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Cas:78-95-5
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Negotiable
Type:Trading Company
inquiryConditions | Yield |
---|---|
With chlorine; calcium carbonate In water at 110℃; Reagent/catalyst; Temperature; | 95.6% |
With methanol; sulfuryl dichloride In dichloromethane | 85% |
With sulfuryl dichloride |
(C4H9)3SnOCH(CH2Cl)2
A
tributyltin chloride
B
chloroacetone
C
epichlorohydrin
Conditions | Yield |
---|---|
63% decompn. at 210°C (1 h); | A n/a B 5% C 95% |
Conditions | Yield |
---|---|
With trichloroisocyanuric acid; boron trifluoride diethyl etherate In acetic acid for 1h; Heating; Yields of byproduct given; | A n/a B 88% |
With water; chlorine; calcium carbonate |
Conditions | Yield |
---|---|
With sulfuric acid for 3h; Heating; | 85% |
Conditions | Yield |
---|---|
With HT4-c823 In water at 149.84℃; under 750.075 Torr; for 0.5h; Catalytic behavior; Reagent/catalyst; Temperature; Flow reactor; chemoselective reaction; | A 18.9% B 80.5% |
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 1h; Ambient temperature; | A 50% B 14% |
diazoacetone
N,N-dimethyl-formamide
A
chloroacetone
B
2-diazo-3-oxobutanal
Conditions | Yield |
---|---|
With oxalyl dichloride In dichloromethane for 1h; Ambient temperature; | A 50% B 14% |
diazoacetone
B
hydroxy-2-propanone
C
chloroacetone
D
1,1'-oxydi(propan-2-one)
Conditions | Yield |
---|---|
With hydrogenchloride; gallium(III) trichloride; water In dichloromethane at 20℃; for 0.0833333h; | A 34% B 8% C 20% D 31% |
cis/trans-3,5-Bis-(chloromethyl)-3-fluoro-5-methyl-1,2,4-trioxolane
A
chloroacetone
B
chloroacetyl chloride
Conditions | Yield |
---|---|
With triphenylphosphine In chloroform-d1 | A 28 % Spectr. B 23 % Spectr. C 33% |
{Pd2(μ-H)(COCH3)2(μ-dppm)2}BPh4
Pd2(CH3)2(Cl)2(μdppm)2
B
acetaldehyde
C
chloroacetone
Conditions | Yield |
---|---|
In dichloromethane warming of {Pd2(μ-H)(COCH3)2(dppm)2}BPh4 in CH2Cl2 (23°C, 24 h); | A 32% B n/a C n/a |
Conditions | Yield |
---|---|
With chlorine at 0 - 10℃; Kochen des Reaktionsprodukts mit Wasser; |
Conditions | Yield |
---|---|
With sulfuric acid Destillieren der Loesung mit Wasser; |
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether | |
Stage #1: diazoacetone With ethylaluminum dichloride In hexane; dichloromethane at 20℃; for 0.0166667h; Stage #2: With methanol In hexane; dichloromethane |
Conditions | Yield |
---|---|
With water; chlorine |
chloroform
1,4-dichloro-2-methyl-2-butene
A
2-chloroethanal
B
chloroacetone
Conditions | Yield |
---|---|
beim Ozonisierung und Behandeln des Ozonids mit Wasser bei 75-80grad; |
Conditions | Yield |
---|---|
bei der Ozonspaltung; |
Conditions | Yield |
---|---|
beim Destillieren unter gewoehnlichem Druck; |
Conditions | Yield |
---|---|
With water |
Conditions | Yield |
---|---|
at -20℃; |
Conditions | Yield |
---|---|
With N-oxo-N-nitrosoamine at 280℃; under 367754 Torr; |
Conditions | Yield |
---|---|
With chromic acid | |
With ruthenium(IV) oxide; sodium chloride In water; ethyl acetate electrooxidation; | |
With sodium hydroxide; N-bromoacetamide In water at 24.9℃; Mechanism; Kinetics; Thermodynamic data; var. of temp. (Tab. VI); ΔH(excit.), ΔS(excit.), ΔF(excit.); |
methyloxirane
chloroacetone
Conditions | Yield |
---|---|
With chlorine at 0℃; |
Conditions | Yield |
---|---|
With hydrogenchloride 1.) ether, 2 h, -20 to 0 deg C, 2.) -20 deg C to room temp.; Multistep reaction; |
Conditions | Yield |
---|---|
for 48h; |
1,3-Dichloro-2-propanol
A
2,3-Dichloro-1-propanol
B
1,2,3-trichloropropane
C
1-chloro-3-(2-chloro-1-chloromethyl-ethoxy)-propan-2-ol
D
chloroacetone
Conditions | Yield |
---|---|
at 180℃; Product distribution; also in the presence of 1.5 percent HCl or 5percent epichlorhydrin; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 4h; | 100% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 1h; | 100% |
With potassium carbonate In tetrahydrofuran |
O-benzylhydoxylamine hydrochloride
chloroacetone
1-chloropropan-2-one O-benzyloxime
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 20℃; for 5h; | 100% |
With sodium hydroxide In methanol 2.) room temp., 5 h; | 91% |
2,6-dimethyl-1,5-dihydroxynaphthalene
chloroacetone
2,6-Dimethyl-1,5-bis(2-oxopropoxy)naphthalene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide Ambient temperature; | 100% |
2,6-Dipropyl-1,5-naphthalenediol
chloroacetone
2,6-Dipropyl-1,5-bis(2-oxopropoxy)naphthalene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide Ambient temperature; | 100% |
Diethyl 2-methyl-2-(4-thiocarbamoylphenyl)malonate
chloroacetone
Diethyl 2-methyl-2-<4-(4-methylthiozol-2-yl)phenyl>malonate
Conditions | Yield |
---|---|
In benzene for 3.25h; Heating; | 100% |
chloroacetone
1-trimethylsilylpyrazole
Conditions | Yield |
---|---|
at 80℃; for 1h; | 100% |
chloroacetone
1-trimethylsilyl-1,2,4-triazole
Conditions | Yield |
---|---|
at 100℃; for 1h; | 100% |
chloroacetone
1-(trimethylsilyl)-1H-benzotriazole
Conditions | Yield |
---|---|
at 100℃; for 1h; | 100% |
chloroacetone
5-(4-pyridinyl)-1,3,4-oxadiazole-2-thiol
1-(5-Pyridin-4-yl-[1,3,4]oxadiazol-2-ylsulfanyl)-propan-2-one
Conditions | Yield |
---|---|
With sodium hydroxide for 12h; Ambient temperature; | 100% |
8-Chloro-2-methyl-2,3-dihydro-5H-benzo[b][1,4]thiazepin-4-one
chloroacetone
Conditions | Yield |
---|---|
With potassium hydroxide; tetrabutylammomium bromide In tetrahydrofuran Ambient temperature; | 100% |
chloroacetone
6-Fluoro-4-methyl-2-phenyl-thieno[2,3-d]pyrimidin-5-ylamine
6-acetyl-5-amino-4-methyl-2-phenylthieno[2,3-d]pyrimidine
Conditions | Yield |
---|---|
With potassium carbonate | 100% |
Conditions | Yield |
---|---|
at 60℃; for 12h; Solid phase reaction; substitution; | 100% |
chloroacetone
5-(2-chlorophenyl)-3-mercapto-2-cyclohexen-1-one
5-(2-chlorophenyl)-3-[(2-oxopropyl)thio]-2-cyclohexen-1-one
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 20℃; for 5h; | 100% |
With sodium ethanolate In ethanol at 20℃; for 5h; |
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide | 100% |
With sodium hydride In dimethyl sulfoxide at 20℃; | 23% |
2-bromo-4-fluoro-phenol
chloroacetone
1-(2-bromo-4-fluorophenoxy)propan-2-one
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In tetrahydrofuran for 4h; Heating / reflux; | 100% |
With potassium carbonate; potassium iodide In tetrahydrofuran for 4h; Heating / reflux; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 0 - 20℃; | 59% |
With potassium carbonate; potassium iodide In acetone at 55℃; for 2h; | |
With potassium iodide; potassium carbonate In tetrahydrofuran; ethyl acetate | 2.7 gm (100%) |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone at 0 - 20℃; for 1h; Heating / reflux; | 100% |
N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)pyridin-2-yl]thiourea
chloroacetone
{2-[(4-methyl-1,3-thiazol-2-yl)amino]pyridin-4-yl}methanol
Conditions | Yield |
---|---|
In ethanol for 16h; Heating / reflux; | 100% |
In ethanol for 16h; Heating / reflux; | 100% |
In ethanol for 16h; Heating / reflux; Under nitrogen; | 100% |
2-Cyclopropylamino-4,6-difluoro-benzoic acid
chloroacetone
2-Cyclopropylamino-4,6-difluoro-benzoic acid 2-oxo-propyl ester
Conditions | Yield |
---|---|
Stage #1: 2-Cyclopropylamino-4,6-difluoro-benzoic acid With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 1h; Stage #2: chloroacetone In N,N-dimethyl-formamide at 20 - 55℃; for 1.5h; | 100% |
1-(5-bromo-3-(phenylthio)pyridin-2-yl)thiourea
chloroacetone
N-(5-bromo-3-(phenylthio)pyridin-2-yl)-4-methylthiazol-2-amine
Conditions | Yield |
---|---|
With triethylamine In ethanol at 70℃; for 6h; | 100% |
tert-butyl (S)-1-amino-3-(1H-indol-3-yl)-1-thioxopropan-2-yl carbamate
chloroacetone
tert-butyl [(S)-1-(4-hydroxy-4-methyl-4,5-dihydro-thiazol-2-yl)-2-(1H-indol-3-yl)-ethyl]-carbamate
Conditions | Yield |
---|---|
With potassium hydrogencarbonate In 1,2-dimethoxyethane at 45 - 70℃; | 100% |
C9H9ClOS
chloroacetone
1-(4-chloro-1H-benzo[b]thiophen-2-yl)ethanone
Conditions | Yield |
---|---|
With calcium oxide In acetone at 59℃; | 100% |
With calcium oxide for 3h; Reflux; |
2-(ethylsulfanyl)benzenecarbaldehyde
chloroacetone
2-acetyl benzo[b]thiophene
Conditions | Yield |
---|---|
With calcium oxide In acetone at 59℃; | 100% |
With calcium oxide for 3h; Reflux; |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 20h; | 100% |
With sodium hydrogencarbonate In toluene at 110 - 120℃; for 3h; Inert atmosphere; | 22.2% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide In water at 0 - 5℃; Inert atmosphere; | 100% |
chloroacetone
(S)-11-thioxo-2,3,11,11a-tetrahydro-1H-benzo[e]-pyrrolo[1,2-a][1,4]diazepin-5(10H)-one
C15H16N2O2S
Conditions | Yield |
---|---|
Stage #1: (S)-11-thioxo-2,3,11,11a-tetrahydro-1H-benzo[e]-pyrrolo[1,2-a][1,4]diazepin-5(10H)-one With sodium hydride In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere; Stage #2: chloroacetone In dimethyl sulfoxide at 20℃; for 0.666667h; Inert atmosphere; | 100% |
2-amino-3-chloro-4-iodopyridine
chloroacetone
8-chloro-7-iodo-2-methylimidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
In ethanol at 65℃; | 100% |
2,3-dimethylbromobenzene
chloroacetone
2-(2,3-dimethylphenyl)-2-methyloxirane
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethylbromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: chloroacetone In tetrahydrofuran; hexane; toluene at -78 - 20℃; for 1.33333h; Product distribution / selectivity; | 100% |
Stage #1: 2,3-dimethylbromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: chloroacetone In tetrahydrofuran; hexane; toluene at -78 - 20℃; Product distribution / selectivity; | 100% |
1H-indole-3-carbothioamide
chloroacetone
4-methyl-2-(3-indolyl)thiazole
Conditions | Yield |
---|---|
In ethanol at 80℃; for 1.5h; Reflux; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane; acetonitrile at 20℃; for 8h; Reflux; | 100% |
With potassium carbonate In dichloromethane; acetonitrile for 8h; Reflux; | 100% |
With potassium carbonate In dichloromethane; acetonitrile for 8h; Reflux; |
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