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Cas:3218-36-8
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryHebei yanxi chemical co., LTD is a professional research, development and production Cyromazine、lead diacetate trihydrate /Lead acetate trihydrateC、 2-phenylacetamide 、 4-Aminophenyl-1-phenethylpiperidine 、Citric acid monohydrate 、 Citric acid/c
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Type:Manufacturers
inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
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inquiryProduct name 4-Biphenylcarboxaldehyde Product category Biphenyl series CAS NO. 3218-36-8 Structural formula Appearance:White powder Storage:Store in cool and dry place, away from sun light. Packa
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inquiryProduct Name: 4-Biphenylcarboxaldehyde Synonyms: p-Biphenylcarboxaldehyde p-Diphenylaldehyde p-Diphenylcarboxaldehyde;Biphenyl-4-carboxaldehyde 98%;Biphenyl-4-carboxaldehyde, 98+%;4-Biphenylcarboxaldehyde,99%;Of phenyl-benzaldehyde;4-Biphenylca
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Min.Order:1 Gram
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inquiry4-Biphenylcarboxaldehyde CAS:3218-36-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i
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inquiryProduct name: 4-Biphenyl Carboxaldehyde CAS No.: 3218-36-8 Molecule Formula:C13H10O Molecule Weight:182.22 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING I
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inquiryConditions | Yield |
---|---|
With potassium carbonate In methanol at 100℃; for 0.166667h; Suzuki-Miyaura Coupling; Microwave irradiation; | 100% |
With 2,2-bis-(N-2-morpholinethylbenzimidazolium)-ethylether dichloride; potassium tert-butylate; palladium diacetate In water; N,N-dimethyl-formamide at 50℃; for 3h; Reagent/catalyst; Suzuki Coupling; | 100% |
With caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane for 1h; Suzuki-Miyaura coupling; Heating; | 99% |
Conditions | Yield |
---|---|
With sodium phosphate; palladium on activated charcoal In water; isopropyl alcohol at 20℃; for 6h; Suzuki-Miyaura reaction; | 100% |
With sodium carbonate; palladium on activated charcoal In ethanol at 20℃; for 5h; Suzuki-Miyaura cross-coupling; | 100% |
With potassium carbonate; bis(2-diphenylphosphinoxynaphthalen-1-yl)methane; palladium diacetate In methanol at 20℃; for 1h; Suzuki cross-coupling reaction; | 100% |
Conditions | Yield |
---|---|
With n-butyltriphenylphosphonium permanganate In acetonitrile at 20℃; for 0.25h; | 100% |
With silica-supported Jones reagent In dichloromethane for 0.00269444h; | 99.7% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-methyl-N-[3-(4'-diacetoxyiodo)phenoxy-1-propyl]pyrrolidinium 4-methylbenzenesulfonate In dichloromethane at 20℃; for 6h; | 99% |
Conditions | Yield |
---|---|
With [Pd(N-(naphthyl)-salicylaldimine(-2H))(triphenylphosphine)]; sodium hydroxide at 120℃; for 3h; Suzuki Coupling; | 100% |
With tetra-n-propylammonium bromide; sodium carbonate In water at 100℃; for 0.5h; Catalytic behavior; Suzuki-Miyaura Coupling; | 100% |
With potassium carbonate; palladium dichloride In water at 20 - 90℃; Suzuki coupling; Inert atmosphere; | 99% |
1,1-diacetoxy-1-(4-biphenyl)methane
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
zeolite HSZ-360 for 0.333333h; Irradiation; | 99% |
With zirconium(IV) chloride In methanol at 20℃; for 0.05h; | 96% |
With 2,6-dicarboxypyridinium chlorochromate In acetonitrile at 20℃; for 0.5h; | 70% |
Conditions | Yield |
---|---|
With bis(1,1'-ethylene-3,3'-divinylimidazole-2,2'-diylidene)nickel(II) dibromide dihydrate; potassium carbonate In water; N,N-dimethyl-formamide at 100℃; for 8h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 99% |
With potassium carbonate In water; N,N-dimethyl-formamide at 30℃; for 4h; Suzuki-Miyaura Coupling; Irradiation; Inert atmosphere; | 98% |
With potassium phosphate In ethanol; water at 80℃; for 3h; Suzuki-Miyaura Coupling; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water at 80℃; for 2h; Suzuki-Miyaura Coupling; | 99% |
With palladium diacetate In water; isopropyl alcohol at 27℃; for 1h; Suzuki-Miyaura Coupling; | 96% |
With C12H12Cl2N4O2Pd; caesium carbonate In water at 60℃; for 5h; Suzuki-Miyaura Coupling; | 90% |
Conditions | Yield |
---|---|
With sodium hydroxide; palladium diacetate In water at 110℃; for 2h; Suzuki-type reaction; | 99% |
With sodium carbonate at 100℃; for 0.666667h; Suzuki Coupling; | 97% |
With sodium carbonate at 80℃; for 0.716667h; Catalytic behavior; Suzuki Coupling; | 97% |
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole
4-chlorobenzaldehyde
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In water at 20℃; for 6h; Suzuki-Miyaura Coupling; | 99% |
biphenyl-4-carbaldehyde oxime
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With 1-benzyl-4-aza-1-azoniabiyclo<2.2.2>octane peroxodisulfate In acetonitrile for 0.25h; Heating; | 98% |
With 1-benzyl-4-aza-1-azoniabiyclo<2.2.2>octane peroxodisulfate In acetonitrile for 0.25h; Oxidation; Heating; | 98% |
With tris[trinitratocerium(IV)] paraperiodate at 90℃; for 0.166667h; | 95% |
With Nitrogen dioxide In acetonitrile at 25℃; for 0.0833333h; |
4-(trifluormethanesulfonyloxy)benzaldehyde
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride; bis(dibenzylideneacetone)-palladium(0); CyJohnPhos In tetrahydrofuran for 6h; Heating; | 98% |
Conditions | Yield |
---|---|
With [Pd(N-(3-chloro-2-quinoxalinyl)-N'-(2,6-diisopropylphenyl)imidazolium)(PPh3)Cl2]; potassium carbonate In water at 70℃; for 3h; Catalytic behavior; Suzuki-Miyaura Coupling; | 98% |
With palladium diacetate; potassium carbonate In ethanol; water at 25℃; for 2h; Suzuki-Miyaura Coupling; | 95% |
With 5%-palladium/activated carbon; oxygen; potassium carbonate In ethanol; water at 80℃; for 0.416667h; Suzuki-Miyaura Coupling; | 93% |
Conditions | Yield |
---|---|
With cesium fluoride In water; N,N-dimethyl-formamide at 40℃; for 5h; Stille coupling; | 98% |
With [Pd{C6H2-(CH2CH2NH2)-(OMe)2-3,4}Br(PPh3)]; potassium carbonate In N,N-dimethyl-formamide at 90℃; for 0.0666667h; Stille coupling; Microwave irradiation; | 95% |
With C31H33INPPd In N,N-dimethyl-formamide at 80℃; for 24h; Stille coupling; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran; water at 25℃; Suzuki coupling; | 98% |
4-(dibromomethyl)-1,1'-biphenyl
dimethyl sulfoxide
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
at 100℃; for 2h; | 97% |
Conditions | Yield |
---|---|
With sodium carbonate at 80℃; for 3.16667h; Catalytic behavior; Stille Cross Coupling; | 97% |
With (2-methylacetatobenzyl)triphenylphosphonium hexabromodipalladate(II); potassium carbonate at 90℃; for 0.166667h; Stille Cross Coupling; | 95% |
With potassium carbonate for 0.4h; Stille Cross Coupling; | 95% |
4-formylphenylboronic acid,
diphenyl(2,2,2-trifluoroethyl)sulfonium trifluoromethanesulfonate
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium hydrogencarbonate In N,N-dimethyl-formamide at 60℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; Glovebox; Sealed tube; | 97% |
4-bromo-1,1'-biphenyl
N,N-dimethyl-formamide
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With samarium; copper(l) iodide at 20℃; for 4h; Inert atmosphere; | 96% |
Formylation; | 88% |
(i) nBuLi, Et2O, (ii) /BRN= 605365/; Multistep reaction; |
[2-(hydroxymethyl)phenyl](dimethyl)phenylsilane
p-(iodophenyl)carboxaldehyde
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate; N-cyclohexyl-1-[2-(diphenylphosphanyl)phenyl]methanimine; palladium dichloride In water; dimethyl sulfoxide at 50℃; for 27h; | 96% |
Conditions | Yield |
---|---|
With dichlorobis(tricyclohexylphosphine)nickel(II) In benzene at 25℃; for 1h; | 96% |
Conditions | Yield |
---|---|
Stage #1: phenylzinc iodide-lithium chloride complex With trans-[1,3-bis(2,6-diisopropylphenyl)imidazolin-2-ylidene]PdCl2(NC5H5) In tetrahydrofuran at 20℃; for 0.05h; Inert atmosphere; Stage #2: 4-(Methylthio)benzaldehyde In tetrahydrofuran; acetonitrile at 20℃; for 4h; Inert atmosphere; | 96% |
4-formylbenzene-1-sulfonyl fluoride
phenylboronic acid
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With palladium diacetate; diisopropylamine In ethanol; water at 25℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Temperature; Suzuki-Miyaura Coupling; | 96% |
Conditions | Yield |
---|---|
With sodium hydroxide; PEG encapsulated palladium nanoparticle In water at 90℃; for 2.5h; Hiyama cross-coupling reaction; | 95% |
With sodium hydroxide In ethanol; water at 110℃; for 0.1h; Hiyama coupling; Microwave irradiation; | 95% |
With sodium hydroxide In ethylene glycol at 100℃; for 1h; Hiyama Coupling; | 95% |
4-(trifluormethanesulfonyloxy)benzaldehyde
phenylboronic acid
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With sodium carbonate; palladium on activated charcoal In ethanol; water at 20℃; for 24h; Suzuki-Miyaura coupling reaction; | 95% |
Conditions | Yield |
---|---|
With triphenyl phosphite; potassium phosphate tribasic trihydrate; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride; palladium diacetate In tert-butyl alcohol at 80℃; for 4h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; (9-phenanthrenyl)Ni(II)(PPh3)2Cl; potassium carbonate In toluene at 110℃; for 20h; Suzuki Coupling; Inert atmosphere; | 95% |
With 2-hydroxy-3-(p-tolyl)-2,3-dihydroindan-1-one; palladium diacetate; potassium carbonate In ethanol for 2h; Reagent/catalyst; Solvent; Time; Suzuki-Miyaura Coupling; Reflux; | 92% |
With potassium phosphate; Ni(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)[P(OPh)3]2 In tetrahydrofuran at 70℃; for 18h; Suzuki-Miyaura Coupling; Sealed tube; | 22% |
Conditions | Yield |
---|---|
Stage #1: 4-hydroxy-benzaldehyde With fluorosulfonyl fluoride; potassium carbonate In ethanol; water at 20℃; for 4h; Stage #2: phenylboronic acid With potassium carbonate; palladium dichloride In ethanol; water at 20℃; for 6h; | 95% |
With potassium phosphate; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); 4-methyl-N-phenyl-N-tosylbenzenesulfonamide In 1,4-dioxane at 110℃; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 90% |
Stage #1: 4-hydroxy-benzaldehyde With potassium phosphate; fluorosulfonyl fluoride In 1,4-dioxane at 20℃; for 48h; Stage #2: phenylboronic acid With bis(tricyclohexylphosphine)nickel(II) dichloride; tricyclohexylphosphine tetrafluoroborate In 1,4-dioxane at 80℃; for 15h; | 40% |
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole
4-bromo-benzaldehyde
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water at 20℃; Suzuki-Miyaura Coupling; Green chemistry; | 95% |
With dichloro bis(acetonitrile) palladium(II); potassium phosphate; 1,1'-bis(di-tertbutylphosphino)ferrocene In tetrahydrofuran; water at 60℃; for 20h; Suzuki Coupling; Inert atmosphere; | 88% |
With potassium hydroxide In water; isopropyl alcohol at 80℃; for 6h; Reagent/catalyst; Suzuki-Miyaura Coupling; Schlenk technique; Green chemistry; |
tetraphenyltin(IV)
4-bromo-benzaldehyde
A
biphenyl
B
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With dmap; palladium dichloride for 0.333333h; Stille Cross Coupling; Microwave irradiation; | A 3% B 95% |
lithium cyanide
benzoyl chloride
4-Phenylbenzaldehyde
α-Benzoyloxy-α-(4-biphenylyl)acetonitrile
Conditions | Yield |
---|---|
In tetrahydrofuran for 0.5h; Ambient temperature; | 100% |
2,6-dichloro-p-phenylenediamine
4-Phenylbenzaldehyde
N'-[1-Biphenyl-4-yl-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine
Conditions | Yield |
---|---|
In ethanol for 1.5h; Heating; | 100% |
4-Phenylbenzaldehyde
4-(thiomorpholinomethyl)aniline
Conditions | Yield |
---|---|
With acetic acid | 100% |
With acid Condensation; | 93% |
Conditions | Yield |
---|---|
In ethanol for 4h; Heating; | 100% |
4-Phenylbenzaldehyde
N2-[2R-isobutyl-3S-(9-fluorenylmethoxycarbonylamino)-4-hydroxysuccinyl]-L-tert-leucine-N1-methylamide
Conditions | Yield |
---|---|
Multistep reaction; | 100% |
4-(trifluoromethyl)benzoic acid hydrazide
4-Phenylbenzaldehyde
4-trifluoromethylbenzoyl acid biphenyl-4-yl-methylene hydrazide
Conditions | Yield |
---|---|
In methanol for 3h; Heating / reflux; | 100% |
4-Phenylbenzaldehyde
1-t-Butoxycarbonylpiperazine
tert-butyl 4-([1,1'-biphenyl]-4-ylmethyl)piperazine-1-carboxylate
Conditions | Yield |
---|---|
With triethylamine; trimethyl orthoformate In dichloromethane at 20℃; for 1h; | 100% |
With sodium tris(acetoxy)borohydride; acetic acid In methanol for 15h; Inert atmosphere; |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 2h; Reflux; | 100% |
Conditions | Yield |
---|---|
With [Pd(N-(naphthyl)-4-methoxy-salicylaldimine(-2H))(triphenylphosphine)]; sodium hydroxide at 120℃; for 4h; Reagent/catalyst; Suzuki Coupling; | 100% |
1,3-diaminoguanidine hydrochloride
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
In ethanol for 16h; Reflux; | 100% |
In ethanol at 100℃; for 0.166667h; Microwave irradiation; | 81% |
(methyl-d3)triphenylphosphonium iodide
4-Phenylbenzaldehyde
4-(vinyl-β,β-d2)-1,1'-biphenyl
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 16h; Cooling; | 100% |
ethane-1,2-dithiol
4-Phenylbenzaldehyde
2-biphenyl-4-yl-1,3-dithiolane
Conditions | Yield |
---|---|
With amberlyst-15 In acetonitrile for 1h; | 99.97% |
With zeolite HSZ-360 In dichloromethane for 15h; Ambient temperature; | 88% |
4-Phenylbenzaldehyde
malononitrile
2-([1,1’-biphenyl]-4-ylmethylene)malononitrile
Conditions | Yield |
---|---|
In ethanol; water for 23h; Knoevenagel condensation; | 99% |
With potassium carbonate In ethanol at 70℃; under 750.075 Torr; for 2.5h; Inert atmosphere; | 99.9% |
With [Cd(2,4,5-tris(pyridin-4-yl)imidazole)(naphthalene-1,5-disulfonate)]n In neat (no solvent) at 20℃; for 24h; Knoevenagel Condensation; Green chemistry; | 97% |
1.3-propanedithiol
4-Phenylbenzaldehyde
2-([1,1'-biphenyl]-4-yl)-1,3-dithiane
Conditions | Yield |
---|---|
With amberlyst-15 In acetonitrile for 1h; | 99.06% |
With hydrogenchloride In benzene Heating; | |
With hydrogenchloride In chloroform for 0.583333h; | |
With boron trifluoride diethyl etherate In dichloromethane Inert atmosphere; | |
With boron trifluoride diethyl etherate In dichloromethane at 0 - 25℃; |
4-Phenylbenzaldehyde
biphenyl-4-carbaldehyde oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium carbonate In methanol; water at 20℃; for 3h; | 99% |
With sodium hydroxide; hydroxylamine hydrochloride In ethanol; water at 25 - 30℃; for 1h; | 98% |
With hydroxylamine hydrochloride; sodium acetate In tetrahydrofuran; ethanol; water at 20℃; for 72h; | 98% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 80℃; for 48h; | 99% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; O-benzenesulfonyl-acetohydroxamic acid ethyl ester In dichloromethane at 23℃; for 24h; Inert atmosphere; | 99% |
With ammonium sulfate; sodium carbonate; sulfur In dimethyl sulfoxide at 120℃; for 10h; Sealed tube; | 99% |
With trifluorormethanesulfonic acid; trimethylsilylazide In acetonitrile at 25℃; for 0.00277778h; Schmidt Reaction; Flow reactor; | 98% |
Conditions | Yield |
---|---|
Stage #1: 4-Phenylbenzaldehyde With zinc diacetate In tetrahydrofuran at 65℃; for 0.166667h; Stage #2: With methyl-di(n-propoxy)silane In tetrahydrofuran at 65℃; for 24h; Stage #3: With hydrogenchloride; water at 0℃; for 1h; | 99% |
With iron(II) fluoro{tris[2-(diphenylphosphino)phenyl]phospino}tetrafluoroborate; hydrogen; trifluoroacetic acid In isopropyl alcohol at 120℃; under 15001.5 Torr; for 2h; Inert atmosphere; Autoclave; chemoselective reaction; | 99% |
With C46H49CoN3P4(2+)*2BF4(1-); hydrogen; potassium hydroxide In ethanol; acetonitrile at 60℃; under 22801.5 Torr; for 24h; Autoclave; Glovebox; chemoselective reaction; | 99% |
4-Phenylbenzaldehyde
Conditions | Yield |
---|---|
With pyridine; hydroxylamine hydrochloride In ethanol at 150℃; for 2.5h; | 99% |
With hydroxylamine hydrochloride; sodium acetate In methanol for 0.5h; Heating; Yield given; |
4-Phenylbenzaldehyde
2-thiomorpholin-4-ylmethyl-phenylamine
Conditions | Yield |
---|---|
With acid Condensation; | 99% |
Conditions | Yield |
---|---|
With potassium tert-butylate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; dirhodium(II) tetrakis(perfluorobutyrate) In tert-Amyl alcohol at 60℃; for 1h; | 99% |
With [(quinone)Rh(COD)]-*K+; water at 75℃; for 3h; | 93% |
BF4(1-)*C14H16O2Rh(1-)*2K(1+) In water at 75℃; for 3h; Conversion of starting material; | 93% |
With potassium phosphate monohydrate; nickel(II) perchlorate hexahydrate In isopropyl alcohol at 80℃; Inert atmosphere; | 89% |
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