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Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water |
mercury(II) diacetate
sodium hydrogen phthalate hemihydrate
acetic acid
A
carbon dioxide
Conditions | Yield |
---|---|
With H2O In water slow evapn. from dilute aq. soln. contg. equimolar amts. of nitrate, diamine and sodium phthalate; |
Conditions | Yield |
---|---|
With H2O In water slow evapn. from dilute aq. soln. contg. equimolar amts. of nitrate, diamine and sodium phthalate; |
Conditions | Yield |
---|---|
With H2O In water slow evapn. from dilute aq. soln. contg. equimolar amts. of nitrate, diamine and sodium phthalate; |
sodium hydrogen phthalate hemihydrate
[29H,31H-phthalocyanine-2,9,16,23-tetrasulfonato(2-)-N29,N30,N31,N32]copper
Conditions | Yield |
---|---|
With NH4Cl; urea In nitrobenzene mixture ground until homogenous, added slowly to nitrobenzene while temp. maintained between 160 and 190°C, heated for further 6 h at 180°C; ground, washed with MeOH, placed in HCl satd. with NaCl, dialysed through a cellulose membrane for 6 days, filtered, concd., refluxed with EtOHfor 2 h, filtered, vacuum dried (E-3 mmHg) at room temp., UV, elem. anal.; |
sodium hydrogen phthalate hemihydrate
copper(II)dihydrate-biphthalate
Conditions | Yield |
---|---|
In water hot soln. of Na salt (distd. H2O) poured to soln. of Cu salt in min. amt. of hot distd. H2O in stoich. ratio; cooled to room temp., ppt. filtered, washed (H2O), dried in air; elem. anal., detd. by TGA; |
sodium hydrogen phthalate hemihydrate
Conditions | Yield |
---|---|
In water hot soln. of Na salt (distd. H2O) poured to soln. of Co salt in min. amt. of hot distd. H2O in stoich. ratio; cooled to room temp., ppt. filtered, washed (H2O), dried in air; elem. anal., detd. by TGA; |
sodium hydrogen phthalate hemihydrate
Conditions | Yield |
---|---|
In water in inert atm.; hot soln. of Na salt (distd. H2O) poured to soln. of Fe salt in min. amt. of hot distd. H2O in stoich. ratio; cooled to room temp., ppt. filtered, washed (H2O), dried in air, recrystd. from H2O; elem. anal., detd. by TGA; |
sodium hydrogen phthalate hemihydrate
Conditions | Yield |
---|---|
In water in inert atm.; hot soln. of Na salt (distd. H2O) poured to soln. of Ni salt in min. amt. of hot distd. H2O in stoich. ratio; cooled to room temp., ppt. filtered, washed (H2O), dried in air; elem. anal., detd. by TGA; |
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