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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryTIANFUCHEM--921-03-9--High purity 1,1,3-Trichloroacetone factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable
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Cas:921-03-9
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inquiry1,1,3-Trichloroacetone CAS:921-03-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
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Min.Order:1 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquirysuperior quality moderate price & quick delivery Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Antianemic fol
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:10 Gram
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inquiry1,1,3-Trichloroacetone 921-03-9Appearance:powder Storage:Store in dry, dark and ventilated place Package:according to customers' requirements Application:921-03-9 Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ec
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiry1,1,3-Trichloroacetone Basic information Product Name: 1,1,3-Trichloroacetone Synonyms: 1,1,3-trichloro-2-propanon;1,1,3-TRICHLORO-2-PROPANONE;1,1,3-TRICHLOROACETONE;1,1,3-TCA;1,1,3-TRICHLOROACETONE, WACKER QUALITY;2-Propanone, 1,1,3-trichloro
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Conditions | Yield |
---|---|
Stage #1: acetone With 2-isopropylaniline for 1h; Reflux; Stage #2: With chlorine; sodium hydroxide at 60℃; under 3000.3 Torr; pH=8; Reagent/catalyst; Temperature; pH-value; | 85% |
Stage #1: acetone With 4,4'-bipyridine; chlorine In chlorobenzene at 20 - 30℃; for 2h; Stage #2: With 7,7',8,8'-tetracyanoquinodimethane In chlorobenzene at 50 - 60℃; for 5h; Reagent/catalyst; | 83.2% |
With chlorine at 30℃; Temperature; | 48.1% |
With nickel dichloride at 70℃; bei der Chlorierung; |
Conditions | Yield |
---|---|
With methyllithium; lithium bromide In tetrahydrofuran; diethyl ether at -78℃; for 0.333333h; | 50% |
1) tetrahydrofuran, diethyl ether, -78 deg C, 10 min, 2) water; Yield given. Multistep reaction; |
diazomethane
dichloroacethyl chloride
diethyl ether
1,1,3-trichloroacetone
Conditions | Yield |
---|---|
at -10℃; bei der Behandlung des Reaktionsprodukts mit aether. HCl; |
diazomethane
dichloroacethyl chloride
1,1,3-trichloroacetone
Conditions | Yield |
---|---|
With diethyl ether Behandeln des Reaktionsgemisches mit aether.HCl bei -10grad; |
Conditions | Yield |
---|---|
With chlorine at 30 - 40℃; | |
With chlorine at 40℃; under 750.075 Torr; for 10h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With chlorine at 100℃; Irradiation.mit UV-Licht; |
Conditions | Yield |
---|---|
With chlorine Irradiation; |
Conditions | Yield |
---|---|
With ruthenium(IV) oxide; sodium chloride In water; ethyl acetate at 5℃; Product distribution; other organic solvents; | A 1 % Chromat. B 62 % Chromat. |
pentachloroacetone
(methyloxycarbonylmethyl)triphenylphosphonium bromide
A
1,1,3-trichloroacetone
B
methyl 3-(dichloromethyl)-4,4-dichlorocrotonate
Conditions | Yield |
---|---|
With triethylamine Product distribution; Mechanism; multistep reaction: 1.) THF, 24 h, room t., 2.) THF, 24 h reactions with var. chlorinated propanones under var. conditions; |
chlorine
chloroacetone
A
1,1,3-trichloroacetone
B
1,1,1-trichloroacetone
Conditions | Yield |
---|---|
at 30 - 40℃; |
acetone
A
1,1-Dichloroacetone
B
1,1,3-trichloroacetone
C
chloroacetone
D
1,3-Dichloroacetone
Conditions | Yield |
---|---|
at 70℃; |
1,1,3-trichloroacetone
Conditions | Yield |
---|---|
With ethanol; mercury dichloride |
1,1-Dichloroacetone
chlorine
A
1,1,3-trichloroacetone
B
1,1,1-trichloroacetone
acetone
A
1,1-Dichloroacetone
B
1,1,3-trichloroacetone
C
1,1,1-trichloroacetone
Conditions | Yield |
---|---|
With hydrogenchloride; chlorine at 20 - 80℃; for 8.5h; |
chloroacetone
A
1,1-Dichloroacetone
B
1,1,3-trichloroacetone
C
1,3-Dichloroacetone
Conditions | Yield |
---|---|
With hydrogenchloride; platinum on carbon In water at 95 - 100℃; for 17h; Product distribution / selectivity; | |
With toluene-4-sulfonic acid; platinum on carbon In water at 95 - 100℃; for 17h; Product distribution / selectivity; | |
With toluene-4-sulfonic acid; lithium chloride; platinum on carbon In water at 95 - 100℃; for 17h; Product distribution / selectivity; |
chloroacetone
A
1,1-Dichloroacetone
B
1,1,3-trichloroacetone
C
1,3-Dichloroacetone
D
acetone
Conditions | Yield |
---|---|
dihydrogen hexachloroplatinate In water at 95 - 100℃; for 17h; Product distribution / selectivity; | |
mercury dichloride In water at 95 - 100℃; for 17h; Product distribution / selectivity; | |
cobalt(II) chloride In water at 95 - 100℃; for 17h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With chlorine; iron at 45 - 55℃; for 3h; | 36.96 g |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20 - 70℃; for 16.5h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20 - 70℃; for 16.5h; | 100% |
Conditions | Yield |
---|---|
Stage #1: C15H26O4Si; 1,1,3-trichloroacetone With 2,2,2-trifluoroethanol; triethylamine Stage #2: With zinc In methanol Further stages.; | 98% |
2-aminopyridine
1,1,3-trichloroacetone
A
imidazo[1,2-a]pyridine-2-carbaldehyde
B
2-dichloromethylimidazo<1,2-a>pyridine
C
2-diethoxymethylimidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 4h; Ambient temperature; | A 5% B 90% C 5% |
1,1,3-trichloroacetone
N-(4-aminobenzoyl)-L-glutamic acid
2,4,5-triamino-6-hydroxypyrimidine sulfate
folate
Conditions | Yield |
---|---|
With sodium metabisulfite at 20 - 30℃; for 2h; Temperature; Ionic liquid; | 83.2% |
With sodium metabisulfite; sodium acetate at 45℃; for 3h; Temperature; | 46.2% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20 - 70℃; for 16.5h; | 83% |
2-aminopyridine
1,1,3-trichloroacetone
imidazo[1,2-a]pyridine-2-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-aminopyridine; 1,1,3-trichloroacetone In tetrahydrofuran at 25℃; for 10h; Chichibabin Amination; Stage #2: With calcium carbonate In water at 100℃; for 1h; | 82% |
1,1,3-trichloroacetone
N-(4-aminobenzoyl)-L-glutamic acid
2,4,5-triamino-6-hydroxypyrimidine sulfate
(S)-2-(4-(((2-amino-4-hydroxypteridin-6-yl)methyl)amino)benzamido)pentanedioic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 55℃; for 9h; pH=3; | 80% |
Stage #1: 1,1,3-trichloroacetone; 2,4,5-triamino-6-hydroxypyrimidine sulfate With sodium metabisulfite In methanol; water for 0.5h; Large scale; Stage #2: N-(4-aminobenzoyl)-L-glutamic acid With sodium hydroxide In methanol; water at 40 - 45℃; for 6h; pH=3 - 3.5; Solvent; Large scale; | 69.7% |
Conditions | Yield |
---|---|
Stage #1: 1,1,3-trichloroacetone; tert-butyl (furan-3-ylmethoxy)dimethylsilane With sodium In 2,2,2-trifluoroethanol Stage #2: With zinc/copper couple In methanol | 76% |
Conditions | Yield |
---|---|
In diethyl ether at -10 - -5℃; Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
With sodium acetate for 2h; Hantzsch Thiazole Synthesis; Reflux; | 76% |
1,1,3-trichloroacetone
4,5,6-trimethoxy-9-oxa-1-aza-cyclopenta[a]acenaphthylene
16-aza-10,11,12-trimethoxy-18-oxapentacyclo[7.7.1.12,6.02,8.013,17]octadeca-1(16),7,9(10),11,13(17),14-hexaen-4-one
Conditions | Yield |
---|---|
Stage #1: 1,1,3-trichloroacetone; 4,5,6-trimethoxy-9-oxa-1-aza-cyclopenta[a]acenaphthylene With 2,2,2-trifluoroethanol; triethylamine at 20℃; for 72h; Foehlisch cycloaddition; Stage #2: With ammonium chloride; zinc In methanol at 20℃; for 10h; sonication; Further stages.; | 73% |
1,1,3-trichloroacetone
A
1,1,3,3-tetrachloropropanone
B
pentachloroacetone
Conditions | Yield |
---|---|
With sulfuryl dichloride; N-benzyl-N,N,N-triethylammonium chloride at 55℃; for 168h; | A 72% B n/a |
2-Amino-6-bromopyridine
1,1,3-trichloroacetone
5-bromoimidazo[1,2-a]pyridine-2-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-Amino-6-bromopyridine; 1,1,3-trichloroacetone In 1,2-dimethoxyethane at 25 - 65℃; Inert atmosphere; Large scale reaction; Stage #2: With hydrogenchloride In 1,2-dimethoxyethane; water at 75℃; Large scale reaction; Stage #3: With sodium hydroxide In 1,2-dimethoxyethane at 10℃; pH=8; Large scale reaction; | 72% |
In 1,2-dimethoxyethane at 25 - 65℃; for 2 - 4h; Product distribution / selectivity; | 72% |
Stage #1: 2-Amino-6-bromopyridine; 1,1,3-trichloroacetone In 1,2-dimethoxyethane at 70℃; for 15h; Stage #2: In ethanol for 7h; Heating / reflux; Stage #3: With calcium carbonate In water for 1.5h; Product distribution / selectivity; Heating / reflux; | 50% |
Conditions | Yield |
---|---|
With hydrogenchloride In 1,2-dimethoxyethane; water at 10 - 75℃; | 72% |
2-aminopyridine
1,1,3-trichloroacetone
2-dichloromethylimidazo<1,2-a>pyridine
Conditions | Yield |
---|---|
Stage #1: 2-aminopyridine; 1,1,3-trichloroacetone In 1,2-dimethoxyethane at 20℃; for 4h; Stage #2: In ethanol for 12h; Heating; | 71% |
In 1,2-dimethoxyethane; ethanol for 4h; Reflux; | 5.2 g |
Conditions | Yield |
---|---|
With sodium acetate for 0.666667h; Hantzsch Thiazole Synthesis; Reflux; | 71% |
2-aminopyridine-3-carboxylic acid ethyl ester
1,1,3-trichloroacetone
ethyl 2-(dichloromethyl)imidazo[1,2-a]pyridine-8-carboxylate
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 20℃; | 70% |
2-aminopyridine-3-carboxylic acid ethyl ester
ethanol
1,1,3-trichloroacetone
A
ethyl 2-(dichloromethyl)imidazo[1,2-a]pyridine-8-carboxylate
B
ethyl 2-(diethoxymethyl)imidazo[1,2-a]pyridine-8-carboxylate
Conditions | Yield |
---|---|
Stage #1: 2-aminopyridine-3-carboxylic acid ethyl ester; 1,1,3-trichloroacetone In 1,2-dimethoxyethane at 20℃; for 76h; Inert atmosphere; Stage #2: ethanol for 18h; Inert atmosphere; Reflux; Stage #3: With sodium hydrogencarbonate In water | A 70% B 4% |
1,1,3-trichloroacetone
Conditions | Yield |
---|---|
With sodium acetate for 1h; Hantzsch Thiazole Synthesis; Reflux; | 66% |
1,1,3-trichloroacetone
6-fluoro-pyridin-2-ylamine
2-(dichloromethyl)-5-fluoroimidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 85℃; for 15h; | 65% |
In 1,2-dimethoxyethane at 85℃; for 15h; | 65% |
In 1,2-dimethoxyethane at 85℃; for 15h; Product distribution / selectivity; | 65% |
In 1,2-dimethoxyethane at 85℃; for 15h; | 65% |
In 1,2-dimethoxyethane at 80℃; for 12h; | 63% |
Conditions | Yield |
---|---|
In diethyl ether at -10 - -5℃; Inert atmosphere; | 62% |
Conditions | Yield |
---|---|
Stage #1: 2-Amino-3-bromopyridine; 1,1,3-trichloroacetone In 1,2-dimethoxyethane at 40 - 80℃; Stage #2: With N-ethyl-N,N-diisopropylamine In 1,2-dimethoxyethane at 80℃; for 60h; Stage #3: With calcium carbonate In water at 90℃; for 1h; | 56% |
1,1,3-trichloroacetone
4-(furan-3'-yl)butan-1-ol
6-(4-hydroxy-butyl)-8-oxa-bicyclo[3.2.1]oct-6-en-3-one
Conditions | Yield |
---|---|
Stage #1: 1,1,3-trichloroacetone; 4-(furan-3'-yl)butan-1-ol With sodium 2,2,2-trifluoroethanolate In 2,2,2-trifluoroethanol at 0 - 20℃; for 72h; Stage #2: With copper(I) bromide; zinc In methanol at 20℃; for 48h; | 54% |
1,1,3-trichloroacetone
sodium 2,2,2-trifluoroethanolate
cyclopenta-1,3-diene
Conditions | Yield |
---|---|
Stage #1: 1,1,3-trichloroacetone; cyclopenta-1,3-diene In 2,2,2-trifluoroethanol at 0 - 20℃; for 1h; Stage #2: sodium 2,2,2-trifluoroethanolate In 2,2,2-trifluoroethanol for 10h; Heating; | 53% |
3,6-difluoropyridin-2-amine
1,1,3-trichloroacetone
2-(dichloromethyl)-5,8-difluoroimidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
In 1,4-dioxane at 50 - 100℃; for 120h; | 52% |
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 3h; Heating; | 47% |
Conditions | Yield |
---|---|
Stage #1: 1,1,3-trichloroacetone; C20H28O3 With triethylamine In 1,1,1,3,3,3-hexafluoroisopropaol at 20℃; for 48h; Cooling with ice; Stage #2: With copper; ammonium chloride; zinc In methanol | A 46% B 47% |
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