 99% |
With carbon dioxide; potassium carbonate; 1,3-bis(mesityl)imidazolium chloride In dimethyl sulfoxide at 20℃; under 760.051 Torr; for 72h; | 95% |
4-formyl-N,N-bis(pyridin-2-ylmethyl)benzamide
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-formyl-N,N-bis(pyridin-2-ylmethyl)benzamide With methanol; copper(II) bis(trifluoromethanesulfonate) at 20℃; for 16h; Stage #2: With barium(II) hydroxide In methanol; water at 20℃; Stage #3: With hydrogenchloride In methanol; water | 99% |
Conditions | Yield |
---|---|
With air; hydrogen bromide; acetic acid; cobalt(II) acetate; manganese(II) acetate at 180℃; under 25745 Torr; for 0.166667h; | A 98.3% B 1.4% |
With 9,10-Dibromoanthracene; acetic acid; cobalt(II) acetate; cerium(III) acetate at 165℃; under 25745 Torr; for 0.166667h; | A 98.2% B 1.1% |
With 9,10-Dibromoanthracene; acetic acid; cobalt(II) acetate; manganese(II) acetate at 170℃; under 25745 Torr; for 0.166667h; | A 97.5% B 1.9% |
para-xylene
A
terephthalic acid
B
4-methyl-benzaldehyde
C
4-Carboxybenzaldehyde
D
p-Toluic acid
Conditions | Yield |
---|---|
With hydrogen bromide; oxygen; acetic acid; cobalt(II) acetate; manganese(II) acetate In water at 190℃; under 16501.7 Torr; for 1h; Product distribution / selectivity; | A 98.1% B 0.2% C 0.4% D 0.4% |
With oxygen; acetic acid; palladium diacetate; antimony(III) acetate In water at 182 - 195℃; under 16501.7 - 20929.4 Torr; for 1 - 1.5h; Product distribution / selectivity; | A 50.3% B 7.2% C 6.4% D 6.2% |
With hydrogen bromide; oxygen; acetic acid; zirconium oxyacetate; cobalt(II) acetate In water at 190℃; under 16501.7 Torr; for 1h; Product distribution / selectivity; | A 4.9% B 3% C 1.9% D 36.9% |
Conditions | Yield |
---|---|
With C13H26B(1-)*K(1+) In tetrahydrofuran for 24h; Ambient temperature; | 98% |
carbon dioxide
5,5-dimethyl-2-(4-formylphenyl)-1,3,2-dioxaborinane
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With potassium tert-butylate; copper(l) chloride; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride In tetrahydrofuran at 70℃; under 760.051 Torr; for 24h; | 97% |
Stage #1: carbon dioxide; 5,5-dimethyl-2-(4-formylphenyl)-1,3,2-dioxaborinane With potassium tert-butylate; silver(I) acetate; triphenylphosphine In tetrahydrofuran at 70℃; under 15201 Torr; for 16h; Inert atmosphere; Autoclave; Stage #2: With hydrogenchloride In tetrahydrofuran; water Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
With [PhCOPd(PtBu3)I]; dtbpf In diethylene glycol dimethyl ether at 120℃; for 18h; Inert atmosphere; | 97% |
diphenylmethylsilanecarboxylic acid
p-(iodophenyl)carboxaldehyde
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With potassium trimethylsilonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; bis(dibenzylideneacetone)-palladium(0) In toluene at 40℃; for 0.333333h; | 97% |
Conditions | Yield |
---|---|
Stage #1: carbon dioxide With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate In 1,4-dioxane at 65℃; for 0.333333h; Schlenk technique; Stage #2: 4-bromo-benzaldehyde With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane; toluene at 100℃; for 2h; Schlenk technique; Sealed tube; | 97% |
Stage #1: carbon dioxide With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate In 1,4-dioxane at 60℃; for 0.416667h; Schlenk technique; Stage #2: 4-bromo-benzaldehyde With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane; toluene at 100℃; for 6h; Schlenk technique; | 66% |
acetic acid
p-Toluic acid
A
terephthalic acid
B
3-hydroxymethyl-benzoic acid
C
p-acetoxymethyl benzoic acid
D
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; air; cobalt(II) acetate; manganese(II) acetate at 150℃; under 22800 Torr; for 3h; | A 95% B n/a C n/a D n/a |
Conditions | Yield |
---|---|
With LACTIC ACID; dihydrogen peroxide at 30℃; for 7h; | 95% |
With Burgess Reagent; dimethyl sulfoxide at 20℃; for 0.0833333h; Schlenk technique; Inert atmosphere; | 92% |
With ammonium hydroxide; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In water for 24h; Reflux; Green chemistry; | 90% |
Conditions | Yield |
---|---|
Stage #1: carbon dioxide With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate In 1,4-dioxane at 65℃; for 0.333333h; Schlenk technique; Stage #2: 4-chlorobenzaldehyde With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane; toluene at 100℃; for 5h; Schlenk technique; Sealed tube; | 93% |
Stage #1: carbon dioxide With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate In 1,4-dioxane at 60℃; for 0.416667h; Schlenk technique; Stage #2: 4-chlorobenzaldehyde With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane; toluene at 100℃; for 16h; Schlenk technique; | 41% |
Conditions | Yield |
---|---|
With water; potassium hydroxide In methanol at 20℃; for 18h; | 92% |
Stage #1: methyl 4-formylbenzoate With water; sodium hydroxide In methanol Stage #2: In water Acidic conditions; | 80% |
With sulfuric acid | |
With lithium hydroxide In tetrahydrofuran; methanol | |
With water; sodium hydroxide In methanol at 20℃; for 4h; |
p-Trimethylsiloxymethylbenzoesaeure
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With aluminium trichloride; tetramethylammonium chlorochromate In acetonitrile for 0.916667h; Heating; | 90% |
4-<(tetrahydropyran-2-yloxy)methyl>benzoic acid
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With aluminium trichloride; tetramethylammonium chlorochromate In acetonitrile for 0.833333h; Heating; | 90% |
dicobalt octacarbonyl
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane; water at 20℃; for 16h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 90% |
benzyl 4-formylbenzoate
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 25℃; for 3h; Inert atmosphere; | 90% |
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 50℃; for 5h; Inert atmosphere; | 90% |
para-xylene
A
terephthalic acid
B
4-Carboxybenzaldehyde
C
p-Toluic acid
Conditions | Yield |
---|---|
With carbon dioxide; oxygen; 1-hydroxy-pyrrolidine-2,5-dione; cobalt(II) acetate In acetic acid at 60℃; under 44269 Torr; for 1h; Product distribution / selectivity; | A 89.2% B n/a C n/a |
With oxygen; 1-hydroxy-pyrrolidine-2,5-dione; cobalt(II) acetate In acetic acid at 25 - 125℃; under 12049.9 - 44475.9 Torr; for 1 - 6h; Product distribution / selectivity; | A 79.77% B 0.67% C 0.3% |
With carbon dioxide; oxygen; 1-hydroxy-pyrrolidine-2,5-dione; cobalt acetylacetonate In acetic acid at 60℃; under 49337.2 Torr; for 1h; Product distribution / selectivity; | A 74% B n/a C n/a |
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With poly(amidoamine) dendrimer functionalized sulfonic acid In methanol at 20℃; for 0.25h; | 89% |
4-(Methoxymethyl)benzoic acid
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With nitric acid In dichloromethane at 20℃; for 1h; | 88% |
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With diethoxymethylane; ferric benzoylacetonate In i-Amyl alcohol at 100℃; for 24h; | 85% |
Conditions | Yield |
---|---|
With 1,2-bis(2,4,8,10-tetra-tert-butyl-5,7-dioxa-6-phosphadibenzo[a,c]cyclohepten-6-yloxy)ethane; methylphenylsilane; copper(l) cyanide; 2,2-dimethylpropanoic anhydride In dimethyl sulfoxide at 80℃; for 20h; Schlenk technique; Inert atmosphere; | 84% |
para-xylene
A
terephthalic acid
B
3-hydroxymethyl-benzoic acid
C
4-Carboxybenzaldehyde
D
p-Toluic acid
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; manganese(II) acetate; cobalt(II) acetate In acetic acid at 100℃; under 760 Torr; for 14h; Kinetics; Product distribution; Further Variations:; Catalysts; Reagents; Solvents; Temperatures; ratio; | A 82% B n/a C n/a D 4% |
dicobalt octacarbonyl
4-(trifluormethanesulfonyloxy)benzaldehyde
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane; water at 20℃; for 16h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 81% |
4-(hydroxylmethyl)benzaldehyde
A
terephthalic acid
B
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride; oxygen In 1,2-dichloro-ethane at 25℃; for 48h; Schlenk technique; | A 6 %Spectr. B 80% |
Multi-step reaction with 2 steps 1: recombinant 5-hydroxymethylfurfural oxidase / aq. phosphate buffer / 24 h / 25 °C / pH 8 / Enzymatic reaction 2: recombinant 5-hydroxymethylfurfural oxidase / aq. phosphate buffer / 4 h / 25 °C / pH 7 / Enzymatic reaction View Scheme | |
Multi-step reaction with 2 steps 1: recombinant 5-hydroxymethylfurfural oxidase / aq. phosphate buffer / 4 h / 25 °C / pH 8 / Enzymatic reaction 2: recombinant 5-hydroxymethylfurfural oxidase / aq. phosphate buffer / 4 h / 25 °C / pH 7 / Enzymatic reaction View Scheme | |
Multi-step reaction with 2 steps 1: recombinant 5-hydroxymethylfurfural oxidase / aq. phosphate buffer / 4 h / 25 °C / pH 8 / Enzymatic reaction 2: recombinant 5-hydroxymethylfurfural oxidase / aq. phosphate buffer / 4 h / 25 °C / pH 7 / Enzymatic reaction View Scheme |
Conditions | Yield |
---|---|
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; for 2h; Sealed tube; | 77% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; Inert atmosphere; Sealed tube; | 75% |
Conditions | Yield |
---|---|
With formic acid; 1,3-bis-(diphenylphosphino)propane; nickel(II) acetate tetrahydrate; acetic anhydride In tetrahydrofuran at 100℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube; | 76% |
4-mercaptomethylbenzoic acid
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; tetrakis(pyridine)silver(II) peroxodisulfate; oxygen In N,N-dimethyl-formamide at 23℃; under 760.051 Torr; Irradiation; | 74% |
Conditions | Yield |
---|---|
With copper(I) 2-hydroxy-3-methylbenzoate; oxygen; ascorbic acid In N,N-dimethyl acetamide at 40℃; for 2h; chemoselective reaction; | 67% |
With riboflavin tetraacetate In dimethylsulfoxide-d6; water-d2 for 0.166667h; Irradiation; In air; |
4-Carboxybenzaldehyde
4-formylbenzoyl chloride
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In tetrahydrofuran at 20℃; | 100% |
With oxalyl dichloride In tetrahydrofuran; N,N-dimethyl-formamide at 0 - 20℃; for 2h; | 100% |
With thionyl chloride In toluene for 1.5h; Heating; | 97.9% |
Conditions | Yield |
---|---|
In 1,4-dioxane; ethanol | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-Carboxybenzaldehyde With alkali metal carbonate In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere; | 100% |
With caesium carbonate In ethyl acetate; N,N-dimethyl-formamide | 97% |
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 3h; | 97% |
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
4-Carboxybenzaldehyde
N-butylamine
Conditions | Yield |
---|---|
Multistep reaction; | 100% |
4-Carboxybenzaldehyde
4-formylphenyl isocyanate
Conditions | Yield |
---|---|
With diphenylphosphoranyl azide; triethylamine In dichloromethane for 6h; Heating; | 100% |
With diphenyl phosphoryl azide; triethylamine In dichloromethane for 6h; Reflux; | 100% |
Multi-step reaction with 3 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 0 °C 2: sodium azide / water; acetone / 1 h / 0 °C 3: toluene / 1 h / 100 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / tetrahydrofuran / 2 h / Inert atmosphere 2: sodium azide / water / 1 h 3: toluene / 2 h / Inert atmosphere; Reflux View Scheme |
4-Carboxybenzaldehyde
allylgallium dichloride
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane at 0℃; for 0.8h; | 100% |
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 100% |
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
With perchloric acid In 1,4-dioxane at 20℃; | 100% |
1-hydroxy-pyrrolidine-2,5-dione
4-Carboxybenzaldehyde
succinimidyl 4-formylbenzoate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 25℃; for 14h; | 100% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 95% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 95% |
tert-butyl diethylphosphonoacetate
4-Carboxybenzaldehyde
(E)-4-(2-tert-Butoxycarbonylvinyl)benzoic acid
Conditions | Yield |
---|---|
With sodium hydride In 1,2-dimethoxyethane at 0 - 20℃; for 4h; | 100% |
4-Carboxybenzaldehyde
methyl (E)-4-carboxyl cinnamate
Conditions | Yield |
---|---|
Stage #1: trimethyl phosphonoacetate; 4-Carboxybenzaldehyde With potassium carbonate In water at 0 - 20℃; for 1.5h; Stage #2: In water pH=1; Acidic aqueous solution; | 100% |
With potassium carbonate In water at 0 - 20℃; pH=Ca. 2; | 95% |
4-chloro-aniline
4-Carboxybenzaldehyde
4-[(4-chlorophenylamino)methyl]benzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-chloro-aniline; 4-Carboxybenzaldehyde In methanol for 0.5h; Heating / reflux; Stage #2: With sodium cyanoborohydride; acetic acid In methanol at 20 - 35℃; for 0.5h; Stage #3: With water In methanol at 20℃; for 16h; | 100% |
Conditions | Yield |
---|---|
In methanol | 100% |
In dichloromethane | |
In dichloromethane | |
Multi-step reaction with 2 steps 1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C 2: copper(II) bis(trifluoromethanesulfonate) / 16 h / 20 °C View Scheme |
methyl {4-(6-chloro-3'-ethyl-2-biphenylyl)-4-hydroxy-4-[(3R)-3-piperidinyl]butyl}carbamate
4-Carboxybenzaldehyde
methyl (4-(6-chloro-3'-ethyl-2-biphenylyl)-4-{(3R)-1-[(4-formylphenyl)carbonyl]-3-piperidinyl}-4-hydroxybutyl)carbamate
Conditions | Yield |
---|---|
Stage #1: 4-Carboxybenzaldehyde With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 0.166667h; Stage #2: methyl {4-(6-chloro-3'-ethyl-2-biphenylyl)-4-hydroxy-4-[(3R)-3-piperidinyl]butyl}carbamate In dichloromethane for 0.583333h; | 100% |
6-(tert-butyl)-4-hydrazinothieno[2,3-d]pyrimidine
4-Carboxybenzaldehyde
4-{[(6-tert-butylthieno[2,3-d]pyrimidin-4-yl)hydrazono]methyl}benzoic acid
Conditions | Yield |
---|---|
In benzene for 3h; Reflux; | 100% |
4-Carboxybenzaldehyde
methylamine
4-[(Z)-Methyliminomethyl]-benzoic acid
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
4-Carboxybenzaldehyde
t-butyl 3-N-t-butylaminopropionate
tert-butyl 3-(N-tert-butyl-4-formylbenzamido)propanoate
Conditions | Yield |
---|---|
Stage #1: 4-Carboxybenzaldehyde With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 5.5h; Reflux; Stage #2: t-butyl 3-N-t-butylaminopropionate With triethylamine In dichloromethane at 20℃; | 100% |
3-Methyl-2-thioxo-thiazolidin-4-on
4-Carboxybenzaldehyde
4-[(3-methyl-4-oxo-2-thioxothiazolidin-5-ylidene)methyl]benzoic acid
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid at 180℃; for 0.0833333h; Knoevenagel Condensation; Microwave irradiation; | 100% |
3-(2-phenylethyl)-2-thioxo-1,3-thiazolidin-4-one
4-Carboxybenzaldehyde
4-[(4-oxo-3-phenethyl-2-thioxothiazolidin-5-ylidene)methyl]benzoic acid
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid at 180℃; for 0.0833333h; Knoevenagel Condensation; Microwave irradiation; | 100% |
3-(4-methylbenzyl)-2-thioxothiazolidin-4-one
4-Carboxybenzaldehyde
4-[(3-(4-methylbenzyl)-4-oxo-2-thioxothiazolidin-5-ylidene)methyl]benzoic acid
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid at 180℃; for 0.0833333h; Knoevenagel Condensation; Microwave irradiation; | 100% |
1-(4-fluorophenyl)-2-(2-oxo-1,2-dihydropyridin-4-yl)ethane-1,2-dione
4-Carboxybenzaldehyde
4-(4-(4-fluorophenyl)-5-(2-oxo-1,2-dihydropyridin-4-yl)-1H-imidazol-2-yl)benzoic acid
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid at 180℃; for 0.166667h; | 100% |
2-chloro-4-fluorobenzylamine
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-Carboxybenzaldehyde With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide Stage #2: 2-chloro-4-fluorobenzylamine In N,N-dimethyl-formamide at 20℃; | 100% |
4-Carboxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-Carboxybenzaldehyde With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 0.666667h; Stage #2: β-alanine tert-butyl ester hydrochloride In N,N-dimethyl-formamide at 20℃; for 18h; | 100% |
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0333333h; | 100% |
4-Carboxybenzaldehyde
2,7-bis-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-benzo-[lmn]-[3,8]phenanthroline-1,3,6,8-tetraone
2,7-bis(2-(2-(2-(2-(4-formylphenylcarboxy)ethoxy)ethoxy)ethoxy)ethyl)benzo[lmn]-(3,8)phenanthroline-1,3,6,8-tetraone
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane for 168h; Inert atmosphere; Darkness; | 99.5% |
Conditions | Yield |
---|---|
With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane at 20℃; for 5h; | 99% |
With graphene oxide at 100℃; for 24h; | 90% |
With sulfuric acid for 18h; Heating / reflux; | 83.1% |
4-Carboxybenzaldehyde
malononitrile
(4-carboxybenzylidene)malononitrile
Conditions | Yield |
---|---|
With activated microporous polyurethane material with BET surface area of 312 m2 g-1 In tetrahydrofuran at 50℃; for 14h; Catalytic behavior; Knoevenagel Condensation; | 99% |
With MIL-53(Fe) metal organic framework encapsulated on silica-coated nickel ferrite magnetic nanoparticles In ethanol at 20℃; for 1.16667h; Knoevenagel Condensation; | 97% |
With (propyleneimine) dendrimer-G3 on silica coated magnetite nanohybrid In ethanol at 20℃; for 0.5h; Solvent; Knoevenagel Condensation; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With C55H44O2P4Ru; hydrogen at 80℃; under 38002.6 Torr; for 18h; Glovebox; Autoclave; | 99% |
With C55H44O2P4Ru; hydrogen In tetrahydrofuran at 80℃; under 38002.6 Torr; for 18h; Inert atmosphere; Glovebox; Autoclave; | 99% |
With sodium tetrahydroborate; Dowex1-x8 In tetrahydrofuran at 20℃; for 0.15h; | 96% |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 100℃; under 2250.23 Torr; for 3h; Catalytic behavior; Inert atmosphere; | 99% |
With W-7 Raney-Nickel In ethanol for 5h; Heating; | 89% |
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