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inquiryGood quality Tris(4-Methoxyphenyl)Phosphine CAS 855-38-9 with competitive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates,
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inquiryHigh purity CAS 855-38-9 TRIS(4-METHOXYPHENYL)PHOSPHINE in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
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inquiryName Tris(p-methoxyphenyl)phosphine Structural Formula CAS No. 855-38-9 Molecular Formula
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inquiryProduct Name: TRIS(4-METHOXYPHENYL)PHOSPHINE CAS: 855-38-9 MF: C21H21O3P MW: 352.36 EINECS: 212-723-0 Mol File: 855-38-9.mol Melting point 131-134 °C (lit.) Boiling point 457.8±40.0 °C(Predicted) density
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryConditions | Yield |
---|---|
With chloro-trimethyl-silane; tetrabutylammomium bromide; copper; zinc In acetonitrile at 45℃; Electrochemical reaction; Inert atmosphere; | 93% |
With chloro-trimethyl-silane; magnesium at 20℃; for 2h; | 93% |
With oxalyl dichloride; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; triethylamine In dichloromethane at 40℃; for 2h; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With phosphorus trichloride | 89% |
Stage #1: 1-bromo-4-methoxy-benzene With magnesium In tetrahydrofuran at 42 - 55℃; for 2h; Stage #2: With phosphorus trichloride In tetrahydrofuran at 25 - 85℃; for 3.5h; Stage #3: With hydrogenchloride In tetrahydrofuran; water for 1.5h; | 75.62% |
Stage #1: 1-bromo-4-methoxy-benzene With n-butyllithium In tetrahydrofuran; hexane at -50℃; for 0.5h; Inert atmosphere; Stage #2: With phosphorus trichloride In tetrahydrofuran; hexane at -50 - -10℃; Inert atmosphere; | 55% |
(4-methoxyphenyl)zinc(II) bromide
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
With phosphorus trichloride In acetonitrile at 20℃; for 2h; | 45% |
4-methoxyphenyl magnesium bromide
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
With diethyl ether; hydrogen; phosphorus trichloride |
p-methoxyphenyllithium
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
With phosphorus trichloride at -20℃; Yield given; |
(2-quinaldinate)(carbonyl)(P(4-CH3O-C5H4)3)2rhodium(I)
(2-quinaldinate)(carbonyl)(P(4-CH3O-C5H4)3)rhodium(I)
B
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In not given 24 h; |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
With 4-phenylthioxanthone In methanol at 20℃; under 760.051 Torr; for 0.666667h; Mechanism; Solvent; Irradiation; | 100% |
With potassium permanganate | 99% |
With gold(III) complex supported on cellulose extracted from Carthamus tinctorius immobilized on nanofibrous phosphosilicate; air at 20℃; for 1h; Irradiation; | 98% |
Conditions | Yield |
---|---|
With palladium diacetate In benzene at 120℃; for 25h; | 100% |
P(p-CH3OC6H4)3
tris(4-methoxyphenyl)phosphine selenide
Conditions | Yield |
---|---|
With selenium In toluene for 6h; Heating; | 100% |
With selenium In toluene at 90℃; | 97% |
With selenium In ethanol Heating; |
P(p-CH3OC6H4)3
B
[(η5-C5H4Me)Fe(CO)2P(p-C6H4OMe)3]I
Conditions | Yield |
---|---|
di(cyclopentadienideiron dicarbonyl) In neat (no solvent) Fe-compound and P-compound placed in 1:5 molar ratio in agate mortar; gently ground; transferred into NMR tube; placed at 100°C for 15 min; chilled in ice; | A 0% B 100% |
In neat (no solvent) Fe-compound and P-compound placed in 1:5 molar ratio in agate mortar; gently ground; transferred into NMR tube; placed at 70°C for 0.5 or4 min; chilled in ice; | A 0% B 100% |
di(cyclopentadienideiron dicarbonyl) In neat (no solvent) Fe-compound and P-compound placed in 1:5 molar ratio in agate mortar; gently ground; transferred into NMR tube; placed at 100°C for 5 min; chilled in ice; | A 0% B 84% |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
With tetrafluoroboric acid In diethyl ether at 20℃; Inert atmosphere; | 100% |
(tetrahydrothiophene)gold(I) chloride
P(p-CH3OC6H4)3
(tris(4-methoxyphenyl)phosphine)gold(I) chloride
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 15h; Inert atmosphere; | 100% |
In dichloromethane at 20℃; for 1h; | 63% |
In not given addn. of P compd. to Au complex; |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In toluene at 20℃; Inert atmosphere; Schlenk technique; | 99.5% |
P(p-CH3OC6H4)3
1-adamantyl isocyanide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; | 99% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3h; Inert atmosphere; | 99% |
P(p-CH3OC6H4)3
methyl 4-azidotetrafluorobenzoate
Conditions | Yield |
---|---|
at 25℃; for 2h; Kinetics; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In chloroform at 60℃; for 24h; Schlenk technique; Inert atmosphere; | 99% |
P(p-CH3OC6H4)3
3-hydroxy-4-iodopyridine
Conditions | Yield |
---|---|
In chloroform at 50℃; for 19h; | 99% |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In chloroform at 80℃; for 19h; | 99% |
P(p-CH3OC6H4)3
5-bromo-2-chloro-4-iodopyridine
Conditions | Yield |
---|---|
In chloroform at 80℃; for 19h; | 99% |
Conditions | Yield |
---|---|
In chloroform at 20℃; for 36h; | 99% |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In dichloromethane dropping of soln. of phosphane derivative to soln. of Pt complex then stirring at 0°C for 6 h; evapg. of solvent, hydrolysing with ice water, sepg., extg. of aq. layer with C6H6 then CH2Cl2, washing with H2O, drying over MgSO4, evapg. to dryness, dissolving in CH2Cl2 then pptg. with n-hexane; elem. anal.; | 98% |
allyl(cyclopentadiene)palladium(II)
4-fluoro-1-iodobenzene
P(p-CH3OC6H4)3
(4-fluorophenyl)Pd(P(4-methoxyphenyl)3)2I
Conditions | Yield |
---|---|
In dichloromethane Ar-atmosphere; stirring (room temp., 5 - 15 min); filtering (PTFE membrane), crystn. on concg. and hexane addn. (-30°C, overnight), filtering, drying (vac.); elem. anal.; | 98% |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In dichloromethane (Ar); stirring a soln. of cobalt complex and phosphine in CH2Cl2 at roomtemp. for 5 min; evapn., column chromy.; | 98% |
Conditions | Yield |
---|---|
In toluene for 5h; Reflux; | 98% |
(tris(4-methoxyphenyl)phosphine)gold(I) chloride
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In dichloromethane for 1h; Darkness; | 98% |
3-chloro-4 iodopyridine
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In chloroform at 20℃; for 36h; | 98% |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In chloroform at 50℃; for 19h; | 98% |
Conditions | Yield |
---|---|
In dichloromethane at 25℃; for 15h; Inert atmosphere; | 98% |
allyl(cyclopentadiene)palladium(II)
4-tolyl iodide
P(p-CH3OC6H4)3
(4-methylphenyl)Pd(P(4-methoxyphenyl)3)2I
Conditions | Yield |
---|---|
In dichloromethane Ar-atmosphere; stirring (room temp., 5 - 15 min); filtering (PTFE membrane), crystn. on concg. and hexane addn. (-30°C, overnight), filtering, drying (vac.); elem. anal.; | 97% |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In dichloromethane solid P(C6H4OMe-p)3 added at room temp.to a suspn. of Au-complex, stirred for 1 h; concd., Et2O added, filtered off, recrystd. from CH2Cl2-Et2O; elem. anal.; | 96% |
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: CO; Irradiation (UV/VIS); (Ar); irradn. of a soln. of chromium complex and phosphine in THF at -20°C for 2.5 h; evapn., chromy. (silica gel, pentane/CH2Cl2/THF); elem. anal.; | 96% |
ferrocenium(III) tetrafluoroborate
dichloromethane
(OC)3Fe((CH2)3S2)Ni(Ph2P(CH2)2PPh2)
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
With pentane In dichloromethane MBraun glovebox, under N2; soln. of NiFe compd. and FcBF4 in CH2Cl2, rapid stirring for 1 min, above soln. added to phosphine in CH2Cl2, 0.5 min, pentane added (-28°C, then 1 h at this temp.); filtered, washed (pentane, -28°C), dried; elem. anal.; | 96% |
dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II)
P(p-CH3OC6H4)3
Conditions | Yield |
---|---|
With trimethylamine-N-oxide In dichloromethane; acetonitrile at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 96% |
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