As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry6-[[(4-methylphenyl)sulphonyl]amino]hexanoic acid CAS:78521-39-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryCorrosion Inhibitor for water based lubricants and functional fluids Appearance:white powder Storage:store in a cool and dry place Package:25kg/bag Application:Corrosion Inhibitor for water based lubricants and functional fluids Transportation
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry6-[[(4-Methylphenyl)sulphonyl]amino]hexanoic acid cas 78521-39-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta
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inquiryBecrosan 2128Appearance:White powder Storage:Ventilation and drying Package:barrel Application:MSA75 is green water-soluble corrosion inhibitor, mainly used in metalworking fluid, circulating water treatment, engine coolant etc. Transportation:By e
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Cas:78521-39-8
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inquiry1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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inquiryp-toluenesulfonyl chloride
6-aminohexanoic acid
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran for 2h; | 95% |
With sodium carbonate In water at 90℃; for 1h; | 80% |
With sodium hydroxide |
caprolactam
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere 1.2: 2 h / -78 - 20 °C / Inert atmosphere 2.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere View Scheme |
toluene-4-sulfonamide
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere 1.2: 2 h / -78 - 20 °C / Inert atmosphere 2.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere View Scheme |
1-(4-Methylbenzene)sulfonyl-2H-hexahydroazepin-2-one
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
With lithium hydroxide In tetrahydrofuran; water at 20℃; for 0.5h; Inert atmosphere; |
methanol
Tosyl-ε-aminocapronsaeure
6-<<(4-Methylphenyl)sulfonyl>amino>hexansaeure-methylester
Conditions | Yield |
---|---|
With sulfuric acid at 25℃; for 48h; | 100% |
Tosyl-ε-aminocapronsaeure
6-(4-methylphenylsulfonamido)hexanamide
Conditions | Yield |
---|---|
With urea at 180 - 200℃; for 4h; | 60% |
Tosyl-ε-aminocapronsaeure
1-(4-Methylbenzene)sulfonyl-2H-hexahydroazepin-2-one
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane Ambient temperature; | 42% |
at 125℃; under 0.01 Torr; | |
With thionyl chloride | |
With phosphorus pentachloride |
Tosyl-ε-aminocapronsaeure
dimethyl sulfate
6-[methyl-(toluene-4-sulfonyl)-amino]-hexanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
Tosyl-ε-aminocapronsaeure
N-Tosyl-ε-aminocapronsaeurechlorid
Conditions | Yield |
---|---|
With thionyl chloride | |
With thionyl chloride for 1h; Heating; |
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0℃; for 0.333333h; Condensation; | |
With dicyclohexyl-carbodiimide In 1,4-dioxane at 0℃; |
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dicyclohexylcarbodiimide / tetrahydrofuran / 0.33 h / 0 °C 2: 4-dimethylaminopyridine / tetrahydrofuran / 0 °C View Scheme |
Tosyl-ε-aminocapronsaeure
N-(5-Amino-pentyl)-4-methyl-benzenesulfonamide; hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 60 percent / urea / 4 h / 180 - 200 °C 2: 70 percent / 1.) phenyliodosyl bis(trifluoroacetate), 2.) HCl conc. / 1.) MeCN-H2O, RT, 6 h, 2.) H2O View Scheme |
Tosyl-ε-aminocapronsaeure
3-(3-Cyano-phenyl)-2-[6-(toluene-4-sulfonylamino)-hexanoylamino]-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h View Scheme |
Tosyl-ε-aminocapronsaeure
3-(4-Cyano-phenyl)-2-[6-(toluene-4-sulfonylamino)-hexanoylamino]-propionic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h View Scheme |
Tosyl-ε-aminocapronsaeure
6-(Toluene-4-sulfonylamino)-hexanoic acid [1-(3-cyano-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-amide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature View Scheme |
Tosyl-ε-aminocapronsaeure
6-(Toluene-4-sulfonylamino)-hexanoic acid [1-(4-cyano-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-amide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature View Scheme |
Tosyl-ε-aminocapronsaeure
6-(Toluene-4-sulfonylamino)-hexanoic acid [2-oxo-2-piperidin-1-yl-1-(3-thiocarbamoyl-benzyl)-ethyl]-amide
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature 5: TEA, H2S / pyridine / 48 h / Ambient temperature View Scheme |
Tosyl-ε-aminocapronsaeure
6-(Toluene-4-sulfonylamino)-hexanoic acid [2-oxo-2-piperidin-1-yl-1-(4-thiocarbamoyl-benzyl)-ethyl]-amide
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature 5: TEA, H2S / pyridine / 48 h / Ambient temperature View Scheme |
Tosyl-ε-aminocapronsaeure
3-(4-Cyano-phenyl)-2-[6-(toluene-4-sulfonylamino)-hexanoylamino]-propionic acid 4-nitro-phenyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h View Scheme |
Tosyl-ε-aminocapronsaeure
3-(3-Cyano-phenyl)-2-[6-(toluene-4-sulfonylamino)-hexanoylamino]-propionic acid 4-nitro-phenyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h View Scheme |
Tosyl-ε-aminocapronsaeure
Nα-Tosyl-(ε-aminocapronyl)-3-amidinophenylalaninpiperididhydroiodid
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature 5: TEA, H2S / pyridine / 48 h / Ambient temperature 6: 0.3 g / acetone / 48 h / Ambient temperature 7: 45 percent / CH3COONH4 / ethanol / 2.5 h / 60 °C View Scheme |
Tosyl-ε-aminocapronsaeure
Nα-Tosyl-(ε-aminocapronyl)-4-amidinophenylalaninpiperididhydroiodid
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature 5: TEA, H2S / pyridine / 48 h / Ambient temperature 6: 0.3 g / acetone / 48 h / Ambient temperature 7: 60 percent / CH3COONH4 / ethanol / 2.5 h / 60 °C View Scheme |
Tosyl-ε-aminocapronsaeure
3-{3-Oxo-3-piperidin-1-yl-2-[6-(toluene-4-sulfonylamino)-hexanoylamino]-propyl}-thiobenzimidic acid methyl ester; hydriodide
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature 5: TEA, H2S / pyridine / 48 h / Ambient temperature 6: 0.3 g / acetone / 48 h / Ambient temperature View Scheme |
Tosyl-ε-aminocapronsaeure
4-{3-Oxo-3-piperidin-1-yl-2-[6-(toluene-4-sulfonylamino)-hexanoylamino]-propyl}-thiobenzimidic acid methyl ester; hydriodide
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: SOCl2 / 1 h / Heating 2: NaOH (1 mol/l) / benzene; H2O / 12 h 3: DCC / pyridine / 24 h 4: pyridine / 24 h / Ambient temperature 5: TEA, H2S / pyridine / 48 h / Ambient temperature 6: 0.3 g / acetone / 48 h / Ambient temperature View Scheme |
Tosyl-ε-aminocapronsaeure
6,6'-<<(4-Methylphenyl)sulfonyl>imino>bishexansaeure
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating View Scheme |
Tosyl-ε-aminocapronsaeure
6,6'-<<(4-Methylphenyl)sulfonyl>imino>bis(hexanoylchlorid)
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating 4: 95 percent / oxalyl chloride / benzene / 48 h / Ambient temperature View Scheme |
Tosyl-ε-aminocapronsaeure
1-<(4-Methylphenyl)sulfonyl>-1,8,15-triazacycloheneicosan
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating 4: 95 percent / oxalyl chloride / benzene / 48 h / Ambient temperature 5: 55 percent / toluene / 0 - 2 °C 6: 1.) 1N BH3, 2.) 6N HCl / 1.) THF, 1 h, room temp., 2 h, reflux, 2.) ethanol, 1 h, reflux View Scheme |
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating View Scheme |
Tosyl-ε-aminocapronsaeure
8-<(4-Methylphenyl)sulfonyl>-1,8,15-triazacycloheneicosan-2,14-dion
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating 4: 95 percent / oxalyl chloride / benzene / 48 h / Ambient temperature 5: 55 percent / toluene / 0 - 2 °C View Scheme |
Tosyl-ε-aminocapronsaeure
8,22-Bis<(4-methylphenyl)sulfonyl>-1,8,15,22-tetraazabicyclo<13.13.6>tetratriacontan
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating 4: 95 percent / oxalyl chloride / benzene / 48 h / Ambient temperature 5: 55 percent / toluene / 0 - 2 °C 6: 1.) 1N BH3, 2.) 6N HCl / 1.) THF, 1 h, room temp., 2 h, reflux, 2.) ethanol, 1 h, reflux 7: 50 percent / triethylamine / benzene; toluene 8: 1.) 1M BH3, 2.) conc. H2SO4 / 1.) THF, 1 h, ice-bath temp. to room temp., 14 h, reflux, 2.) ethanol, reflux View Scheme | |
Multi-step reaction with 6 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating 4: 95 percent / oxalyl chloride / benzene / 48 h / Ambient temperature 5: 50 percent / triethylamine / benzene; toluene 6: 1.) 1M BH3, 2.) conc. H2SO4 / 1.) THF, 1 h, ice-bath temp. to room temp., 14 h, reflux, 2.) ethanol, reflux View Scheme |
Tosyl-ε-aminocapronsaeure
8,22-Bis<(4-methylphenyl)sulfonyl>-1,8,15,22-tetraazabicyclo<13.13.6>tetratriacontan-2,14-dion
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating 4: 95 percent / oxalyl chloride / benzene / 48 h / Ambient temperature 5: 55 percent / toluene / 0 - 2 °C 6: 1.) 1N BH3, 2.) 6N HCl / 1.) THF, 1 h, room temp., 2 h, reflux, 2.) ethanol, 1 h, reflux 7: 50 percent / triethylamine / benzene; toluene View Scheme | |
Multi-step reaction with 5 steps 1: 100 percent / conc. H2SO4 / 48 h / 25 °C 2: potassium t-butylate / 2-methyl-propan-2-ol / 24 h / Heating 3: NaOH / H2O; ethanol / Heating 4: 95 percent / oxalyl chloride / benzene / 48 h / Ambient temperature 5: 50 percent / triethylamine / benzene; toluene View Scheme |
Tosyl-ε-aminocapronsaeure
6-(methylamino)hexanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH-solution 2: hydrochloric acid / 100 °C View Scheme |
Tosyl-ε-aminocapronsaeure
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaOH-solution 2: hydrochloric acid / 100 °C 3: hydrochloric acid View Scheme |
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