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inquiryProduct Name: (Aminomethyl)cyclohexane Synonyms: cyclohexanemethanamine;Cyclohexylmethanamine;RARECHEM AL BW 0122;HEXAHYDROBENZYLAMINE;CYCLOHEXANEMETHYLAMINE;AMINOMETHYLCYCLOHEXANE;Cyclohexanemethylamine,97%;Cyclohexylmethylamine, Hexahydrobenz
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inquiry(Aminomethyl)cyclohexane CAS:3218-02-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryProduct name: Cyclohexanemethylamine CAS No.:3218-02-8 Molecule Formula:C7H15N Molecule Weight:113.20 Purity: 99% Package: 200kg/drum Description:Light yellow transparent liquid Manufacture Standards:Enterprise Standard TESTING I
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(Aminomethyl)cyclohexane CAS NO.3218-02-8 Application:(Aminomethyl)cyclohexane CAS NO.3218-02-8
Conditions | Yield |
---|---|
With [Ru(H)(BH4)(CO)(PPh3)(3-(di-tert-butylphosphino)-N-((1-methyl-1H-imidazol-2 yl)methyl)propylamine)]; hydrogen In isopropyl alcohol at 70℃; for 3h; Inert atmosphere; Autoclave; | 99% |
With ammonia; hydrogen In toluene at 120℃; under 22502.3 Torr; for 16h; Autoclave; | 92% |
With hydrogen In ethanol at 88℃; under 37503.8 Torr; for 0.5h; | 91% |
N-(cyclohexylmethyl)-4-methylbenzenesulfonamide
cyclohexylmethylamine
Conditions | Yield |
---|---|
Stage #1: N-(cyclohexylmethyl)-4-methylbenzenesulfonamide With n-butyllithium In tetrahydrofuran at 0℃; Stage #2: With naphthalene; lithium In tetrahydrofuran at -78 - 20℃; | 94% |
Stage #1: N-(cyclohexylmethyl)-4-methylbenzenesulfonamide With n-butyllithium In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With naphthalene; lithium In tetrahydrofuran at -78 - 25℃; Stage #3: With water In tetrahydrofuran | 94% |
Conditions | Yield |
---|---|
With ammonium hydroxide; hydrogen In ethanol at 130℃; under 7500.75 Torr; for 18h; Autoclave; | 92.8% |
With ammonium formate In toluene at 80℃; for 3h; Inert atmosphere; chemoselective reaction; | 90% |
With ammonium formate In toluene at 80℃; for 3h; Inert atmosphere; chemoselective reaction; | 90% |
cyclohexylcarboxamide
A
cyclohexylmethylamine
B
cyclohexylmethyl alcohol
Conditions | Yield |
---|---|
With hydrogen at 160℃; under 75007.5 Torr; | A 91% B 8% |
With dodecacarbonyl-triangulo-triruthenium; hydrogen; molybdenum hexacarbonyl In 1,2-dimethoxyethane at 160℃; under 75007.5 Torr; for 16h; Inert atmosphere; | |
With hydrogen In 1,2-dimethoxyethane at 160℃; under 75007.5 Torr; for 16h; | |
With 5 wt% ruthenium/carbon; water; hydrogen at 59.84℃; under 60006 Torr; for 4h; Reagent/catalyst; Autoclave; Sealed tube; |
cyclohexylcarboxamide
A
N,N-dicyclohexylmethylamine
B
cyclohexylmethylamine
Conditions | Yield |
---|---|
at 160℃; under 75007.5 Torr; | A 7% B 89% |
With ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6h; Catalytic behavior; | A 18 %Chromat. B 80 %Chromat. |
cyclohexane carbonitrile
A
N,N-dicyclohexylmethylamine
B
cyclohexylmethylamine
Conditions | Yield |
---|---|
With 10% rhodium on carbon; hydrogen In cyclohexane at 25℃; under 760.051 Torr; for 24h; | A 89% B n/a |
(azidomethyl)cyclohexane
cyclohexylmethylamine
Conditions | Yield |
---|---|
With ammonium formate; zinc In methanol at 20℃; for 0.166667h; | 88% |
With hydrogen; 25% palladium on carbon In methanol under 2585.81 Torr; for 2h; |
cyclohexylamine
benzonitrile
A
N-phenyl(methylidene)cyclohexanamine
B
cyclohexylmethylamine
Conditions | Yield |
---|---|
With ammonium hydroxide; hydrogen In hexane at 100℃; under 3750.38 Torr; for 36h; Autoclave; Green chemistry; | A 78.2% B 10.6% |
benzoic acid
A
cyclohexane
B
N-(cyclohexylmethyl)cyclohexanecarboxamide
C
N,N-dicyclohexylmethylamine
D
cyclohexylcarboxamide
E
cyclohexylmethylamine
Conditions | Yield |
---|---|
Stage #1: benzoic acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A 5% B 2% C 7% D 4% E 78% |
cyclohexylcarboxamide
A
N,N-dicyclohexylmethylamine
B
cyclohexylmethylamine
C
cyclohexylmethyl alcohol
Conditions | Yield |
---|---|
With hydrogen at 150℃; under 75007.5 Torr; | A 9% B 77% C 13% |
With tris(2,4-pentanedionato)ruthenium(III); hydrogen; molybdenum hexacarbonyl In 1,2-dimethoxyethane at 160℃; under 75007.5 Torr; for 16h; Inert atmosphere; | |
With hydrogen; lithium hydroxide In 1,2-dimethoxyethane at 160℃; under 75007.5 Torr; for 16h; |
Conditions | Yield |
---|---|
With platinum(IV) oxide; hydrogen In ethanol at 30℃; under 30003 Torr; for 12h; Autoclave; | A 77% B 21% C 2% |
Conditions | Yield |
---|---|
With carbonylchlorohydrido(4,5-bis((diisopropylphosphino)methyl)acridine)ruthenium(II); ammonia In toluene under 5700.38 Torr; for 25h; Inert atmosphere; Reflux; | A 73% B n/a |
With ammonia; carbonylchlorohydrido(4,5-bis((diisopropylphosphino)methyl)acridine)ruthenium(II) In toluene under 5700.38 Torr; for 25h; Product distribution / selectivity; Reflux; |
Pentafluorobenzonitrile
A
cyclohexylmethylamine
B
cyclohexylmethyl alcohol
Conditions | Yield |
---|---|
With water In aq. phosphate buffer at 25℃; for 18h; pH=2.7 - 3.2; Electrochemical reaction; | A 33% B 65% |
Conditions | Yield |
---|---|
With ammonium hydroxide; hydrogen In ethanol at 130℃; under 7500.75 Torr; for 12h; Autoclave; | A 64.8% B 16.9% |
4-fluorobenzonitrile
A
cyclohexylmethylamine
B
cyclohexylmethyl alcohol
Conditions | Yield |
---|---|
With water In aq. phosphate buffer at 25℃; for 6h; pH=2.7 - 3.2; Electrochemical reaction; | A 35% B 63% |
isophthalic acid
A
3-azabicyclo<3.3.1>nonane
B
3-azabicyclo[3.3.1]nonan-2-one
C
(3-methylcyclohexyl)methanamine
D
cyclohexylmethylamine
Conditions | Yield |
---|---|
Stage #1: isophthalic acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A 57% B 21% C 11% D 3% |
salicylic acid
A
2-METHYLCYCLOHEXYLAMINE
B
cyclohexylamine
C
cyclohexylcarboxamide
D
cyclohexylmethylamine
Conditions | Yield |
---|---|
Stage #1: salicylic acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A 11% B 50% C 11% D 10% |
Conditions | Yield |
---|---|
Stage #1: 3-Methoxybenzoic acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A n/a B n/a C 6% D 44% |
Conditions | Yield |
---|---|
In ethanol for 2h; Inert atmosphere; Schlenk technique; Reflux; | A 36% B n/a |
cyclohexylmethylene diacetate
cyclohexylmethylamine
Conditions | Yield |
---|---|
With methanol; ammonia; nickel at 100℃; under 106400 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With sodium azide; sulfuric acid |
cyclohexylmethylcarbamic acid methyl ester
cyclohexylmethylamine
Conditions | Yield |
---|---|
With calcium hydroxide |
benzylamine hydrochloride
cyclohexylmethylamine
Conditions | Yield |
---|---|
With platinum(IV) oxide; ethanol at 50 - 60℃; under 1520 - 2280 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With ammonia; nickel at 100 - 110℃; under 91938.4 Torr; Hydrogenation; | |
With i-Amyl alcohol; sodium | |
(i) H2, Raney-Ni, (ii) aq. HCl; Multistep reaction; |
Conditions | Yield |
---|---|
With lithium |
formamide
cyclohexanecarbaldehyde
cyclohexylmethylamine
Conditions | Yield |
---|---|
With ammonium sulfate anschliessend mit wss.HCl; |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | |
Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: P2O5 / durch Destillation 2: sodium; alcohol View Scheme |
Conditions | Yield |
---|---|
With nickel at 170 - 180℃; Hydrogenation; | |
With acetic acid; platinum at 50 - 60℃; under 1520 - 2280 Torr; Hydrogenation; | |
With hydrogen In neat (no solvent) at 80℃; under 7600.51 Torr; for 24h; Autoclave; | 54 %Spectr. |
With hydrogen In tert-butyl alcohol at 135℃; for 24h; Autoclave; | 93 %Chromat. |
With hydrogen In 1,4-dioxane at 100℃; under 15001.5 Torr; for 3.33333h; Autoclave; |
Conditions | Yield |
---|---|
With ammonia; nickel at 185℃; | |
Multi-step reaction with 2 steps 1.1: potassium tert-butylate; copper diacetate / toluene / 120 h / 150 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 2.2: -78 - 25 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C 2: sodium azide / N,N-dimethyl-formamide / 65 °C 3: hydrogen / 25% palladium on carbon / methanol / 2 h / 2585.81 Torr View Scheme |
chloroacetyl chloride
cyclohexylmethylamine
2-chloro-N-(cyclohexylmethyl)acetamide
Conditions | Yield |
---|---|
In dichloromethane | 100% |
With potassium carbonate In dichloromethane Heating; | 97% |
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 60% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane Heating; | 100% |
N-(4-fluoro-3-nitrophenyl)acetamide
cyclohexylmethylamine
N-{4-[(cyclohexylmethyl)amino]-3-nitrophenyl}acetamide
Conditions | Yield |
---|---|
With sodium carbonate In ethanol at 60℃; for 48h; Heating; | 100% |
With sodium carbonate In ethanol at 20 - 60℃; for 48h; | 100% |
With sodium carbonate In ethanol at 20 - 60℃; for 48h; | 100% |
4-fluoro-3-nitrobenzonitrile
cyclohexylmethylamine
4-[(cyclohexylmethyl)amino]-3-nitro-benzonitrile
Conditions | Yield |
---|---|
With sodium carbonate In ethanol at 20℃; | 100% |
di-tert-butyl dicarbonate
cyclohexylmethylamine
tert-butyl N-cyclohexylmethylcarbamate
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; | 100% |
With triethylamine In tetrahydrofuran for 1h; Cooling with ice; | 85% |
3-oxobenzo[d]isothiazole-2(3H)-carbaldehyde 1,1-dioxide
cyclohexylmethylamine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.25h; chemoselective reaction; | 100% |
tert-butyl-[(1S,2S)-(4R)-4-(4-tert-butylsulfonylthieno[3,2-d]pyrimidin-7-yl)-2-(methoxymethoxymethyl)cyclopentoxy]-dimethyl-silane
cyclohexylmethylamine
7-[(1R,3S,4S)-3-[tert-butyl(dimethyl)silyl]oxy-4-(methoxymethoxymethyl)cyclopentyl]-N-(cyclohexylmethyl)thieno[3,2-d]pyrimidin-4-amine
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 150℃; for 3h; Microwave irradiation; | 100% |
cyclohexylmethylamine
2,4-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With DIPEA | 100% |
4-fluoro-3-nitro-benzoic acid methyl ester
cyclohexylmethylamine
4-(cyclohexylmethyl-amino)-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 100% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine | 100% |
4-chloro-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidine
cyclohexylmethylamine
Conditions | Yield |
---|---|
In ethanol for 24h; Reflux; | 100% |
cyclohexylmethylamine
Conditions | Yield |
---|---|
In 1,4-dioxane for 20h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran Ambient temperature; | 99% |
Cyclohexyl isocyanate
cyclohexylmethylamine
1-Cyclohexyl-3-cyclohexylmethyl-urea
Conditions | Yield |
---|---|
In hexane at 20℃; | 99% |
cyclohexylmethylamine
(4-fluoro-3-nitrophenyl)carbamic acid tert butyl ester
N-(4-[(cyclohexylmethyl)amino]-3-nitrophenyl)-2,2-dimethylpropanamide
Conditions | Yield |
---|---|
With triethylamine In ethanol at 75℃; for 24h; | 99% |
4-(4'-trifluoromethyl-biphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid
cyclohexylmethylamine
N-(cyclohexylmethyl)-4-(4'-trifluoromethylbiphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid amide
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In N-methyl-acetamide | 99% |
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In N-methyl-acetamide | 99% |
2,3,5,6-tetrabromoterephthaloyl dichloride
cyclohexylmethylamine
C22H28Br4N2O2
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 23h; Reflux; | 99% |
2-cyclopropyl-5-((2-trimethylsilanyl)ethoxymethyl)-5H-pyrrolo[2,3-b]pyrazin-7-carboxylic acid
cyclohexylmethylamine
2-cyclopropyl-5-(2-trimethylsilanyl-ethoxymethyl)-5H-pyrrolo[2,3-b]pyrazine-7-carboxylic acid cyclohexylmethyl-amide
Conditions | Yield |
---|---|
Stage #1: 2-cyclopropyl-5-(2-trimethylsilanyl-ethoxymethyl)-5H-pyrrolo[2,3-b]pyrazine-7-carboxylic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 60℃; for 0.75h; Stage #2: cyclohexylmethylamine In tetrahydrofuran at 20℃; for 3h; | 99% |
dimethyl (S)-2-[N-(chloroacetyl)-N-(naphthalen-1-ylmethyl)amino]butandioate
cyclohexylmethylamine
methyl (S)-2-[4-(cyclohexylmethyl)-1-(naphthalen-1-ylmethyl)-3,6-dioxopiperazin-2-yl]acetate
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 20℃; for 16h; Molecular sieve; | 99% |
With triethylamine In acetonitrile at 20℃; Inert atmosphere; |
N,N-dimethyl-formamide
cyclohexylmethylamine
1,3-Bis(cyclohexylmethyl)urea
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In 5,5-dimethyl-1,3-cyclohexadiene at 165℃; for 24h; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With pentamethoxy tantalum; 1-(Trimethylsilyl)imidazole In neat (no solvent) at 50℃; for 48h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With sodium carbonate In water pH=9 - 10; | 99% |
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 7h; | 98% |
cyclohexylmethylamine
2-(bromomethyl)-7-(benzyloxy)chroman
(7-Benzyloxy-chroman-2-ylmethyl)-cyclohexylmethyl-amine
Conditions | Yield |
---|---|
at 100℃; for 2h; | 98% |
cyclohexylmethylamine
Methacryloyl chloride
N-(cyclohexylmethyl)methacrylamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 98% |
2-chloro-3-methyl-5-nitropyridine
cyclohexylmethylamine
N-(cyclohexylmethyl)-3-methyl-5-nitro-2-pyridinamine
Conditions | Yield |
---|---|
With triethylamine In ethanol for 12h; Heating / reflux; | 98% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; under 760.051 Torr; for 36h; | 98% |
cyclohexylmethylamine
carbonic acid dimethyl ester
cyclohexylmethylcarbamic acid methyl ester
Conditions | Yield |
---|---|
lipase from Candida antarctica In toluene at 70℃; for 15h; | 98% |
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