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inquiryProduct Description Product website: http://www.finerchem.com Product Name 3,4-Dichlorophenylacetonitrile CAS No.
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inquiry3,4-Dichlorophenylacetonitrile Basic information Product Name: 3,4-Dichlorophenylacetonitrile Synonyms: Benzeneacetonitrile, 3,4-dichloro-;3,4-Dichlorophenylacetonitrile,98%;3,4-DICHLOROPHENYLACETONITRILE;3,4-DICHLOROBENZYL CYANIDE;3,4-DCCN;2-(
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inquiryISO Factory/Good qualityAppearance:off white Storage:dry and cool place Package:10G/BAG; 1KG/BAG ;25KG/DRUM Application:Active pharaceutical ingredients Transportation:BY SEA,AIR,EXPRESS Port:SHANGHAI;BEIJING
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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2-aminoacetonitrile hydrochloride
3,4-dichlophenylboronic acid
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
With sodium nitrite In water; toluene at 50℃; for 24h; Schlenk technique; | 85% |
3,4-dichlorophenyl acetic acid
N-cyano-N-phenyl-p-toluenesulfonamide
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
Stage #1: 3,4-dichlorophenyl acetic acid With lithium diisopropyl amide In tetrahydrofuran; hexane at 0℃; for 0.25h; Inert atmosphere; Stage #2: N-cyano-N-phenyl-p-toluenesulfonamide In tetrahydrofuran; hexane at 0 - 20℃; for 18h; Inert atmosphere; | 84% |
potassium cyanide
3,4-dichlorobenzyl bromide
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
In ethanol; water for 4h; Heating; | 79% |
sodium cyanide
3,4-Dichlorophenylmethyl chloride
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 80℃; for 2h; | 65% |
In ethanol Heating; | |
In dimethyl sulfoxide at 40 - 50℃; for 5h; Yield given; |
potassium cyanide
3,4-Dichlorophenylmethyl chloride
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
In ethanol; water |
sodium cyanide
3,4-dichlorobenzyl bromide
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
In water |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: PBr3 / CH2Cl2 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 57 percent / cerium(III) ammonium nitrate, potassium bromide / acetic acid / 1.5 h / 80 - 90 °C 2: 79 percent / ethanol; H2O / 4 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Br2 / Irradiation 2: H2O View Scheme |
Conditions | Yield |
---|---|
With sulfuric acid for 20h; Heating; | 100% |
With potassium hydroxide | |
With sodium hydroxide In ethanol Heating; Yield given; |
carbonic acid dimethyl ester
3,4-dichloro-benzeneacetonitrile
cyano-(3,4-dichlorophenyl)acetic acid methyl ester
Conditions | Yield |
---|---|
With sodium methylate In toluene Heating; | 100% |
With sodium methylate In toluene Heating; | 100% |
With sodium methylate In toluene at 85℃; for 3h; | 93% |
Conditions | Yield |
---|---|
Stage #1: 3,4-dichloro-benzeneacetonitrile With n-butyllithium In tetrahydrofuran at -75℃; for 0.333333h; Stage #2: 2-(methylsulfanyl)benzaldehyde In tetrahydrofuran at -75℃; for 0.5h; Stage #3: With borane-THF In tetrahydrofuran at -75℃; Temperature; Reflux; | 100% |
(S)-epichlorohydrin
3,4-dichloro-benzeneacetonitrile
((1S,2R)-2-(aminomethyl)-2-(3,4-dichlorophenyl)cyclopropyl)methanol
Conditions | Yield |
---|---|
Stage #1: (S)-epichlorohydrin; 3,4-dichloro-benzeneacetonitrile With sodium hexamethyldisilazane In tetrahydrofuran at -15 - 4℃; Inert atmosphere; Stage #2: With dimethylsulfide borane complex at -5 - 40℃; for 6.5h; | 100% |
3,4-dichloro-benzeneacetonitrile
2-(3,4-dichlorophenyl)ethanamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; aluminium trichloride | 98% |
With ammonia; hydrogen; nickel In ethanol; water under 760.051 Torr; for 6h; | 92% |
With potassium borohydride; copper dichloride In water; isopropyl alcohol at 60℃; for 5h; | 85% |
3,4-dichloro-benzeneacetonitrile
(3,4-dichlorophenyl)hydroxyiminoacetic acid
Conditions | Yield |
---|---|
With potassium hydroxide; nitrous acid isobutyl ester In methanol at 50 - 90℃; for 26h; | 98% |
With potassium hydroxide; isopentyl nitrite In methanol; acetonitrile at 50 - 90℃; for 11.5h; | 89% |
Conditions | Yield |
---|---|
Stage #1: ethanol; 3,4-dichloro-benzeneacetonitrile With hydrogenchloride In diethyl ether at 0 - 5℃; Pinner Imino Ether Synthesis; Stage #2: With sodium hydrogencarbonate In diethyl ether; water at 4 - 8℃; for 0.166667h; Pinner Imino Ether Synthesis; | 98% |
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran at 0℃; for 1.5h; Inert atmosphere; | 97% |
With potassium tert-butylate In tetrahydrofuran at 0℃; Inert atmosphere; | 97% |
With sodium hydroxide In water; dimethyl sulfoxide at 45℃; for 2h; |
Conditions | Yield |
---|---|
With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; Sealed tube; | 95% |
4-fluorobenzaldehyde
3,4-dichloro-benzeneacetonitrile
2-(3,4-dichloro-phenyl)-3c-(4-fluoro-phenyl)-acrylonitrile
Conditions | Yield |
---|---|
With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; Sealed tube; | 94% |
5-phenylfuran-2-carbaldehyde
3,4-dichloro-benzeneacetonitrile
C19H11Cl2NO
Conditions | Yield |
---|---|
With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; Sealed tube; | 94% |
3,4-dichloro-benzeneacetonitrile
methyl iodide
2-(3,4-dichlorophenyl)propanenitrile
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃; for 1h; | 93% |
Stage #1: 3,4-dichloro-benzeneacetonitrile With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With potassium carbonate In methanol for 5h; Ambient temperature; | 92% |
2-methoxynicotinaldehyde
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
Stage #1: 3,4-dichloro-benzeneacetonitrile With n-butyllithium In tetrahydrofuran; diethyl ether; hexane at -75 - -60℃; Inert atmosphere; Stage #2: 2-methoxynicotinaldehyde In tetrahydrofuran; diethyl ether; hexane at -75 - -60℃; for 1.5h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
Stage #1: 4-(methylamino)benzaldehyde; 3,4-dichloro-benzeneacetonitrile In water at 50℃; Knoevenagel Condensation; Stage #2: With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; | 92% |
Conditions | Yield |
---|---|
With iron (III) perchlorate monohydrate In neat (no solvent) at 80℃; for 2h; Ritter Amidation; | 91% |
3,4-dichloro-benzeneacetonitrile
2-(3,4-dichlorophenyl)ethanethioamide
Conditions | Yield |
---|---|
Stage #1: 3,4-dichloro-benzeneacetonitrile With calcium hydride; tiolacetic acid at 80℃; for 1.5h; Stage #2: With water In ethyl acetate at 20℃; | 90% |
With hydrogen sulfide; triethylamine In ethanol at 20℃; | 55% |
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water at 60℃; for 6h; pH=Ca. 10; | 90% |
Conditions | Yield |
---|---|
With hydrogenchloride In chloroform | 89.8% |
With acetyl chloride at 0℃; Inert atmosphere; | 80% |
With hydrogenchloride In diethyl ether | |
With hydrogenchloride In diethyl ether Pinner Imino Ether Synthesis; | |
With hydrogenchloride at 0 - 5℃; |
acetic anhydride
3,4-dichloro-benzeneacetonitrile
N-<2-(3,4-dichlorophenyl)ethyl>acetamide
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide under 2068.6 Torr; for 5h; | 89% |
ethyl bromoacetate
3,4-dichloro-benzeneacetonitrile
3-cyano-3-(3,4-dichloro-phenyl)-pentanedioic acid diethyl ester
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran | 89% |
With sodium hexamethyldisilazane In tetrahydrofuran | |
With hydrogenchloride; sodium hydroxide; sodium hexamethyldisilazane In tetrahydrofuran; tert-butyl methyl ether; water; isopropyl alcohol |
Conditions | Yield |
---|---|
With piperidine In water at 50℃; for 5h; Solvent; Knoevenagel Condensation; Ionic liquid; Sealed tube; | 89% |
With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; Sealed tube; | 72% |
N-benzyl-trimethylammonium hydroxide In water Knoevenagel condensation; Heating; | |
With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; |
4-Trifluoromethylbenzaldehyde
3,4-dichloro-benzeneacetonitrile
C16H8Cl2F3N
Conditions | Yield |
---|---|
With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; Sealed tube; | 89% |
3,4-dichloro-benzeneacetonitrile
Conditions | Yield |
---|---|
With sodium methylate In methanol for 1.5h; Knoevenagel Condensation; Reflux; | 89% |
Conditions | Yield |
---|---|
With trifluoromethylsulfonic anhydride In chloroform for 24h; Heating; | 88% |
Conditions | Yield |
---|---|
Stage #1: 3,4-dichloro-benzeneacetonitrile With n-butyllithium In tetrahydrofuran; hexane at -75℃; Stage #2: 3-nitro-benzaldehyde In tetrahydrofuran; hexane at -75 - -70℃; | 87% |
Conditions | Yield |
---|---|
Stage #1: 3,4-dichloro-benzeneacetonitrile With n-butyllithium In tetrahydrofuran; diethyl ether; hexane at -78 - -60℃; Stage #2: ortho-anisaldehyde In tetrahydrofuran; diethyl ether; hexane at -75 - -55℃; | 87% |
Conditions | Yield |
---|---|
Stage #1: 4-aminobenzaldehyde; 3,4-dichloro-benzeneacetonitrile In water at 50℃; Knoevenagel Condensation; Stage #2: With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; | 87% |
Conditions | Yield |
---|---|
Stage #1: 3-nitro-benzaldehyde; 3,4-dichloro-benzeneacetonitrile In water at 50℃; Knoevenagel Condensation; Stage #2: With N-benzyl-trimethylammonium hydroxide In water at 50℃; for 5h; Knoevenagel Condensation; | 87% |
2-Chlorobenzonitrile
3,4-dichloro-benzeneacetonitrile
2-[Cyano-(3,4-dichloro-phenyl)-methyl]-benzonitrile
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 25℃; for 4h; | 85% |
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