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inquiryUnique advantages of 4-Dimethylaminobenzoic acid Cas 619-84-1 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White powder Storage:Cool dry place Package:1kg/foill ba
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inquiryAbout Product Details
Cas:619-84-1
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inquiryProduct Name: 4-Dimethylaminobenzoic acid Synonyms: 4-Diaminomethylbenzoic acid;4-DIMETHYLAMINOBENZOIC ACID, TECH., 90%;4-Dimethylaminobenzoic acid, 98+%;PARA(DIMETHYLAMINO)BENZOICACID;N,N-DIMETHYL-PARA-AMINOBENZOICACID;LR-78;Of diMeth
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inquiry4-Dimethylaminobenzoic acid CAS No.: 619-84-1 Appearance: White to yellowish crystalline powder Formula: C9H11NO2 Exact Mass: 165.08
Cas:619-84-1
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inquiryProduct Name: 4-Dimethylaminobenzoic acid CAS: 619-84-1 MF: C9H11NO2 MW: 165.19 EINECS: 210-615-8 Mol File: 619-84-1.mol 4-Dimethylaminobenzoic acid Structure 4-Dimethylaminobenzoic acid Chemical Properties Melting point 241-2
Cas:619-84-1
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inquirysuperior quality moderate price & quick delivery Appearance:light grey powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:4-(Dimethyl
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryProduct name: 4-Dimethylamino Benzonic Acid CAS No.:619-84-1 Molecule Formula:C9H10NO2 Molecule Weight:164.18 Purity: 95.0% Package: 25kg/drum Description:Grayish crystalline powder Manufacture Standards:Enterprise Standard
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryConditions | Yield |
---|---|
With silica-supported Jones reagent In dichloromethane for 0.035h; | 99.6% |
With oxygen In acetonitrile at 20℃; for 7h; Catalytic behavior; | 96% |
With tert.-butylhydroperoxide; copper(ll) bromide In water; acetonitrile at 20℃; for 22.5h; Inert atmosphere; chemoselective reaction; | 90% |
2,2,2-trichloro-1-[4-(dimethylamino)phenyl]ethan-1-ol
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide In methanol for 10h; | 98% |
Conditions | Yield |
---|---|
With sodium hydroxide for 0.0166667h; microwave irradiation; | 97% |
allyl 4-(dimethylamino)benzoate
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide; mineral oil at 25℃; for 4h; Inert atmosphere; | 97% |
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 60℃; for 3h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With Co4HP2Mo15V3O62; N-(4-sulfonic acid)butyl triethylammonium tetrafluoroborate; dihydrogen peroxide In water at 20℃; for 3h; Green chemistry; | 95% |
With tert.-butylhydroperoxide; copper(ll) bromide In water; acetonitrile at 20℃; for 4.5h; Inert atmosphere; chemoselective reaction; | 92% |
With sodium chlorite In acetonitrile 1.) 10 deg C, 2 h, 2.) RT, 3 h; | 89% |
carbon dioxide
4-bromo-N,N-dimethylaniline
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With C26H30B10Cl2P2Pd In toluene at 50℃; under 760.051 Torr; for 8h; | 90% |
With [2,2]bipyridinyl; lithium chloride; cobalt(II) iodide; zinc In N,N-dimethyl-formamide; acetonitrile at 40℃; under 760.051 Torr; for 14h; Sealed tube; | 61% |
With diethylzinc; palladium diacetate; tert-butyl XPhos In hexanes; N,N-dimethyl acetamide at 40℃; under 7600.51 Torr; Automated synthesizer; | 40% |
Stage #1: 4-bromo-N,N-dimethylaniline With tert.-butyl lithium In tetrahydrofuran; pentane at -78℃; for 0.5h; Stage #2: With [2,2]bipyridinyl; (-)-menthol In tetrahydrofuran; pentane Inert atmosphere; Stage #3: carbon dioxide In tetrahydrofuran; pentane at 20℃; under 5171.62 Torr; for 0.0166667h; Flow reactor; |
carbon dioxide
5,5-dimethyl-2-(4-(N,N-dimethylamino)phenyl)-1,3,2-dioxaborinane
A
methyl 4-(N,N-dimethylamino)benzoate
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With potassium tert-butylate; copper(l) chloride; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride In tetrahydrofuran at 70℃; under 760.051 Torr; for 24h; | A 87% B n/a |
carbon dioxide
5,5-dimethyl-2-(4-(N,N-dimethylamino)phenyl)-1,3,2-dioxaborinane
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
Stage #1: carbon dioxide; 5,5-dimethyl-2-(4-(N,N-dimethylamino)phenyl)-1,3,2-dioxaborinane With [Ni(N,N'-bis[2,6-bis(diphenylmethyl)-4-methylphenyl]imidazole-2-ylidene)(allyl)Cl]; potassium tert-butylate In toluene at 100℃; under 760.051 Torr; for 15h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride In water; ethyl acetate; toluene at 20℃; | 84% |
carbon dioxide
N-methyl-p-aminobenzoic acid
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With phenylsilane In N,N-dimethyl acetamide at 60℃; for 4h; Reagent/catalyst; Sealed tube; | 84% |
tert-butylisonitrile
4-(dimethylamino)benzene-boronic acid
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
Stage #1: tert-butylisonitrile; 4-(dimethylamino)benzene-boronic acid With copper diacetate; palladium diacetate In N,N-dimethyl-formamide at 100℃; for 24h; Molecular sieve; Sealed tube; Stage #2: With water In N,N-dimethyl-formamide Molecular sieve; Sealed tube; | 83% |
carbon dioxide
4-(dimethylamino)benzene-boronic acid
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium methanolate In N,N-dimethyl acetamide at 70℃; for 24h; Schlenk technique; Sealed tube; | 78% |
ethyl p-dimethyaminolbenzoate
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
Stage #1: ethyl p-dimethyaminolbenzoate With iron(III) chloride In tetrachloromethane at 85℃; for 24h; Inert atmosphere; Stage #2: With hydrogenchloride; water In tetrachloromethane Inert atmosphere; | 77% |
With sodium hydroxide In ethanol at 85℃; for 6h; |
Conditions | Yield |
---|---|
With iodine; aluminium In acetonitrile at 80℃; for 18h; | 77% |
4-amino-benzoic acid
carbonic acid dimethyl ester
A
N-methyl-p-aminobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With sodium-exchanged Y-zeolite at 130℃; for 9h; | A 74% B n/a |
carbon dioxide
4-N,N-dimethylaminophenyl magnesium chloride
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
In tetrahydrofuran at 1℃; for 0.0833333h; | 72% |
carbon dioxide
4-dimethylaminophenylmagnesium bromide
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
In tetrahydrofuran at 1℃; for 0.0833333h; | 71% |
Methyl formate
4-chlorobenzonitrile
A
4-formamidobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With potassium hydroxide; (bis(tricyclohexyl)phosphine)palladium(II) dichloride; dodecacarbonyl-triangulo-triruthenium; cetyltrimethylammonim bromide at 160℃; for 10h; | A 58.2% B 7% |
4-Bromobenzoic acid
N,N-dimethyl-formamide
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With potassium carbonate In water at 140℃; for 10h; | 54% |
4-dimethylamino-benzaldehyde
diethyl malonate
A
diethyl p-(N,N'-dimethylamino)-benzylidenemalonate
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With bentonite Actisil FF for 0.25h; Irradiation; | A 48% B 3% |
4-iodobenzoic acid
N,N-dimethyl-formamide
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With potassium carbonate In water at 140℃; for 10h; | 48% |
p-(1,3-dithiolan-2-yl)-N,N-dimethylaniline
A
p-N,N-dimethylaminobenzoic acid
B
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With potassium superoxide; tetraethylammonium bromide In N,N-dimethyl-formamide at 20℃; | A 18% B 44% |
N,N-dimethyl-formamide
para-chlorobenzoic acid
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With potassium carbonate In water at 140℃; for 10h; | 35% |
carbon monoxide
4-(dimethylamino)benzenediazonium tetrafluoroborate
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With water at 100℃; under 795063 Torr; for 2.5h; | 4.63% |
1,4-dioxane
potassium tert-butylate
bis(p-dimethylaminophenyl)methanone
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With water | |
Multi-step reaction with 3 steps 1: triethylamine / diethyl ether 2: hydrogenchloride / water; acetonitrile 3: water; dimethyl sulfoxide / 25 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: magnesium; 1,2-dibromoethane / tetrahydrofuran / 0.5 h / 200 °C / microwave irradiation 2: 72 percent / tetrahydrofuran / 0.08 h / 1 °C View Scheme | |
With carbon dioxide; sodium; benzene |
Conditions | Yield |
---|---|
With n-butyllithium; diethyl ether anschliessend Behandeln mit Kohlendioxid; | |
With sodium; benzene anschliessend Behandeln mit Kohlendioxid; |
2-(4-(dimethylamino)phenyl)-2-oxoacetic acid
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With sulfuric acid at 120℃; |
5-[(5-amino-2-methylbenzoylamino)-methyl]-7H-pyrrolo[2,3-b]pyridine-2-carboxylic acid methyl ester
p-N,N-dimethylaminobenzoic acid
5-{[5-(4-dimethylaminobenzoylamino)-2-methylbenzoylamino]-methyl}-1H-pyrrolo[2,3-b]pyridine-2-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 12h; | 4% |
p-N,N-dimethylaminobenzoic acid
1-(4-aminophenyl)cyclopentane-1-carbonitrile
N-[4-(1-cyano-cyclopentyl)-phenyl]-4-dimethylamino-benzamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate In dichloromethane at 20℃; for 72h; | 5% |
2-hydroxy-3-aminopyridine
p-N,N-dimethylaminobenzoic acid
N,N-dimethyl-4-oxazolo[5,4-b]pyridin-2-yl-aniline
Conditions | Yield |
---|---|
With polystyrene triphenylphosphine; trichloroacetonitrile In acetonitrile at 150℃; for 0.25h; Microwave; | 6.6% |
p-N,N-dimethylaminobenzoic acid
descarboethoxyloratadine
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 4℃; for 0.5h; | 11% |
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
11.5% |
Conditions | Yield |
---|---|
With hydroxylamine In 1-Methylpyrrolidine; 1,4-dioxane; methanol; dichloromethane; water | 12% |
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
Stage #1: p-N,N-dimethylaminobenzoic acid With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole In acetonitrile at 20℃; Stage #2: 2-(N-(4-sulfamoylphenyl)sulfamoyl)ethanamine hydrochloride In water; acetonitrile | 12% |
p-N,N-dimethylaminobenzoic acid
(2R,3R,4R,5R)-2-(aminomethyl)-5-(hydroxymethyl)pyrrolidine-3,4-diol
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 25℃; for 4.5h; | 16% |
p-Anisidinothioformyl-hydrazin
p-N,N-dimethylaminobenzoic acid
5-(4-(dimethylamino)phenyl)-N-(4-methoxyphenyl)-1,3,4-oxadiazol-2-amine
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; | 16% |
n-vinylformamide
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(I) acetate; potassium hydrogencarbonate In benzonitrile at 80℃; for 24h; Schlenk technique; | 16% |
4-(p-chlorophenyl)-3-thiosemicarbazide
p-N,N-dimethylaminobenzoic acid
N-(4-chlorophenyl)-5-(4-(dimethylamino)phenyl)-1,3,4-oxadiazol-2-amine
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; | 19% |
Conditions | Yield |
---|---|
With PPA at 195℃; for 0.25h; | 20% |
p-N,N-dimethylaminobenzoic acid
N1-(4-methoxybenzoyl)-1,2-benzenediamine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 48h; Acylation; | 20% |
p-N,N-dimethylaminobenzoic acid
tetramethylammonium 4-(dimethylamino)benzoate
Conditions | Yield |
---|---|
In methanol | 20% |
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 16h; | 20% |
2-(hydroxymethyl)-3-methylbenzofuran
p-N,N-dimethylaminobenzoic acid
2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 3h; Ambient temperature; | 22% |
Conditions | Yield |
---|---|
With dmap; N'-methyl polystyrene HL; N-cyclohexylcarbodiimide In dichloromethane at 20℃; for 72h; | 22% |
C18H28O5
C18H31NO4
isocyanoacetic acid methyl ester
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
Stage #1: C18H28O5; C18H31NO4; p-N,N-dimethylaminobenzoic acid In methanol at 20℃; for 0.5h; Ugi Condensation; Stage #2: isocyanoacetic acid methyl ester With Ugi Condensation In methanol | 22% |
p-N,N-dimethylaminobenzoic acid
4-(dimethylamino)benzoyl fluoride
Conditions | Yield |
---|---|
With (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane at 0℃; for 0.5h; Schlenk technique; Inert atmosphere; | 22% |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide / dichloromethane / 0.28 h / 0 - 20 °C / Sealed tube 2: triethylamine tris(hydrogen fluoride) / 2 h / 20 °C View Scheme | |
With potassium fluoride; Tetrafluorophthalonitrile In acetonitrile at 80 - 90℃; under 760.051 Torr; for 24h; Temperature; Reagent/catalyst; Glovebox; Inert atmosphere; Sealed tube; | 85 %Spectr. |
With (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane at 20℃; for 3h; Inert atmosphere; |
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water-d2 at 60℃; for 6h; Sealed tube; | 23% |
3-(4-aminomethylphenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-5-ol
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
Stage #1: 3-(4-aminomethylphenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-5-ol; p-N,N-dimethylaminobenzoic acid With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide for 16h; Stage #2: With ammonium chloride In dichloromethane; water; N,N-dimethyl-formamide | 24% |
Conditions | Yield |
---|---|
With tetrachloromethane; triphenylphosphine In dichloromethane at 25℃; for 2.5h; | 28% |
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With sodium borodeuteride; palladium 10% on activated carbon; water-d2 at 150℃; sealed tube; Microwave irradiation; Inert atmosphere; | 29% |
(9H-fluoren-9-yl)methyl (4-((2,3-diaminopyridin-4-yl)oxy)phenyl)carbamate
p-N,N-dimethylaminobenzoic acid
4-(7-(4-aminophenoxy)-3H-imidazo[4,5-b]pyridin-2-yl)-N,N-dimethylaniline
Conditions | Yield |
---|---|
With polyphosphoric acid at 250℃; for 4h; | 30% |
Conditions | Yield |
---|---|
Stage #1: p-N,N-dimethylaminobenzoic acid With sodium t-butanolate In N,N-dimethyl-formamide at 100℃; for 0.75h; Schlenk technique; Inert atmosphere; Stage #2: 4-n-chlorophenylacetylene; (py)CuIII(CF3)3 In N,N-dimethyl-formamide at 100℃; for 12h; Schlenk technique; Inert atmosphere; stereoselective reaction; | 30% |
Conditions | Yield |
---|---|
Stage #1: p-N,N-dimethylaminobenzoic acid With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: C57H72IrN9O3 In N,N-dimethyl-formamide at 20℃; for 12h; | 34% |
p-N,N-dimethylaminobenzoic acid
methyl iodide
(4-carboxyphenyl)trimethylammonium iodide
Conditions | Yield |
---|---|
In methanol for 16h; Heating; | 35% |
p-N,N-dimethylaminobenzoic acid
2-amino-5-methoxy-thiophenol
4-(6-methoxybenzo[d]thiazol2-yl)-N,N-dimethylaniline
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 170℃; for 0.5h; | 35% |
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