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Cas:586-77-6
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inquiryProduct Description Product Name 4-Bromo-N,N-dimethylaniline CAS No. 586-77-6 Appearance White sheet crystal
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
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inquiry4-Bromo-N,N-dimethylaniline CAS 586-77-6 P-BROMO-N,N-DIMETHYLANILINE CAS no 586-77-6 4-bromo-dimethylaniline 4-Bromo-N,N-dimethylaniline Manufacturer High quality Best price In stock factory CAS 586-77-6 4-Bromo-N,N-dimethylaniline COA TDS pric
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inquiry4-Bromo-N,N-dimethylaniline Basic information Product Name: 4-Bromo-N,N-dimethylaniline Synonyms: P-BROMO-N,N-DIMETHYLANILINE;N,N-DIMETHYL-P-BROMOANILINE;N-(4-BROMOPHENYL)-N,N-DIMETH
Cas:586-77-6
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:586-77-6
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:586-77-6
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inquiryProduct Name: 4-Bromo-N,N-dimethylaniline Synonym: 4-N,N-dimethylaminobromobenzene; 4-Dimethylaminobromobenzene;Intermediate of Mifepristone Cas No.: 586-77-6 Formula: C8H10BrN MW: 200.08 EINECS No.:209-582-2 Density: 1.4±0.1 g/cm3 Boiling p
1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:586-77-6
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:586-77-6
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inquiry4-Bromo-N,N-dimethylaniline CAS:586-77-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
Cas:586-77-6
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:586-77-6
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:586-77-6
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:586-77-6
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:586-77-6
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inquiry586-77-6 factory Buy 4-Bromo-N,N-dimethylaniline Molecular Formula C8H10BrN Molar Mass 200.08 Density 1.3220 Melting Point 52-54 °C (lit.) Boling Point 264 °C (lit.) Flash
Cas:586-77-6
Min.Order:1 Gram
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:586-77-6
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:586-77-6
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:586-77-6
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inquiryProduct name: 4-Bromo-N,N-Dimethylaniline CAS No.:586-77-6 Molecule Formula:C8H10BrN Molecule Weight:200.08 Purity: 98.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
Cas:586-77-6
Min.Order:1 Kilogram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:586-77-6
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inquiry4-Bromo-N,N-dimethylaniline Chemical Properties Melting point 52-54 °C (lit.) Boiling point 264 °C (lit.) density 1.3220 refractive index 1.5748 (estimate) Fp >230 °F storage temp. 2-8°C pka 4.23(at 25℃)
Cas:586-77-6
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:586-77-6
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:586-77-6
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:586-77-6
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inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
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4-(dimethylamino)benzene-boronic acid
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at 20℃; for 0.166667h; | 100% |
With 2-bromopentane; sodium hydride In dimethyl sulfoxide at 80℃; | |
Multi-step reaction with 2 steps 1: toluene / 1 h / 20 °C / Inert atmosphere 2: N-Bromosuccinimide / dichloromethane / 0.17 h / 20 °C View Scheme |
(4-(N,N-dimethylamino)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at 20℃; for 0.166667h; | 100% |
Conditions | Yield |
---|---|
With methanol; tetraethylammonium chloride; bromine In dichloromethane at 35℃; other substituted anilines: regioselectivity of bromination; | 99% |
With methanol; tetraethylammonium chloride; bromine In dichloromethane at 35℃; | 99% |
With hexabromocyclopenta-1,3-diene; triethylamine In acetonitrile for 24h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid at 0 - 65℃; for 3.42h; | 99% |
With Zr(BH4)2Cl2(dabco)2; zirconium(IV) chloride In methanol; water at 20℃; for 0.1h; | 95% |
With sodium tetrahydroborate In 2,2,2-trifluoroethanol for 4.3h; Reflux; | 94% |
Conditions | Yield |
---|---|
With phenylsilane; triphenylphosphine In tetrahydrofuran at 120℃; under 3750.38 Torr; for 24h; Autoclave; Green chemistry; | 99% |
With sodium tetrahydroborate In 1,4-dioxane at 100℃; under 7500.75 Torr; for 24h; Autoclave; | 93% |
With diphenylsilane; [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene In N,N-dimethyl-formamide at 50℃; under 760.051 Torr; chemoselective reaction; | 91% |
Conditions | Yield |
---|---|
With formic acid; triethylamine at 150℃; for 12h; Inert atmosphere; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With diphenylsilane; C21H41N3NiP2 In acetonitrile at 120℃; under 2052.14 Torr; for 24h; Autoclave; | 87% |
With dimanganese decacarbonyl; phenylsilane; C29H33N2P In acetonitrile at 100℃; under 750.075 Torr; for 15h; | 79% |
With methanesulfonic acid; hydrogen; tris(acetylacetonato)ruthenium(III); [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In tetrahydrofuran at 140℃; for 24h; Autoclave; Inert atmosphere; | 89 %Chromat. |
Conditions | Yield |
---|---|
With 0.72 KNaX-BS zeolite at 150℃; for 1h; Reagent/catalyst; | 85% |
carbonic acid dimethyl ester
4-bromo-aniline
A
4-bromo-N-methylaniline
B
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With 0.94 HY-BS zeolite at 150℃; for 1h; | A 81% B 16% |
Conditions | Yield |
---|---|
With Cu1-Mo1/TiO2 In neat liquid at 20℃; for 21h; Catalytic behavior; Inert atmosphere; UV-irradiation; | 80% |
With triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane at 20℃; for 0.5h; chemoselective reaction; | 60% |
With TiO2 supported nano-Pd(0.3) catalyst In water at 20℃; for 5h; Inert atmosphere; Irradiation; Green chemistry; | 8 %Chromat. |
With zinc oxide-supported iridium catalyst at 150℃; under 3750.38 Torr; for 8h; Inert atmosphere; | 38 %Chromat. |
N,N-dimethyl-aniline
A
4-bromo-N,N-dimethylaniline
B
2,4-dibromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With dihydrogen peroxide; vanadia; potassium bromide In chloroform; water at 24.84℃; under 760.051 Torr; | A 75% B 12% |
With [bis(acetoxy)iodo]benzene; lithium bromide In tetrahydrofuran at 20℃; for 0.5h; | A 73% B 18% |
With bromine; acetic acid In tetrachloromethane for 0.0833333h; Ambient temperature; other reagents: bromine, bromodimethylsulfonium bromide, bromodimethylsulfonium bromide/acetic acid; | A 68% B 29% |
(4-dimethylamino-phenyl)-phosphonous acid dichloride
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With pyridine; bromine In dichloromethane at 20℃; for 12h; | 67% |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethylaniline N-oxide With dibromo sulfoxide In tetrahydrofuran at -78℃; for 4h; Inert atmosphere; Stage #2: With triethylamine In tetrahydrofuran at -78 - 23℃; for 0.75h; Solvent; Temperature; Inert atmosphere; regioselective reaction; | 55% |
Conditions | Yield |
---|---|
With rhodium(III) chloride hydrate; potassium tert-butylate at 130℃; for 24h; Sealed tube; High pressure; | 44% |
4-bromo-aniline
methyl iodide
A
4-bromo-N-methylaniline
B
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 20℃; | A 26% B 20% |
With potassium carbonate In tetrahydrofuran at 20℃; | A 26% B 20% |
With potassium carbonate In tetrahydrofuran | A 26% B 20% |
Conditions | Yield |
---|---|
With hydrogenchloride; amalgamated zinc; acetic acid |
5,5-dibromobarbituric acid
ethanol
N,N-dimethyl-aniline
4-bromo-N,N-dimethylaniline
5,5-dibromobarbituric acid
N,N-dimethyl-aniline
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With chloroform; bromine | |
With diethyl ether; bromine |
2-[(4-bromophenyl)(methyl)amino]acetonitrile
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; tetrahydroxydiboron; 5%-palladium/activated carbon In 1,2-dichloro-ethane at 50℃; for 3h; | 100% |
With lithium aluminium tetrahydride; di-tert-butyl peroxide In tetrahydrofuran for 3h; Irradiation; | 93% |
With isopropyl alcohol at 20℃; for 24h; UV-irradiation; chemoselective reaction; | 82% |
4-bromo-N,N-dimethylaniline
phenylboronic acid
N,N-dimethyl-4-biphenylamine
Conditions | Yield |
---|---|
With potassium phosphate; naphthidine di(radical cation)s-stabilized Pd nanoparticles In 1,4-dioxane at 80℃; for 8h; Suzuki-Miyaura cross-coupling reaction; | 100% |
With tetrabutylammomium bromide; potassium carbonate; cyclopalladated N-dodecylferrocenylimine In methanol; water at 20℃; for 18h; Suzuki-Miyaura cross-coupling reaction; | 99% |
With potassium carbonate In ethanol; water at 50℃; for 4h; Suzuki-Miyaura Coupling; | 99% |
4-bromo-N,N-dimethylaniline
methacrylic acid methyl ester
(E)-3-(4-dimethylaminophenyl)-2-methyl acrylic acid methyl ester
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; Cy2NMe2 In 1,4-dioxane at 20℃; for 24h; Heck coupling; | 100% |
With [(C6H5)PdBr2]2[HPtBu3]2 In 1,4-dioxane at 20℃; for 18h; Heck reaction; Inert atmosphere; | 97% |
With N-Methyldicyclohexylamine; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butylphosphonium tetraphenylborate In tetrahydrofuran at 30℃; for 25h; Product distribution / selectivity; | 87% |
sodium cyanide
4-bromo-N,N-dimethylaniline
2-[(4-bromophenyl)(methyl)amino]acetonitrile
Conditions | Yield |
---|---|
With C47H45Cl2N5Ru2(2+)*2F6P(1-); dihydrogen peroxide; acetic acid In methanol at 60℃; for 10h; Inert atmosphere; | 100% |
With dihydrogen peroxide; acetic acid In water at 20℃; for 0.583333h; | 95% |
With oxygen; vanadia; acetic acid In methanol at 60℃; for 2h; | 92% |
Chloro(chloromethyl)dimethylsilane
4-bromo-N,N-dimethylaniline
(chloromethyl)[4-(dimethylamino)phenyl]dimethylsilane
Conditions | Yield |
---|---|
Stage #1: 4-bromo-N,N-dimethylaniline With n-butyllithium In tetrahydrofuran at -78℃; for 1h; Stage #2: Chloro(chloromethyl)dimethylsilane | 99% |
4-bromo-N,N-dimethylaniline
4-chlorobenzophenone
(4'-(dimethylamino)-[1,1'-biphenyl]-4-yl)(phenyl)methanone
Conditions | Yield |
---|---|
Stage #1: 4-bromo-N,N-dimethylaniline With lithium Stage #2: With zinc(II) chloride Stage #3: 4-chlorobenzophenone; nickel phosphine amido pincer complex In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 70℃; for 8h; Negishi cross-coupling; Further stages.; | 99% |
Conditions | Yield |
---|---|
Stage #1: 4-bromo-N,N-dimethylaniline With lithium Stage #2: With zinc(II) chloride Stage #3: chlorobenzene; nickel phosphine amido pincer complex In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 70℃; for 12h; Negishi cross-coupling; Further stages.; | 99% |
2,2,2-trifluoroacetamide
4-bromo-N,N-dimethylaniline
2,2,2-trifluoro-(4-N,N-dimethyphenyl)acetamide
Conditions | Yield |
---|---|
With potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide In 1,4-dioxane at 75℃; | 99% |
sodium cyanide
4-bromo-N,N-dimethylaniline
4-cyano-N,N-dimethylaniline
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; [Pd2(dba)5]; zinc In tetrahydrofuran; acetonitrile at 70℃; for 2h; | 99% |
Diphenylmethane
4-bromo-N,N-dimethylaniline
4-benzhydryl-N,N-dimethylaniline
Conditions | Yield |
---|---|
With KN(SiMe3)2; palladium diacetate; nixantphos In cyclopentyl methyl ether at 24℃; for 12h; Inert atmosphere; | 99% |
With 15-crown-5; NiXantphos; palladium diacetate; sodium hexamethyldisilazane at 23℃; for 12h; Catalytic behavior; Reagent/catalyst; Glovebox; Inert atmosphere; Sealed tube; | 99% |
4-fluorodiphenylmethane
4-bromo-N,N-dimethylaniline
{4-[(4-Fluoro-phenyl)-phenyl-methyl]-phenyl}-dimethyl-amine
Conditions | Yield |
---|---|
With 15-crown-5; NiXantphos; palladium diacetate; sodium hexamethyldisilazane at 23℃; for 12h; Catalytic behavior; Reagent/catalyst; Glovebox; Inert atmosphere; Sealed tube; | 99% |
4-bromo-N,N-dimethylaniline
N-(quinolin-8-yl)-3-(trifluoromethyl)benzamide
C25H20F3N3O
Conditions | Yield |
---|---|
With Ru(OAc)2(p-cymene); sodium carbonate; triphenylphosphine In toluene at 130℃; for 15h; | 99% |
4-bromo-N,N-dimethylaniline
p-tolylboronic pinacol ester
4-dimethylamino-4'-methylbiphenyl
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; potassium hydroxide In neat (no solvent) at 110℃; for 24h; Suzuki-Miyaura Coupling; Schlenk technique; Inert atmosphere; | 99% |
4-bromo-N,N-dimethylaniline
4-tolylmagnesium chloride
4-dimethylamino-4'-methylbiphenyl
Conditions | Yield |
---|---|
With C36H52Br2N4NiSi In tetrahydrofuran at 70℃; for 24h; Kumada Cross-Coupling; Inert atmosphere; Schlenk technique; | 99% |
benzo[c]-[1,2,5]thiadiazole-5,6-dicarbonitrile
4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; palladium diacetate; potassium carbonate; Trimethylacetic acid In toluene at 120℃; Inert atmosphere; Sealed tube; | 99% |
With di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; palladium diacetate; potassium carbonate; Trimethylacetic acid In toluene at 120℃; Inert atmosphere; Sealed tube; |
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