Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:93-61-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:93-61-8
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:93-61-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
Cas:93-61-8
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:93-61-8
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:93-61-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:93-61-8
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:93-61-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:93-61-8
Min.Order:1 Kilogram
FOB Price: $76.0 / 80.0
Type:Trading Company
inquiryN-Methylformanilide CAS:93-61-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
Cas:93-61-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:93-61-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Detail Minimum Order Qty. 10 Gram
Cas:93-61-8
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:93-61-8
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:93-61-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryN-methylformanilide/factory/best price/high qualityAppearance:clear liquid Storage:Store in dry, dark and ventilated place Package:according to customers' requirements Application:intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...)
Cas:93-61-8
Min.Order:1 Gram
Negotiable
Type:Other
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:93-61-8
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryProduct name: N-Methylformanilide CAS No.:93-61-8 Molecule Formula:C8H9NO Molecule Weight:135.16 Purity: 99.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEM
Cas:93-61-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:93-61-8
Min.Order:1 Kilogram
FOB Price: $100.0 / 102.0
Type:Trading Company
inquiryProduct Name: N-Methylformanilide CAS: 93-61-8 MF: C8H9NO MW: 135.16 EINECS: 202-262-3 Mol File: 93-61-8.mol N-Methylformanilide Structure N-Methylformanilide Chemical Properties Melting point 8-13 °C (lit.) Boiling point
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:93-61-8
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiry1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France etc. 3) OEM/ODM Available;
Cas:93-61-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Superior quality, moderate price & quick delivery. Appearance:colorless transparent liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used in organic syn
Conditions | Yield |
---|---|
With copper (II) carbonate hydroxide; phenylsilane; cyclohexyldiphenylphosphine In acetonitrile at 60℃; for 12h; | 99% |
In toluene for 0.0833333h; Reflux; | 96% |
In toluene at 88 - 108℃; | 96% |
N,N-dimethyl-formamide
N-methylaniline
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With zinc(II) phthalocyanine; carbon dioxide; phenylsilane at 25℃; under 3750.38 Torr; for 6h; Reagent/catalyst; Temperature; Pressure; Autoclave; chemoselective reaction; | 99% |
With 1H-imidazole; nickel oxinate at 150℃; | 85% |
With t-butyldimethylsiyl triflate at 20℃; for 24h; | 82% |
With 1,2,4-Triazole; 8-quinolinol; copper(II) choride dihydrate at 150℃; | 74% |
With methyl benzylphosphonic chloride at 130℃; for 3.5h; | 59% |
Conditions | Yield |
---|---|
With copper(II) acetate dihydrate; phenylsilane; 1,2-bis-(diphenylphosphino)ethane In toluene at 25℃; under 760.051 Torr; for 2h; | 99% |
With Zn(salen); phenylsilane at 25℃; under 3750.38 Torr; for 7h; Reagent/catalyst; Pressure; Temperature; | 99% |
With Al(salen); phenylsilane at 100℃; under 37503.8 Torr; for 3h; Reagent/catalyst; Pressure; Temperature; Autoclave; | 99% |
Conditions | Yield |
---|---|
In acetonitrile at 30℃; | 99% |
Conditions | Yield |
---|---|
With formaldehyd; sodium hydroxide In ethanol; water at 27℃; for 9h; | 97% |
With ethanol; oxalic acid anschliessend man erhitzt das abgeschiedene Salz bis zur Beendung der Gasentwicklung auf 160-180grad; |
N-phenylthioacetamide
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite In water at 20℃; for 0.5h; | 97% |
With triphenyltin(IV) hydroxide In benzene-d6 at 90℃; for 3h; | 50% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 27℃; for 9h; | 97% |
With sodium hydroxide In water; toluene at 20℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; chemoselective reaction; | 94% |
With sodium hydroxide In water at 25℃; for 6h; | 93% |
Conditions | Yield |
---|---|
With phenylsilane; C19H37N2(1+)*Br(1-) In neat (no solvent) at 20℃; under 3750.38 Torr; for 6h; Autoclave; | 95% |
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In toluene at 100℃; under 22502.3 Torr; for 20h; Autoclave; | 70% |
diethylzinc at 100℃; under 34200 Torr; for 18h; | 30% |
With Wilkinson's catalyst; copper diacetate; lithium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; under 760.051 Torr; for 36h; Schlenk technique; |
N,N-dimethyl-aniline
triethyl phosphite
A
triethyl phosphate
B
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; oxygen In 1,2-dichloro-ethane; acetonitrile at 25℃; for 24h; Schlenk technique; Irradiation; | A n/a B 95% |
Conditions | Yield |
---|---|
With Cu/Al2O3; dihydrogen peroxide In water at 50℃; for 12h; Green chemistry; | 95% |
methanol
N-methylaniline
A
N-methyl-N-phenylformamide
B
Formanilid
Conditions | Yield |
---|---|
With lithium hydroxide In water for 4h; Air; Reflux; | A 94% B 5% |
Conditions | Yield |
---|---|
With methanol; lithium hydroxide In water at 80℃; for 4h; | A 94% B 5% |
carbon dioxide
N-methylaniline
A
N,N-dimethyl-aniline
B
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With phenylsilane In N,N-dimethyl acetamide at 60℃; for 4h; Time; Sealed tube; | A 94% B 8% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 110℃; under 760.051 Torr; for 48h; Mechanism; Solvent; Reagent/catalyst; Schlenk technique; | A 92% B 8% |
With phenylsilane; C23H23O2P In acetonitrile at 100℃; under 15001.5 Torr; for 24h; | A 8% B 91% |
Conditions | Yield |
---|---|
With potassium fluoride on basic alumina In acetonitrile at 20℃; for 18h; | 93% |
With sodium ethanolate at 50℃; Riemer-Tiemann reaction; Inert atmosphere; | 65% |
Conditions | Yield |
---|---|
With copper(II) acetate dihydrate; nickel(II) chloride hexahydrate; sodium perchlorate; caesium carbonate In dimethyl sulfoxide at 20℃; Reagent/catalyst; Solvent; Electrolysis; | 93% |
Conditions | Yield |
---|---|
at 60℃; for 15h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
In dichloromethane for 1h; Ambient temperature; | 91.2% |
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether In diethyl ether at -78℃; for 0.5h; | 91% |
Conditions | Yield |
---|---|
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine at 25℃; for 48h; | 91% |
at 50℃; | 80% |
(formyloxy)(acetoxy)phenylmethane
N-methylaniline
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; for 1h; | 91% |
Conditions | Yield |
---|---|
With Silphos at 20℃; for 12h; | 90% |
With N1-(3-(trimethoxysilyl)propyl)ethane-1,2-diamine-sulfamic acid supported on mesoporous silica SBA-15 In neat (no solvent) at 50℃; Green chemistry; | 90% |
With immobilized H2SO4 on activated charcoal at 54℃; for 1.33333h; | 90% |
3-phenyl-2-azido-N-(2-iodophenyl)-N-methylpropanamide
A
3-benzyl-1-methyl-2(1H)-quinoxalinone
B
N-methyl-N-phenyl-carbamoyl cyanide
C
phenylacetonitrile
D
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene at 80℃; | A n/a B n/a C 80% D 89% |
α,α,α-iodinefluoroacetophenone
N-methylaniline
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With water; sodium hydroxide In acetonitrile at 20℃; for 0.166667h; | 89% |
chloroform
N-(3-methylbut-2-enyl)-N-methylaniline
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; potassium hydroxide at 20℃; for 4h; | 88% |
Conditions | Yield |
---|---|
With air In 1,2-dimethoxyethane at 20℃; under 760.051 Torr; Solvent; Irradiation; | 87% |
With FeIII(meso-tetrakis(o,o,m,m-tetrafluoro-p-(dimethylamino)phenyl)porphyrinato)OTf; dihydrogen peroxide; acetic acid In methanol; water at 20℃; for 2h; Reagent/catalyst; chemoselective reaction; | 82% |
With benzyl(triethyl)ammoniumpermanganate In dichloromethane | 78% |
2-(1-adamantyl)-2-azido-N-(2-iodophenyl)-N-methylacetamide
A
3-((1s,3s)-adamantan-1-yl)-1-methylquinoxalin-2(1H)-one
B
1-adamantanecarbonitrile
C
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene at 80℃; | A n/a B 86% C 84% |
Conditions | Yield |
---|---|
With TEMPO; oxygen In acetonitrile at 50℃; under 760.051 Torr; for 12h; | A 71% B 86% |
2-azido-N-(2-iodophenyl)-N-methyltridecanamide
A
1-methyl-3-undecyl-2(1H)-quinoxalinone
B
N-methyl-N-phenylformamide
C
undecyl cyanide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene at 110℃; | A 13% B 80% C 85% |
Conditions | Yield |
---|---|
With copper (I) acetate; caesium carbonate; XPhos In water; N,N-dimethyl-formamide at 110℃; for 12h; Reagent/catalyst; Solvent; Schlenk technique; | 85% |
With water In N,N-dimethyl-formamide at 110℃; for 6h; Mechanism; Solvent; Time; Temperature; Reagent/catalyst; Schlenk technique; | 84% |
With copper (I) acetate; caesium carbonate; XPhos In N,N-dimethyl-formamide at 110℃; for 12h; Reagent/catalyst; Solvent; | 82% |
formamide
N-methylaniline
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With sulfated tungstate at 100℃; for 60h; Green chemistry; | 84% |
With [Mn((N'1E,N'2E)-N'1,N'2-bis(phenyl(pyridin-2-yl)methylene)oxalohydrazide(-H))(OAc)(H2O)]2*6H2O In neat (no solvent) at 120℃; for 24h; | 83% |
With 1-(3-sulfopropyl)pyridinium phosphotungstate In neat (no solvent) at 100℃; for 1.5h; Microwave irradiation; | 75% |
2-carbethoxyindole
N-methyl-N-phenylformamide
ethyl 3-formyl-1H-indole-2-carboxylate
Conditions | Yield |
---|---|
With trichlorophosphate In 1,2-dichloro-ethane for 1.5h; Heating / reflux; | 100% |
With trichlorophosphate In 1,2-dichloro-ethane Vilsmeier-Haack reaction; Heating; | 86% |
Stage #1: N-methyl-N-phenylformamide With chlorophosphonic acid at 20℃; for 0.25h; Stage #2: 2-carbethoxyindole In 1,2-dichloro-ethane for 1.5h; Heating / reflux; | 66% |
With 1,2-dichloro-ethane; trichlorophosphate Behandeln des Reaktionsgemisches mit wss. Natriumacetat; |
6,7,8-trimethoxy-1,4-dimethylcarbazole
N-methyl-N-phenylformamide
3-formyl-6,7,8-trimethoxy-1,4-dimethylcarbazole
Conditions | Yield |
---|---|
With trichlorophosphate for 3.5h; Heating; | 100% |
With trichlorophosphate In Trichloroethylene for 3.5h; Heating; | 99% |
3-fluorobromobenzene
N-methyl-N-phenylformamide
2-bromo-6-fluorobenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 3-fluorobromobenzene With hydrogenchloride; n-butyllithium; diisopropylamine In tetrahydrofuran; hexanes at -78 - -70℃; for 2.5h; Stage #2: N-methyl-N-phenylformamide In tetrahydrofuran; hexanes at -78 - -70℃; for 2h; | 100% |
N-methyl-N-phenylformamide
p-aminoethylbenzoate
N-(4-ethoxycarbonylphenyl)-N'-methyl-N'-phenylformamidine
Conditions | Yield |
---|---|
With thionyl chloride In toluene at 20℃; for 19.5h; Reagent/catalyst; | 99.4% |
In water; toluene for 5h; Solvent; Reflux; | 92.2% |
2-butylthiophene
N-methyl-N-phenylformamide
5-butylthiophene-2-carboxaldehyde
Conditions | Yield |
---|---|
With trichlorophosphate | 99% |
With trichlorophosphate |
Conditions | Yield |
---|---|
With phenylsilane; triphenylphosphine In tetrahydrofuran at 120℃; under 3750.38 Torr; for 24h; Autoclave; Green chemistry; | 99% |
Conditions | Yield |
---|---|
With diazoacetic acid ethyl ester; zinc trifluoromethanesulfonate In cyclohexane for 12h; Reflux; stereoselective reaction; | 99% |
7-Methyl-imidazo[1,2-a]pyridine
N-methyl-N-phenylformamide
7-methylimidazo<1,2-a>pyridine-3-carboxaldehyde
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; cyclopentadienyltricarbonyliron; [copper(II)(trifluoroacetylacetonate)2]; N-butylpyridine p-toluenesulfonate In ethanol at 80℃; for 11h; Reagent/catalyst; | 98.8% |
8-methyl-2-phenylimidazo[1,2-a]pyridine
N-methyl-N-phenylformamide
8-methyl-2-phenylimidazo[1,2-a]pyridine-3-carbaldehyde
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; cyclopentadienyltricarbonyliron; [copper(II)(trifluoroacetylacetonate)2]; N-butylpyridine p-toluenesulfonate In chlorobenzene at 80℃; for 10h; Reagent/catalyst; | 98.6% |
2-methylimidazo[1,2-a]pyridine
N-methyl-N-phenylformamide
2-Methylimidazo<1,2-a>pyridin-3-carboxaldehyd
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; cyclopentadienyltricarbonyliron; [copper(II)(trifluoroacetylacetonate)2]; N-butylpyridine p-toluenesulfonate In toluene at 70℃; for 12h; Reagent/catalyst; | 98.3% |
N-methyl-N-phenylformamide
1,4-Dimethoxy-2-[(3-methoxybenzyl)thio]benzol
2,5-Dimethoxy-4-[(3-methoxybenzyl)thio]benzaldehyd
Conditions | Yield |
---|---|
Stage #1: N-methyl-N-phenylformamide; 1,4-Dimethoxy-2-[(3-methoxybenzyl)thio]benzol With trichlorophosphate at 15 - 60℃; Vilsmeier-formylation; Stage #2: With water for 0.5h; | 98% |
N-methyl-N-phenylformamide
methyl 4-methyl-1H-indole-2-carboxylate
methyl 3-formyl-4-methylindole-2-carboxylate
Conditions | Yield |
---|---|
Stage #1: N-methyl-N-phenylformamide With trichlorophosphate at 20℃; for 0.25h; Stage #2: methyl 4-methyl-1H-indole-2-carboxylate In 1,2-dichloro-ethane for 2.5h; Heating; Further stages.; | 98% |
Conditions | Yield |
---|---|
Stage #1: N-methyl-N-phenylformamide With trichlorophosphate at 0℃; for 0.25h; Stage #2: ferrocene at 20℃; Inert atmosphere; | 98% |
With phosphorus oxychloride In neat (no solvent) anilide and P-compd. stirring at room temp. for 30 min, Fe-compd. addn.,mixt. stirring at room temp. for 3 d, quenching by pouring onto ice, aq . layer extn. after 2 h with Et2O, org. layer drying (MgSO4), vac. concn.; residue flash column chromy. (SiO2, petrol/E2O 7:3 to 5:5), recrystn. (hot petroleum); | 87% |
With trichlorophosphate In neat (no solvent) Vilsmeyer formylation; double mol amt. of formylation mixt., few days at ambient temp.;; | 81% |
2-isopropoxynaphthalene
N-methyl-N-phenylformamide
2-iso-Propoxynaphthalin-1-carbaldehyd
Conditions | Yield |
---|---|
Stage #1: 2-isopropoxynaphthalene; N-methyl-N-phenylformamide With trichlorophosphate at 0 - 75℃; for 12h; Vilsmeier-Haack reaction; Stage #2: With water; sodium hydroxide Vilsmeier-Haack reaction; | 98% |
p-methoxybenzyl chloride
N-methyl-N-phenylformamide
4-methoxy-N-methyl-N-phenylbenzenemethanamine
Conditions | Yield |
---|---|
With NHC-Pd(II)-Im; sodium hydroxide In water at 50℃; for 3h; Inert atmosphere; Schlenk technique; | 98% |
With potassium hydroxide In water at 50℃; for 3h; Green chemistry; | 80% |
N-methyl-N-phenylformamide
Conditions | Yield |
---|---|
With 1-(4-sulfonylbutyl)pyridinium p-toluenesulfonate; tert.-butylhydroperoxide; cyclopentadienyltricarbonyliron; [copper(II)(trifluoroacetylacetonate)2] In 1-methyl-pyrrolidin-2-one at 100℃; for 8h; Reagent/catalyst; | 97.9% |
Conditions | Yield |
---|---|
With 1,3-Dimethoxybenzene; trichlorophosphate In dichloromethane at 40℃; for 24h; Product distribution; other carboxamides, var. solvents, var. temp., var. time, var. reagents mole ratio; | 97% |
With C18H37ClMoNO2P2; hydrogen; sodium triethylborohydride In tetrahydrofuran; toluene at 100℃; under 37503.8 Torr; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Pressure; Temperature; Autoclave; Glovebox; | 94% |
With aluminum oxide; potassium fluoride for 0.333333h; microwave irradiation; | 80% |
1,4-dimethoxy-2,3-methylenedioxybenzene
N-methyl-N-phenylformamide
4,7-dimethoxy-benzo[1,3]dioxole-5-carbaldehyde
Conditions | Yield |
---|---|
With trichlorophosphate at 0 - 20℃; for 3h; Vilsmeier-Haack Formylation; | 97% |
With trichlorophosphate for 48h; Ambient temperature; | 87% |
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