As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiry4-Dimethylaminobenzaldehyde Basic information Product Name: 4-Dimethylaminobenzaldehyde Synonyms: P-dimethylaminobenzaldehyde test solution(ChP);4-(Dimethylamino)benzaldehyde test solution(ChP);4-Dim
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inquiryItems Standard Result Appearance White or Light Yellow Powder White crystal
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiry4-Dimethylaminobenzaldehyde CAS 100-10-7 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, Fine chemicals in
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryADVANTAGE: 1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day 2. The products are provided with COA, HPLC, NMR, quality assurance,
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryProduct Code: DMAB Product name: 4-Dimethylaminobenzaldehyde Category: Pharmaceutical intermediates CAS NO.: 100-10-7
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inquiryAppearance:White to off white crystalline powder Storage:R T Package:25kg/Barrel Application:Determination of indole, skatosin, urine blue mother, tryptophan, albumin, hydrogen peroxide, arsine natrix, anthranilic acid, antipyrine ergoline, etc., an
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inquiry1.In No Less SIX years exporting experience. for US clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service&quo
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inquiryAppearance:White Powder Storage:2 Years Package: according to customers' requirements Application:It is used as a reagent for the determination of uridobitin, indoles, alkaloids, etc Transportation:International express delivery Port: China main p
Cas:100-10-7
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inquiryBeluga chemical professional supply High quality p-Dimethylaminobenzaldehyde CAS 100-10-7 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Mad
Cas:100-10-7
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:100-10-7
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:100-10-7
Min.Order:10 Gram
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inquiry1.high quality: quality is life. quality is the most important element for all goods. we have a lab doing research in wuhan china. hplc and nmr is available if needed. 2.reasonable price: we provide high quality products with competi
Cas:100-10-7
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Cas:100-10-7
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:100-10-7
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inquiryHigh qualityHangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service professional enterprise, Our company mainly engages in global phar
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:100-10-7
Min.Order:4 Kilogram
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Type:Lab/Research institutions
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Cas:100-10-7
Min.Order:1 Gram
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Type:Other
inquiry4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde; | 100% |
4-fluorobenzaldehyde
N,N-dimethyl-formamide
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With PdCl(2-HO-C6H4-CH(Ph)-NH-(CH2)3-SeC6H5); potassium carbonate; phenylboronic acid In water Heating; | 100% |
Conditions | Yield |
---|---|
With silica-supported Jones reagent In dichloromethane for 0.00269444h; | 99.3% |
With potassium carbonate In water at 90℃; for 3h; | 99% |
With potassium hydroxide In toluene at 110℃; for 4h; Catalytic behavior; | 99% |
4-(N,N'-dimethylamino)phenyl-1,3-dithiane
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With bis-[(trifluoroacetoxy)iodo]benzene In methanol; water for 0.166667h; Ambient temperature; | 99% |
With silica gel In neat (no solvent) at 20℃; for 0.0583333h; | 90% |
Conditions | Yield |
---|---|
Stage #1: 4-(1,3-dioxolan-2-yl)phenyl trifluoromethanesulfonate With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); XPhos In tetrahydrofuran at 80℃; for 0.0833333h; Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube; Stage #2: dimethyl amine In tetrahydrofuran at 80℃; for 16h; Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube; | 99% |
4-dimethylaminobenzaldehyde oxime
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20℃; for 0.0166667h; neat (no solvent); | 97% |
With water; Dess-Martin periodane In dichloromethane at 5℃; for 0.333333h; | 92% |
With dihydrogen peroxide; tripropylammonium fluorochromate (VI) In acetone at -10℃; for 0.166667h; | 90% |
carbon monoxide
4-bromo-N,N-dimethylaniline
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; hydrogen; palladium diacetate; propyl di-tert-butylphosphinite In toluene at 100℃; under 3750.38 Torr; for 20h; Inert atmosphere; | 95% |
With Cr(CO)3; hydrogen; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride In toluene at 130℃; | 35% |
With 4-methoxy-N'-tetramethylethylenediamine; hydrogen; catacxium A; palladium diacetate In toluene at 100℃; under 3750.3 Torr; for 16h; | 98 % Chromat. |
With N,N,N,N,-tetramethylethylenediamine; hydrogen; catacxium A; palladium diacetate In toluene at 100℃; under 3750.38 Torr; for 16h; | 98 % Chromat. |
With N,N,N,N,-tetramethylethylenediamine; hydrogen; palladium diacetate; catacxium A In toluene at 20 - 100℃; under 3750.38 Torr; Autoclave; | 99 %Chromat. |
4-(N,N-dimethylamino)benzaldehyde dimethyl acetal
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With iron(III) p-toluenesulfonate hexahydrate In water at 20℃; for 0.75h; | 94% |
bismuth(III) iodide In water at 20℃; for 2h; | 85% |
With copper(II) sulfate; sodium iodide In acetone at 20℃; for 3h; | 82% |
4-formylphenyl N,N-dimethylcarbamate
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0) In toluene at 160℃; for 14h; Inert atmosphere; Sealed tube; Glovebox; | 93% |
p-(1,3-dithiolan-2-yl)-N,N-dimethylaniline
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With silica gel In neat (no solvent) at 20℃; for 0.0666667h; | 92% |
With boron trifluoride diethyl etherate; water; mercury(II) oxide In tetrahydrofuran for 1h; Ambient temperature; | 90% |
With Oxone; potassium bromide In water; acetonitrile at 20℃; for 0.333333h; | 82% |
Conditions | Yield |
---|---|
With hexaaquairon(III) perchlorate for 2h; | 91% |
Conditions | Yield |
---|---|
With pyrrolidine; water In acetonitrile at 20℃; for 12h; Inert atmosphere; | 91% |
With morpholine; palladium 10% on activated carbon; oxygen; copper(l) chloride In isopropyl alcohol at 100℃; for 24h; regioselective reaction; | 87% |
N,N-dimethyl-aniline
N,N-dimethyl-formamide
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With bis(trichloromethyl) carbonate In tetrachloromethane at 40 - 50℃; for 2h; Vilsmeier-Haack formylation; | 90% |
With trichlorophosphate for 0.0833333h; Vilsmeier-Haack reaction; Microwave irradiation; | 80% |
With silica gel; trichlorophosphate for 0.025h; Formylation; Microwave irradiation (300 W); | 78% |
Conditions | Yield |
---|---|
90% | |
formylation; | 90% |
4-(azidomethyl)-N,N-dimethylaniline
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With iron(III) chloride; dihydrogen peroxide In dichloromethane; water for 14h; Reflux; Air; | 90% |
Stage #1: 4-(azidomethyl)-N,N-dimethylaniline With sodium hydride In dimethyl sulfoxide; mineral oil at 20℃; for 4h; Inert atmosphere; Stage #2: With water In dimethyl sulfoxide; mineral oil for 0.25h; Inert atmosphere; | 80% |
N-(4-dimethylaminobenzylidene)-p-toluidine
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With tribromo-isocyanuric acid In acetonitrile for 1h; Reflux; | 90% |
5-(4-N,N-dimethylaminobenzylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With oxone In water; acetonitrile at 45℃; for 1h; | 89% |
N,N-dimethyl-4-((phenylimino)methyl)aniline
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With hexaaquairon(III) perchlorate for 2h; | 88% |
Ru3(CO)10H(OCC6H4N(CH3)2)
A
dodecacarbonyl-triangulo-triruthenium
B
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With CO In benzene High Pressure; heating (3 bar CO, 90 min, 80°C); chromy. (hexane); | A 88% B 81% |
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel dichloride In methanol at -10 - 10℃; | 87% |
Conditions | Yield |
---|---|
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; Inert atmosphere; Sealed tube; | 87% |
Conditions | Yield |
---|---|
With hexaaquairon(III) perchlorate for 2h; | 86% |
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With potassium hydrogencarbonate; dimethyl sulfoxide for 0.0583333h; Microwave irradiation; | 86% |
Vilsmeier reagent
N,N-dimethyl-aniline
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: Vilsmeier reagent; N,N-dimethyl-aniline In N,N-dimethyl-formamide at 70℃; for 1h; Stage #2: With water; sodium carbonate In N,N-dimethyl-formamide | 84% |
und anschliessend mit Wasser; |
4-{[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-amino}-3,6,6-trimethyl-4,6-dihydro-1H-cyclopenta[1,2,4]triazine-5,7-dicarboxylic acid dimethyl ester
A
4-dimethylamino-benzaldehyde
B
4-cyano-N,N-dimethylaniline
Conditions | Yield |
---|---|
With sodium methylate In ethanol for 3h; Product distribution; Heating; | A 12% B 84% |
Conditions | Yield |
---|---|
With hexaaquairon(III) perchlorate for 2h; | 84% |
With sodium perborate In acetic acid at 40℃; for 1.5h; Oxidation; |
2-[4-(dimethylamino)phenyl]acetic acid
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With mercury(II) fluoride; oxygen In acetonitrile at 25℃; for 24h; Irradiation; | 84% |
1-(dibromomethyl)-4-fluorobenzene
dimethyl amine
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With water at 60℃; for 2h; | 82% |
N-(4-methylbenzyl)methanesulfonamide
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
With MS3 Angstroem; oxygen; sodium acetate; triphenylphosphine; palladium dichloride In N,N-dimethyl-formamide at 80℃; under 760 Torr; for 14h; | 82% |
BARBITURIC ACID
4-dimethylamino-benzaldehyde
5-(4-dimethylaminobenzylidene)barbituric acid
Conditions | Yield |
---|---|
In methanol Knoevenagel Condensation; Reflux; | 100% |
In methanol at 20℃; Knoevenagel condensation; | 98% |
With 1-butyl-3-methylimidazolium Tetrafluoroborate at 20℃; for 0.166667h; Knoevenagel condensation; | 98% |
N,N'-diethyl-2-thiobarbituric acid
4-dimethylamino-benzaldehyde
5-(4-(dimethylamino)benzylidene)-1,3-diethyl-2-thioxodihydropyrimidine-4,6(1H,5H)-dione
Conditions | Yield |
---|---|
at 20℃; for 1h; Knoevenagel condensation; | 100% |
In water for 0.5h; Reflux; | 93% |
In ethanol at 20℃; Condensation; Knoevenagel condensation; | 87% |
2'-hydroxy-4-dimethylaminochalcone
Conditions | Yield |
---|---|
Stage #1: o-hydroxyacetophenone With sodium hydroxide In ethanol; water at 0 - 5℃; Stage #2: 4-dimethylamino-benzaldehyde In ethanol; water | 100% |
With potassium hydroxide In ethanol at 25℃; | 85% |
With potassium hydroxide In ethanol at 25℃; | 85% |
ethyl 2-cyanoacetate
4-dimethylamino-benzaldehyde
ethyl (E)-2-cyano-3-[4-(dimethylamino)phenyl]prop-2-enoate
Conditions | Yield |
---|---|
With third generation polystyrene supported poly(amidoamine) dendrimer In ethanol at 50℃; for 0.25h; Knoevenagel condensation; | 100% |
With diazabicyclo[5.4.0]undec-7-ene-water complex at 20℃; for 1h; Knoevenagel condensation; | 100% |
With polyacrylonitrile fiber functionalized with N,N-dimethyl-1,3-propanediamine In ethanol for 1.5h; Knoevenagel condensation; Reflux; | 99% |
4,4'-thiobisaniline
4-dimethylamino-benzaldehyde
4,4'-(((thiobis(4,1-phenylene))bis(azanylylidene))bis(methanylylidene))bis(N,N-dimethylaniline)
Conditions | Yield |
---|---|
With piperidine In ethanol | 100% |
With acetic acid In ethanol for 4h; Reflux; | 85% |
With ethanol; zinc(II) chloride |
Conditions | Yield |
---|---|
In diethyl ether for 1h; Ambient temperature; | 100% |
4-dimethylamino-benzaldehyde
acetone
4-p-dimethylaminophenyl-3-buten-2-one
Conditions | Yield |
---|---|
With sodium hydroxide for 72h; Ambient temperature; | 100% |
With water; potassium hydroxide at 20℃; for 0.2h; | 82% |
With sodium hydroxide In water at 0 - 20℃; Aldol condensation; | 67.73% |
4-dimethylamino-benzaldehyde
methylamine
4-(dimethylamino)-N-methylbenzylimine
Conditions | Yield |
---|---|
at 20℃; under 750.06 Torr; Solid phase reaction; gas-solid reaction; | 100% |
at 20℃; for 12h; | 100% |
With benzene |
4-dimethylamino-benzaldehyde
malononitrile
p-(N-dimethylamino benzylidene) malononitrile
Conditions | Yield |
---|---|
With third generation polystyrene supported poly(amidoamine) dendrimer In ethanol at 30℃; for 0.333333h; Knoevenagel condensation; | 100% |
With polymer supported poly(propylene imine)dendrimer In ethanol at 20℃; for 0.0833333h; Knoevenagel Condensation; Green chemistry; | 100% |
With potassium hydrogen phthalate In water at 20℃; for 0.116667h; Knoevenagel Condensation; Green chemistry; | 99% |
4-dimethylamino-benzaldehyde
methyl 2-cyanoacetate
methyl (E)-2-cyano-3-(4-(N,N-dimethylamino)phenyl)-2-propenoate
Conditions | Yield |
---|---|
at 170℃; for 1h; Knoevenagel condensation; | 100% |
With silica sodium carbonate nanoparticles In acetonitrile at 70℃; Knoevenagel Condensation; Sonication; Green chemistry; | 95% |
With tetra(n-butyl)ammonium hydroxide In ethanol; water at 20℃; for 0.166667h; Knoevenagel condensation; | 94% |
4-dimethylamino-benzaldehyde
4-dimethylaminobenzaldehyde oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In acetonitrile for 4h; Reflux; | 100% |
With sodium hydroxide; hydroxylamine hydrochloride at 20℃; for 0.5h; grinding; | 98% |
With 3 A molecular sieve; hydroxylamine hydrochloride; sodium acetate In ethanol for 0.25h; | 94% |
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; hydroxylamine hydrochloride at 100℃; for 0.25h; Condensation; microwave irradiation; | 100% |
With ammonia; iodine In water; N,N-dimethyl-formamide at 20℃; for 0.666667h; | 99% |
With sodium azide; trifluorormethanesulfonic acid In acetonitrile at 20℃; for 0.0333333h; Schmidt reaction; | 98% |
(p-cyanobenzyl)triphenylphosphonium bromide
4-dimethylamino-benzaldehyde
4-(dimethylamino)-4'-cyanostilbene
Conditions | Yield |
---|---|
With potassium tert-butylate In methanol for 24h; Heating; | 100% |
(i) LiOMe, MeOH, (ii) I2, xylene; Multistep reaction; |
4-dimethylamino-benzaldehyde
cyanoacetic acid amide
(E)-2-cyano-3-[4-(dimethylamino)phenyl]-2-propenamide
Conditions | Yield |
---|---|
With triethylamine at 20℃; for 24h; Knoevenagel condensation; | 100% |
With tetra(n-butyl)ammonium hydroxide In ethanol; water at 20℃; for 0.166667h; Knoevenagel condensation; | 94% |
With Tonsil Actisil FF at 80℃; for 0.333333h; Irradiation; | 55% |
With potassium-exchanged zirconium hydrogen phosphate at 100℃; for 4h; Knoevenagel condensation; | 49% |
With diethylamine |
morpholine
4-dimethylamino-benzaldehyde
(4-(dimethylamino)phenyl)(morpholino)methanone
Conditions | Yield |
---|---|
With bromobenzene; potassium carbonate; triphenylphosphine; palladium diacetate In 1,2-dimethoxyethane for 24h; Heating; | 100% |
morpholine
4-dimethylamino-benzaldehyde
4-<4-(Dimethylamino)thiobenzoyl>morpholine
Conditions | Yield |
---|---|
With sulfur for 0.0666667h; Willgerodt-Kindler reaction; microwave irradiation; | 100% |
With 4-methyl-morpholine; sulfur In N,N-dimethyl-formamide at 135℃; for 6h; Willgerodt-Kindler reaction; | 92% |
With sulfur In dimethyl sulfoxide at 20℃; for 16h; | 89% |
3-acetylcoumarin
4-dimethylamino-benzaldehyde
1-(3'-coumarinyl)-3-(4''-dimethylaminophenyl)-2-propen-1-one
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol Reflux; | 100% |
With piperidine In chloroform for 7h; Heating; | 97% |
With piperidine at 45 - 50℃; for 0.5h; | 91% |
cyclohexylamine
4-dimethylamino-benzaldehyde
N-<<4-(dimethylamino)phenyl>methylene>cyclohexylamine
Conditions | Yield |
---|---|
With sodium sulfate In methanol for 4h; Ambient temperature; | 100% |
propylamine
4-dimethylamino-benzaldehyde
p-Dimethylamino-N-n-propyl-iminomethylbenzol
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
In methanol at 25℃; Mechanism; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); kinetic solvent isotope effect; |
2-(hydroxyimino)propionic acid
4-dimethylamino-benzaldehyde
1-Carboxy-N-(4-dimethylaminophenylmethylen)ethylamin-N-oxid
Conditions | Yield |
---|---|
In ethanol Heating; | 100% |
L-Cysteine
4-dimethylamino-benzaldehyde
(2RS,4R)-2-(4-dimethyloamino-phenyl)-thiazolidine-4-carboxylic acid
Conditions | Yield |
---|---|
In ethanol at 20℃; for 5h; | 100% |
In methanol; water | 84% |
In ethanol; water at 20℃; |
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; for 70h; | 100% |
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
In acetic anhydride at 120℃; for 0.5h; | 100% |
4-dimethylamino-benzaldehyde
acetone
4-(4-N,N-dimethylaminophenyl)-3-buten-2-one
Conditions | Yield |
---|---|
With sodium hydroxide In water at 0 - 25℃; for 3h; | 100% |
With sodium hydroxide In water at 5 - 10℃; for 0.583333h; | 98% |
With sodium hydroxide for 2.5h; Ambient temperature; | 96% |
isopropylamine
4-dimethylamino-benzaldehyde
<4-Dimethylamino-benzyliden>-isopropylamin
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
at 20℃; for 48h; | 79% |
3-acetyl-2,4-dihydroxyquinoline
4-dimethylamino-benzaldehyde
Conditions | Yield |
---|---|
100% |
Conditions | Yield |
---|---|
With phosphoric acid In water; isopropyl alcohol for 6h; Heating; | 100% |
4-dimethylamino-benzaldehyde
(2S)-1-(diphenylphosphino)-3-methylbutan-2-amine
Conditions | Yield |
---|---|
In toluene Ambient temperature; | 100% |
In toluene at 20℃; Substitution; |
N-(4-nitrophenyl)ethylenediamine
4-dimethylamino-benzaldehyde
N-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-N'-(4-nitro-phenyl)-ethane-1,2-diamine
Conditions | Yield |
---|---|
In methanol at 25℃; for 1h; Condensation; | 100% |
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