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inquiry2-(METHYLTHIO) BENZALDEHYDE CAS:7022-45-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct Name: 2-(METHYLTHIO) BENZALDEHYDE Synonyms: 2-(METHYLTHIO) BENZALDEHYDE;2-(Methylmercapto)-benzaldehyde;o-(Methylthio)benzaldehyde;2-(METHYLTHIO)BENZALDEHYDE / 2-THIOANISALDEHYDE;2-Methylsulfanylbenzaldehyde;2-(methylthio) Benz
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:7022-45-9
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:7022-45-9
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:7022-45-9
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Type:Lab/Research institutions
inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
FandaChem , a China-based chemical company, specialize in exporting 2-(Methylthio)benzaldehyde cas 7022-45-9 (Fandachem), Please contact us by email freely. Appearance:white crystalline powder Storage:Store in dry, dark and
Cas:7022-45-9
Min.Order:1 Kilogram
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Type:Other
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Type:Lab/Research institutions
inquiry7022-45-9 2-(METHYLTHIO) BENZALDEHYDE Application:7022-45-9 2-(METHYLTHIO) BENZALDEHYDE
Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
Cas:7022-45-9
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Type:Trading Company
inquiryBest quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
Cas:7022-45-9
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Negotiable
Type:Lab/Research institutions
inquiry2-(methylthio)benzyl alcohol
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With dimethylsulfide; N-succinimide; triethylamine In toluene | 94% |
With pyridinium chlorochromate In dichloromethane at 20℃; for 1h; | 69% |
With pyridinium chlorochromate In dichloromethane at 0 - 20℃; for 12h; | 65% |
dimethyl sulfoxide
ortho-bromobenzaldehyde
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide at 130℃; for 12h; Sealed tube; Inert atmosphere; | 93% |
2-chloro-benzaldehyde
sodium thiomethoxide
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide for 5h; Heating; | 86% |
In N,N-dimethyl-formamide at 20℃; for 44h; | 44% |
2-Fluorobenzaldehyde
sodium thiomethoxide
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane; N,N-dimethyl-formamide at 55℃; for 24h; Inert atmosphere; | 85% |
In N,N-dimethyl-formamide at 0.15℃; Inert atmosphere; | 85% |
In acetonitrile Heating; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 55℃; for 24h; | 85% |
Stage #1: methylthiol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1.5h; Inert atmosphere; Stage #2: 2-Fluorobenzaldehyde In N,N-dimethyl-formamide; mineral oil at -40℃; for 2h; Inert atmosphere; |
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane; N,N-dimethyl-formamide | 85% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 55 - 80℃; for 24h; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In water at 189℃; for 24h; | 64% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In water at 189℃; for 15h; | 56% |
2-(Methylthio)thiobenzoesaeure-S-mesitylester
A
2.2'-Bis(methylthio)benzil
B
2-(methylsulfanyl)benzaldehyde
C
bis(2,4,6-trimethylphenyl)disulfide
Conditions | Yield |
---|---|
In benzene at 20℃; for 70h; Irradiation; | A 22% B 11% C 41% |
<2-methylthio-α-oxo-phenylmethan>-diphenylphosphin
A
2-(methylsulfanyl)benzaldehyde
B
<2-Methylthio-α-hydroxyphenylmethan>-diphenyl-phosphinoxid
Conditions | Yield |
---|---|
In benzene at 22℃; for 120h; Irradiation; | A 16% B 14% |
2-Methylthiobenzoesaeuremesitylester
A
2.2'-Bis(methylthio)benzil
B
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
In benzene at 20℃; for 77h; Irradiation; | A 9% B 7% C 5% |
N'-p-Toluolsulfonyl-N-<2-methylmercapto-benzoyl>-hydrazin
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With sodium carbonate In ethylene glycol at 160℃; | |
With sodium carbonate In diethylene glycol |
1-chloromethyl-2-methylsulfanylbenzene
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With hexamethylenetetramine; acetic acid |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran | |
(i) LiAlH4, THF, (ii) aq. HCl; Multistep reaction; |
Dimethyldisulphide
1,3-dimethyl-2-phenylimidazolidine
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
Dimethyldisulphide
1,3-dimethyl-2-phenylimidazolidine
A
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
In acetic acid at 19.9℃; Rate constant; Kinetics; Thermodynamic data; ΔH(excit.), ΔS(excit.), ΔG(excit.), var. temp.; |
2-(Methylsulfinyl)thiobenzoesaeure-S-mesitylester
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2 percent / benzene / 70 h / 20 °C / Irradiation 2: 11 percent / benzene / 70 h / 20 °C / Irradiation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 56 percent / toluene / 2 h / Heating 2: 7 percent / benzene / 77 h / 20 °C / Irradiation View Scheme | |
Multi-step reaction with 2 steps 1: 42 percent / toluene / 2 h / Heating 2: 11 percent / benzene / 70 h / 20 °C / Irradiation View Scheme | |
Multi-step reaction with 2 steps 1: 40 percent / diethyl ether 2: 16 percent / benzene / 120 h / 22 °C / Irradiation View Scheme | |
Multi-step reaction with 2 steps 1: aq. NaOH / dioxane 2: LiAlH4 / tetrahydrofuran View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: LiAlH4 / tetrahydrofuran 2: SOCl2 / benzene 3: hexamethylenetetramine, aq. AcOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: (i) (diazotization), (ii) aq. Na2S2, (iii) aq. Na2S2O4,(iv) (methylation) 2: (i) SOCl2, (ii) /BRN= 1718733/ 3: LiAlH4 / tetrahydrofuran 4: SOCl2 / benzene 5: hexamethylenetetramine, aq. AcOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: (i) SOCl2, (ii) /BRN= 1718733/ 2: LiAlH4 / tetrahydrofuran 3: SOCl2 / benzene 4: hexamethylenetetramine, aq. AcOH View Scheme | |
Multi-step reaction with 2 steps 1: (i) SOCl2, benzene, (ii) /BRN= 741982/ 2: (i) LiAlH4, THF, (ii) aq. HCl View Scheme | |
Multi-step reaction with 3 steps 1: SOCl2 2: aq. NaOH / dioxane 3: LiAlH4 / tetrahydrofuran View Scheme |
2-methylthiobenzohydrazide
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Py 2: Na2CO3 / ethane-1,2-diol / 160 °C View Scheme |
2-(methylthio)cyclohex-1-ene-1-carbaldehyde
A
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
at 24.84℃; for 0.0833333h; Inert atmosphere; Schlenk technique; Glovebox; |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C 2: pyridinium chlorochromate / dichloromethane / 12 h / 0 - 20 °C View Scheme |
2-(methylsulfanyl)benzaldehyde
2-(methylsulfinyl)benzaldehyde
Conditions | Yield |
---|---|
With C42H70O35*Br3Fe; ferric nitrate In acetonitrile at 20℃; for 3h; chemoselective reaction; | 100% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 20℃; | 89% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 20℃; | 89% |
2-(methylsulfanyl)benzaldehyde
(1R,2R)-1,2-diaminocyclohexane
(1R,2R)-N,N'-bis[(2-(methylthio)benzylidene)]-1,2-cyclohexanediamine
Conditions | Yield |
---|---|
In ethanol at 80℃; | 100% |
Conditions | Yield |
---|---|
Stage #1: 3,4-dichloro-benzeneacetonitrile With n-butyllithium In tetrahydrofuran at -75℃; for 0.333333h; Stage #2: 2-(methylsulfanyl)benzaldehyde In tetrahydrofuran at -75℃; for 0.5h; Stage #3: With borane-THF In tetrahydrofuran at -75℃; Temperature; Reflux; | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 18h; Inert atmosphere; Molecular sieve; | 100% |
1,1-pentamethylene-1,2-nonadiene
2-(methylsulfanyl)benzaldehyde
2-(cyclohexylidenemethyl)-1-(2-(methylthio)phenyl)octan-1-one
Conditions | Yield |
---|---|
With [Rh(dppe)]ClO4 In acetone at 55℃; Inert atmosphere; regioselective reaction; | 99% |
C13H18O
2-(methylsulfanyl)benzaldehyde
(E)-2-(2-(furan-2-yl)vinyl)-1-(2-(methylthio)phenyl)octan-1-one
Conditions | Yield |
---|---|
With [Rh(dppe)]ClO4 In acetone at 55℃; Inert atmosphere; regioselective reaction; | 99% |
C13H18S
2-(methylsulfanyl)benzaldehyde
(E)-1-(2-(methylthio)phenyl)-2-(2-(thiophen-2-yl)vinyl)octan-1-one
Conditions | Yield |
---|---|
With [Rh(dppe)]ClO4 In acetone at 55℃; Inert atmosphere; regioselective reaction; | 99% |
2-(methylsulfanyl)benzaldehyde
(4-methylpenta-1,2-dien-1-yl)benzene
(E)-2-isopropyl-1-(2-(methylthio)phenyl)-4-phenylbut-3-en-1-one
Conditions | Yield |
---|---|
With [Rh(dppe)]ClO4 In acetone at 55℃; Inert atmosphere; regioselective reaction; | 99% |
2-(methylsulfanyl)benzaldehyde
buta-1,2-diene-1,4-diyldibenzene
(E)-2-benzyl-1-(2-(methylthio)phenyl)-4-phenylbut-3-en-1-one
Conditions | Yield |
---|---|
With [Rh(dppe)]ClO4 In acetone at 55℃; Inert atmosphere; regioselective reaction; | 99% |
2-(methylsulfanyl)benzaldehyde
[Rh(bis(di-tert-butylphosphino)methane)(cyclooctene)(NCCH2BF3)]
acetone
Conditions | Yield |
---|---|
In acetone | 99% |
(4-bromo-2-ethynylphenyl)carbamic acid 1,1-dimethylethyl ester
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis(dicyclohexylphosphino)methane In acetone at 20℃; for 0.333333h; Inert atmosphere; | 99% |
2-(methylsulfanyl)benzaldehyde
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
Conditions | Yield |
---|---|
With C28H26FeN2S4 In benzene-d6 at 20℃; for 0.5h; | 99% |
With [CoCl2(4'-(4-pyridyl)-2,2':6',2''-terpyridine)]·2H2O; potassium tert-butylate In tetrahydrofuran at 25℃; for 16h; Inert atmosphere; Glovebox; | 95 %Chromat. |
With two-dimensional iron(II) coordination polymer based on a divergent 4'-(4-diphenylamino)phenyl-4,2';6',4''-terpyridine ligand; potassium tert-butylate In neat (no solvent) at 20℃; for 0.5h; Green chemistry; chemoselective reaction; | 88 %Chromat. |
With potassium tert-butylate; Mn(2+)*C20H14N4*2Cl(1-) In tetrahydrofuran at 25℃; for 2h; Inert atmosphere; Glovebox; | |
With 0.55C27H43N3Si3V*0.45C27H44N3Si3V In diethyl ether at 20℃; for 2h; Inert atmosphere; Glovebox; Schlenk technique; chemoselective reaction; |
Conditions | Yield |
---|---|
Stage #1: 2-ethynyl-6-methoxynaphthalene With n-butyllithium In tetrahydrofuran Stage #2: 2-(methylsulfanyl)benzaldehyde In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: 4-trifluoromethylphenylacetylene With n-butyllithium In tetrahydrofuran Stage #2: 2-(methylsulfanyl)benzaldehyde In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 99% |
2-tert-butyl-5-methoxy-phenylamine
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
In toluene Heating; | 98% |
2-(methylsulfanyl)benzaldehyde
2-(1,1-dimethylethyl)-benzenamine
(2-tert-butylphenyl)-(2-thiomethyl-benzylidene)-amine
Conditions | Yield |
---|---|
In toluene Heating; | 98% |
oct-1-ene
2-(methylsulfanyl)benzaldehyde
1-(2-(methylthio)phenyl)nonan-1-one
Conditions | Yield |
---|---|
With C21H44N2P2Rh*C32H12BF24 In acetone at 55℃; for 3h; Inert atmosphere; | 98% |
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; silver perchlorate; bis[2-(diphenylphosphino)phenyl] ether In acetone at 55℃; for 24h; Inert atmosphere; | 73% |
With potassium phosphate; chloro(1,5-cyclooctadiene)rhodium(I) dimer; (11aR)-(+)-10,11,12,13-tetrahydrodiindeno[7,1-de:1', 7'-fg][1,3,2]dioxaphosphocin-5-bis[(R)-1-phenylethyl]amine In 1,2-dichloro-ethane at 70℃; for 72h; Inert atmosphere; | 48% |
With [Rh(η6-C6H5F)(bis(dicyclohexylphosphino)methane)][B(C6H3-3,5-(CF3)2)4] In 1,2-dichloro-ethane at 80℃; for 2h; Inert atmosphere; | |
With C29H39FO2P2Rh(1+)*C32H12BF24(1-) In acetone at 24.84℃; for 0.0833333h; Reagent/catalyst; |
C11H20
2-(methylsulfanyl)benzaldehyde
(E)-2-(3-methylbut-1-enyl)-1-(2-(methylthio)phenyl)heptan-1-one
Conditions | Yield |
---|---|
With [Rh(dppe)]ClO4 In acetone at 55℃; Inert atmosphere; regioselective reaction; | 98% |
N-methylmaleimide
2-(methylsulfanyl)benzaldehyde
1-methyl-3-(2-(methylthio)benzoyl)pyrrolidine-2,5-dione
Conditions | Yield |
---|---|
With C29H39FO2P2Rh(1+)*C32H12BF24(1-) In acetone at 55℃; for 3h; Inert atmosphere; Glovebox; | 98% |
With C29H52N2P2Rh*C32H12BF24 In acetone at 55℃; for 3h; Inert atmosphere; | 81% |
(2-propenyl)propanedioic acid diethyl ester
2-(methylsulfanyl)benzaldehyde
1,3-diethyl 2-(4-(2-(methylthio)phenyl)-4-oxobutyl)malonate
Conditions | Yield |
---|---|
With C21H44N2P2Rh*C32H12BF24 In acetone at 55℃; for 3h; Inert atmosphere; | 98% |
With [Rh(η6-C6H5F)(bis(dicyclohexylphosphino)methane)][B(C6H3-3,5-(CF3)2)4] In 1,2-dichloro-ethane at 80℃; for 2h; Inert atmosphere; |
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis(dicyclohexylphosphino)methane In acetone at 20℃; for 2h; Inert atmosphere; | 98% |
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis(dicyclohexylphosphino)methane In acetone at 20℃; for 0.5h; Inert atmosphere; | 98% |
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis(dicyclohexylphosphino)methane In acetone at 20℃; for 0.333333h; Inert atmosphere; | 98% |
2-(methylsulfanyl)benzaldehyde
ethylenediamine
N,N-bis[(2-methylthio)phenylmethylene]-1,2-ethanediamine
Conditions | Yield |
---|---|
In acetonitrile | 97% |
In ethanol at 80℃; Inert atmosphere; |
2-ethynyl-1-nitrobenzene
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis(dicyclohexylphosphino)methane In acetone at 55℃; for 0.25h; Inert atmosphere; | 97% |
1-ethynyl-4-methoxy-2-nitrobenzene
2-(methylsulfanyl)benzaldehyde
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis(dicyclohexylphosphino)methane In acetone at 55℃; for 0.333333h; Inert atmosphere; | 97% |
2-(methylsulfanyl)benzaldehyde
ethyl (triphenylphosphoranylidene)acetate
o-Methylthio-zimtsaeure-aethylester
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 12h; | 97% |
3-Aethyl-1.1-diphenylallen
2-(methylsulfanyl)benzaldehyde
2-ethyl-1-(2-(methylthio)phenyl)-4,4-diphenylbut-3-en-1-one
Conditions | Yield |
---|---|
With [Rh(dppe)]ClO4 In acetone at 55℃; Inert atmosphere; regioselective reaction; | 96% |
3-ethynylthiophene
2-(methylsulfanyl)benzaldehyde
(E)-1-(2-(methylthio)phenyl)-3-(thiophen-3-yl)prop-2-en-1-one
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; 1,2-bis-(dicyclohexylphosphino)ethane In acetone at 20℃; for 2h; Inert atmosphere; regioselective reaction; | 96% |
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