Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryItems Standard Result Assay (Ursolic acid) 98%min -------------------------------------------------------------------------------
Cas:895152-66-6
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanoneCAS: 895152-66-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, spec
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:895152-66-6
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:895152-66-6
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inquiryProName:High purity (1H-indol-3-yl)(2,2,3,3-te... CasNo:895152-66-6 Molecular Formula:C16H19NO Appearance:white powder Application:INTERMEDIATE DeliveryTime:Prompt PackAge:By foil-alum bag or pap Port:Shanghai ProductionCapacity:99999 Gram
Cas:895152-66-6
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:895152-66-6
Min.Order:10 Gram
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:895152-66-6
Min.Order:100 Gram
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inquiryProduct Name: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone Synonyms: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone;tert-butyl 4-acetoxy-octahydroindole-1-carboxylate CAS: 895152-66-6 MF: C16H19NO MW: 241.32816 EINECS: P
Cas:895152-66-6
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:895152-66-6
Min.Order:1 Milligram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:895152-66-6
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inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:895152-66-6
Min.Order:1 Kilogram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:895152-66-6
Min.Order:1 Gram
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Material Sourcing): (
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:895152-66-6
Min.Order:1 Metric Ton
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inquirySAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:895152-66-6
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Cas:895152-66-6
Min.Order:1 Kilogram
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Type:Other
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:895152-66-6
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:895152-66-6
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inquiryindole
2,2,3,3-tetramethylcyclopropanecarbonyl chloride
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: indole With zirconium(IV) chloride In dichloromethane at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: 2,2,3,3-tetramethylcyclopropanecarbonyl chloride In dichloromethane at 0℃; for 4h; Inert atmosphere; | 85% |
2,2,3,3-tetramethylcyclopropanecarbonyl chloride
A
1-[(2,2,3,3-tetramethylcyclopropyl)carbonyl]-1H-indole
B
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: indole With ethylmagnesium bromide In tetrahydrofuran; dichloromethane at 20℃; for 0.25h; Stage #2: With zinc(II) chloride In tetrahydrofuran; dichloromethane at 20℃; for 0.5h; Stage #3: 2,2,3,3-tetramethylcyclopropanecarbonyl chloride In tetrahydrofuran; dichloromethane at 20℃; for 6h; | A 27% B 42% |
indole
2,2,3,3-tetramethylcyclopropanecarbonyl chloride
A
1-[(2,2,3,3-tetramethylcyclopropyl)carbonyl]-1H-indole
B
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
With ethylmagnesium bromide; zinc(II) chloride | |
Stage #1: indole With ethylmagnesium bromide In tetrahydrofuran; dichloromethane at 20℃; for 0.25h; Stage #2: With zinc(II) chloride In tetrahydrofuran; diethyl ether; dichloromethane for 0.5h; Stage #3: 2,2,3,3-tetramethylcyclopropanecarbonyl chloride In tetrahydrofuran; diethyl ether; dichloromethane at 20℃; for 6h; Further stages.; | A 6.1 g B 9.7 g |
Stage #1: indole With ethylmagnesium bromide In tetrahydrofuran; dichloromethane at 21℃; Stage #2: With zinc(II) chloride In tetrahydrofuran; diethyl ether; dichloromethane for 0.5h; Stage #3: 2,2,3,3-tetramethylcyclopropanecarbonyl chloride In tetrahydrofuran; diethyl ether; dichloromethane at 21℃; for 6h; | A 6.1 g B 9.7 g |
2,2,3,3-tetramethylcyclopropane-1-carboxylic acid
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: thionyl chloride / 2 h / Reflux 2.1: ethylmagnesium bromide / tetrahydrofuran; dichloromethane / 21 °C 2.2: 0.5 h 2.3: 6 h / 21 °C View Scheme |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
propyl bromide
(1-propyl-1H-indol-3-yl)-(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: propyl bromide In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 97% |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
benzyl bromide
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: benzyl bromide In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 92% |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
1-Bromopentane
((1-pentyl-1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone)
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 1-Bromopentane In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 91% |
1-bromo-butane
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
(1-butyl-1H-indol-3-yl)-(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 1-bromo-butane In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 89% |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
N,N-diallyl-2-bromoacetamide
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 1.5h; Schlenk technique; | 85% |
5-bromo-1,2-epoxypentane
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With potassium tert-butylate In tetrahydrofuran; N,N-dimethyl-formamide at 0℃; for 0.25h; Stage #2: 5-bromo-1,2-epoxypentane In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 16h; | 75% |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Methyl 3-bromopropionate
methyl 3-(3-(2,2,3,3-tetramethylcyclopropanecarbonyl)-1H-indol-1-yl)propanoate
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: Methyl 3-bromopropionate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 55% |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
6-chloro-2-hexanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 6-chloro-2-hexanone In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 15% |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
3-chloropropionamide
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 3-chloropropionamide In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 13% |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
2-(morpholin-1-yl)ethyl methanesulfonate
Conditions | Yield |
---|---|
With sodium hydride | |
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; Stage #2: 2-(morpholin-1-yl)ethyl methanesulfonate In N,N-dimethyl-formamide at 45℃; Further stages.; | 6.6 g |
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(morpholin-1-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 6.6 g |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
4-(methanesulfonyloxymethyl)tetrahydropyran
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; Stage #2: 4-(methanesulfonyloxymethyl)tetrahydropyran In N,N-dimethyl-formamide at 45℃; for 2h; Further stages.; | 0.19 g |
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 4-(methanesulfonyloxymethyl)tetrahydropyran In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.19 g |
(tetrahydrofuran-3-yl)methyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: (tetrahydrofuran-3-yl)methyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.16 mg |
2-(tetrahydro-2H-pyran-4-yl)ethyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(tetrahydro-2H-pyran-4-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.36 mg |
2-(pyridin-4-yl)ethyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(pyridin-4-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 42 mg |
2-(tetrahydro-2H-pyran-4-yl)acetyl chloride
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(tetrahydro-2H-pyran-4-yl)acetyl chloride In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.16 g |
tert-butyl 4-(2-((methylsulfonyl)oxy)ethyl)piperazine-1-carboxylate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: tert-butyl 4-(2-((methylsulfonyl)oxy)ethyl)piperazine-1-carboxylate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.22 g |
methanesulfonic acid 3-morpholin-4-yl-propyl ester
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: methanesulfonic acid 3-morpholin-4-yl-propyl ester In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.15 g |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: methanesulfonic acid 2-pyrrolidin-1-ylethyl ester In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 45 mg |
2-(azepan-1-yl)ethyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(azepan-1-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.19 g |
2-(1-methylpyrrolidin-2-yl)ethyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(1-methylpyrrolidin-2-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 85 mg |
(S)-(tetrahydrofuran-2-yl)methyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: (S)-(tetrahydrofuran-2-yl)methyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.23 mg |
(R)-(tetrahydrofuran-2-yl)methyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: (R)-(tetrahydrofuran-2-yl)methyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.28 mg |
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
(1,3-dioxolan-2-yl)methyl methanesulfonate
(1-((1,3-dioxolan-2-yl)methyl)-1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: (1,3-dioxolan-2-yl)methyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.27 g |
2-(2-oxooxazolidin-3-yl)ethyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(2-oxooxazolidin-3-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.2 g |
2-(2-oxopyrrolidin-1-yl)ethyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(2-oxopyrrolidin-1-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.12 g |
2-(2,5-dioxopyrrolidin-1-yl)ethyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 2-(2,5-dioxopyrrolidin-1-yl)ethyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 60 mg |
4,4,4-trifluorobutyl methanesulfonate
(1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone
Conditions | Yield |
---|---|
Stage #1: (1H-indol-3-yl)(2,2,3,3-tetramethylcyclopropyl)methanone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: 4,4,4-trifluorobutyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 45℃; | 0.19 g |
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