Molecular formula: C4H9NO2 Molecular weight: 103.1 99% white powder Appearance:White powder Storage:keep sealed and keep from direct light Package:According to client's requirements Application:pharmaceutical intermediates Transportation:by s
Cas:78191-00-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:78191-00-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:78191-00-1
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryProduct description: Product name N-Methoxy-N-methylacetamide CAS number 78191-00-1 Assay ≥98% Appearance Colorless transparent liquid Capacity 100mt/year Application Pharmac
Cas:78191-00-1
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryFactory supply N-Methoxy-N-methylacetamide CAS 78191-00-1 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Fo
Cas:78191-00-1
Min.Order:10 Kilogram
FOB Price: $10.0
Type:Trading Company
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:78191-00-1
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:78191-00-1
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationships with ma
Cas:78191-00-1
Min.Order:1 Kilogram
FOB Price: $200.0
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:78191-00-1
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryName: N-Methoxy-N-methylacetamide Synonyms: Acetamide, N-methoxy-N-methyl- CAS:78191-00-1 MF: C4H9NO2 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Pharmaceutical Intermediate
Cas:78191-00-1
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:78191-00-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryN-Methoxy-N-methylacetamide CAS:78191-00-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
Cas:78191-00-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:78191-00-1
Min.Order:1 Kilogram
FOB Price: $40.0 / 50.0
Type:Lab/Research institutions
inquiryProduct name: sodium metabisulfite / sodium metabisulphite Molecular weight: 190.10 Specification: 25Kg woven bag Quality guarantee period: 6 months Appearance:white powder/crystal Storage:Store in a cool,dry place and keep away fr
Cas:78191-00-1
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:78191-00-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:78191-00-1
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:78191-00-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:78191-00-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:78191-00-1
Min.Order:100 Gram
Negotiable
Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:78191-00-1
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:78191-00-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirysupplier in China Appearance:clear colorless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used as Pharmaceutical Intermediates Tran
Cas:78191-00-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryN-Methoxy-N-methylacetamide Basic information Product Name: N-Methoxy-N-methylacetamide Synonyms: N-ACETYL-N,O-DIMETHYLHYDROXYLAMINE;N-METHOXY-N-METHYLACETAMIDE;N-METHOXY-N-METHLACETAMIDE;N-Methoxy-N-methylacetamide, 98 %;N-Methoxy-N-methyL;Ac
Cas:78191-00-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:78191-00-1
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Cas:78191-00-1
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryHangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting N-Methoxy-N-methylacetamide,cas:78191-00-1, Please contact us by email freely. We are leading exporter in China. If you really need this cargo, please
Cas:78191-00-1
Min.Order:1 Metric Ton
Negotiable
Type:Other
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:78191-00-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry2-(4-fluorophenyl)-N-methoxy-N-methylacetamide
vinylmagnesium chloride
A
1-(4-fluorophenyl)but-3-en-2-one
B
2-(4-fluorophenyl)-N-methoxyacetamide
D
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: 2-(4-fluorophenyl)-N-methoxy-N-methylacetamide; vinylmagnesium chloride In tetrahydrofuran; toluene at -30℃; for 2h; Stage #2: With acetic anhydride In tetrahydrofuran; toluene at -30℃; for 0.5h; Stage #3: With ammonium chloride In tetrahydrofuran; water; toluene at -30 - 10℃; | A 100% B n/a C n/a D n/a |
N,O-dimethylhydroxylamine*hydrochloride
acetyl chloride
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 1h; | 98% |
With triethylamine In dichloromethane at 0 - 20℃; for 17h; Inert atmosphere; | 83% |
Stage #1: N,O-dimethylhydroxylamine*hydrochloride With triethylamine In dichloromethane at 0℃; for 0.166667h; Inert atmosphere; Stage #2: acetyl chloride In dichloromethane at 0 - 22℃; | 78% |
acetic acid butyl ester
N,O-dimethylhydroxylamine*hydrochloride
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: N,O-dimethylhydroxylamine*hydrochloride With diisobutylaluminium hydride In tetrahydrofuran; toluene Stage #2: acetic acid butyl ester In tetrahydrofuran at 20℃; for 2h; | 91% |
1,1,1-trifluoroacetophenone
A
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: 4,4,4-trifluoro-1-(N-methoxy-N-methylamino)-1-methyl-1-(trimethylsiloxyl)-2-butyne With tetrabutyl ammonium fluoride In tetrahydrofuran; diethyl ether at -15℃; for 0.166667h; Stage #2: 2,2,2-Trifluoroacetophenone In tetrahydrofuran; diethyl ether at 20℃; for 1h; | A n/a B 85% |
N-methoxy-N-methylacetamidine hydroiodide
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
With potassium hydroxide for 2h; Heating; | 62% |
dimethyl sulfate
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
In water at 20℃; for 17h; | 61% |
Methylether von Acetonoxim
A
N-Methoxy-N-methylacetamide
B
3,3,11,11-Tetramethyl-1,2,4,9,10,12-hexaoxa-dispiro[4.2.4.2]tetradecane
Conditions | Yield |
---|---|
With ozone In dichloromethane at 0℃; | A 23% B 9% C 24% |
Methylether von Acetonoxim
1,4-Cyclohexanedione
A
N-Methoxy-N-methylacetamide
B
3,3,11,11-Tetramethyl-1,2,4,9,10,12-hexaoxa-dispiro[4.2.4.2]tetradecane
Conditions | Yield |
---|---|
With ozone In dichloromethane at 0℃; | A 23% B 9% C 24% |
Methylether von Acetonoxim
acetone
A
N-Methoxy-N-methylacetamide
B
3,3,5,5-tetramethyl-1,2,4-trioxolane
Conditions | Yield |
---|---|
With ozone In pentane at 0℃; Yields of byproduct given; | A n/a B 11% |
acetyl chloride
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
With pyridine In chloroform |
2-chloro-N-methoxy-N-methylacetamide
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: 2-chloro-N-methoxy-N-methylacetamide With 3-mercaptophenol; potassium carbonate In N,N-dimethyl-formamide at 23℃; for 2h; Stage #2: With tetra-(n-butyl)ammonium iodide; potassium carbonate; Merrifield resin In N,N-dimethyl-formamide at 50℃; for 2h; Stage #3: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene-d6 at 150℃; for 0.166667h; microwave irradiation; |
A
1-(4-fluorophenyl)but-3-en-2-one
B
2-(4-fluorophenyl)-N-methoxyacetamide
D
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
With acetic anhydride at -30℃; for 0.5h; |
N,O-dimethylhydroxylamine*hydrochloride
acetic acid
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: acetic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 23℃; Stage #2: N,O-dimethylhydroxylamine*hydrochloride With triethylamine In dichloromethane at 0℃; for 2h; |
Conditions | Yield |
---|---|
With sodium hydroxide at 25℃; for 5h; |
N-Methoxy-N-methylacetamide
4-cyclopropyl-4-(2,2-dimethylhydrazono)butan-2-one
Conditions | Yield |
---|---|
Stage #1: 2-(1-cyclopropylethylidene)-1,1-dimethylhydrazine With n-butyllithium; diisopropylamine In tetrahydrofuran; pentane at -78 - 0℃; for 0.583333h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; pentane at -78 - 0℃; for 0.5h; | 100% |
N-(benzylidene)-p-methylbenzenesulfonamide
N-Methoxy-N-methylacetamide
N-methoxy-N-methyl-3-phenyl-3-(tosylamino)propanamide
Conditions | Yield |
---|---|
With triisopropylsilyl trifluoromethanesulfonate; triethylamine In toluene at 20℃; for 12h; Mannich type reaction; | 100% |
N-Methoxy-N-methylacetamide
2-bromo-3-chlorothiophene
1-(5-bromo-3-chlorothiophen-2-yl)ethan-1-one
Conditions | Yield |
---|---|
Stage #1: 2-bromo-3-chlorothiophene With n-butyllithium; diisopropylamine In tetrahydrofuran at -78℃; for 0.5h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran at -78℃; for 0.5h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 3-Ethynylpyridine With ethylmagnesium bromide In tetrahydrofuran; diethyl ether at 0 - 20℃; for 1h; Inert atmosphere; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; diethyl ether at 0 - 20℃; for 18h; Inert atmosphere; | 100% |
triphenylacetaldehyde
N-Methoxy-N-methylacetamide
(RS)-3-hydroxy-N-methoxy-N-methyl-4,4,4-triphenylbutanamide
Conditions | Yield |
---|---|
Stage #1: N-Methoxy-N-methylacetamide With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: triphenylacetaldehyde In tetrahydrofuran; hexane at -78℃; for 0.666667h; Inert atmosphere; | 99% |
N-Methoxy-N-methylacetamide
1-(4,5-dimethylthiazol-2-yl)ethan-1-one
Conditions | Yield |
---|---|
Stage #1: 4,5-Dimethylthiazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 2.16667h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane at -78℃; for 2.16667h; Stage #3: With ammonium chloride In tetrahydrofuran; hexane; water for 0.5h; | 98% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | 98% |
1,1-dimethylethyl 7-bromo-2,3-dihydro-1,4-benzoxazepine-4(5H)-carboxylate
N-Methoxy-N-methylacetamide
1,1-dimethylethyl 7-acetyl-2,3-dihydro-1,4-benzoxazepine-4(5H)-carboxylate
Conditions | Yield |
---|---|
Stage #1: 1,1-dimethylethyl 7-bromo-2,3-dihydro-1,4-benzoxazepine-4(5H)-carboxylate With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane at -78 - 20℃; | 97% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | 96% |
2-lithio-1,3-dithiane
N-Methoxy-N-methylacetamide
1-(1,3-dithian-2-yl)-1-ethanone
Conditions | Yield |
---|---|
With ammonium chloride In tetrahydrofuran at -78 - 0℃; | 95% |
tert-butyl acetoacetate
N-Methoxy-N-methylacetamide
3,5-dioxoheptenoic acid t-butyl ester
Conditions | Yield |
---|---|
Stage #1: tert-butyl acetoacetate With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With n-butyllithium In tetrahydrofuran; hexane; mineral oil at -10℃; for 0.5h; Inert atmosphere; Stage #3: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane; mineral oil at -40 - 20℃; for 2h; Inert atmosphere; | 95% |
With lithium diisopropyl amide In tetrahydrofuran | 93% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | 95% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | 95% |
N-Methoxy-N-methylacetamide
1-benzylaziridine-2-carboxylic acid ethyl ester
1-benzyl-N-methoxy-N-methylaziridine-2-carboxamide
Conditions | Yield |
---|---|
With isopropylmagnesium chloride In tetrahydrofuran Inert atmosphere; | 95% |
5-bromo-1,3-xylene
N-Methoxy-N-methylacetamide
3,5-dimethylacetophenone
Conditions | Yield |
---|---|
Stage #1: 5-bromo-1,3-xylene With iodine; magnesium In tetrahydrofuran at 80℃; for 2h; Inert atmosphere; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran at 80℃; for 2h; | 95% |
7-Bromo-1-fluoronaphthalene
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: 7-Bromo-1-fluoronaphthalene With n-butyllithium In tetrahydrofuran at -70℃; for 1h; Inert atmosphere; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran at -70℃; for 0.333333h; Inert atmosphere; | 95% |
5-methylthiazole
N-Methoxy-N-methylacetamide
1-(5-methylthiazol-2-yl)ethan-1-on
Conditions | Yield |
---|---|
Stage #1: 5-methylthiazole With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran at -78 - 0℃; for 0.6h; Inert atmosphere; | 94% |
Stage #1: 5-methylthiazole With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran at 0℃; for 1.5h; | 51% |
Stage #1: 5-methylthiazole With n-butyllithium In diethyl ether; hexane at -78℃; for 0.25h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; diethyl ether; hexane at 20℃; for 1h; | 43.2% |
Stage #1: 5-methylthiazole With n-butyllithium In diethyl ether at -78℃; for 0.25h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; diethyl ether at -78 - 20℃; |
2-bromo-5-(1-(tert-butyldimethylsilyloxy)-2,2,2-trifluoroethyl)thiazole
N-Methoxy-N-methylacetamide
1-(5-(1-(tert-butyldimethylsilyloxy)-2,2,2-trifluoroethyl)thiazol-2-yl)ethanone
Conditions | Yield |
---|---|
Stage #1: 2-bromo-5-(1-(tert-butyldimethylsilyloxy)-2,2,2-trifluoroethyl)thiazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane at -78℃; for 2h; | 94% |
Stage #1: 2-bromo-5-(1-(tert-butyldimethylsilyloxy)-2,2,2-trifluoroethyl)thiazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane at -78℃; for 2h; | 94% |
Conditions | Yield |
---|---|
Stage #1: n-octyne With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane at 20℃; for 4h; | 93% |
With n-butyllithium In tetrahydrofuran; hexane at -78 - 0℃; for 3.5h; Inert atmosphere; | 86% |
Stage #1: n-octyne With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane at -78 - 20℃; for 4h; Inert atmosphere; | 64% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | 93% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | 93% |
Conditions | Yield |
---|---|
Stage #1: 2-bromobutene With tert.-butyl lithium In diethyl ether; pentane at -78℃; for 1.33333h; Stage #2: N-Methoxy-N-methylacetamide In diethyl ether; pentane at -78℃; for 1h; | 93% |
N-Methoxy-N-methylacetamide
benzaldehyde
N-methoxy-N-methylcinnamamide
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine In dichloromethane for 16h; Mukaiyama Aldol Addition; Inert atmosphere; | 93% |
N-Methoxy-N-methylacetamide
(E)-(2R,3R)-3-Methoxy-6-(4-methoxy-benzyloxy)-2,4-dimethyl-hex-4-enal
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; | 92% |
N-Methoxy-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: 5-bromo-2-((tert-butyldimethylsilyloxy)methyl)-1-methyl-1H-indole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.75h; Inert atmosphere; Stage #2: N-Methoxy-N-methylacetamide In tetrahydrofuran; hexane at -78℃; for 0.166667h; Inert atmosphere; | 92% |
N-Methoxy-N-methylacetamide
2-cyclopropyl-4-(4-fluorophenyl)-3-formylquinoline
N-methoxy-N-methyl3-<2-cyclopropyl-4-(4-fluorophenyl)quinolin-2-yl>-3-hydroxypropanamide
Conditions | Yield |
---|---|
With n-butyllithium; diisopropylamine In tetrahydrofuran | 91% |
With n-butyllithium; diisopropylamine 1.) hexane, THF, -78 deg C, 15 min, 2.) THF, from -78 deg C to RT, 3 h; Yield given. Multistep reaction; |
N-Methoxy-N-methylacetamide
acrolein
3-hydroxypent-4-enoic acid methoxymethylamide
Conditions | Yield |
---|---|
Stage #1: N-Methoxy-N-methylacetamide With lithium diisopropyl amide Stage #2: acrolein at -78℃; | 91% |
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