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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

6-Chloro-2-hexanone Manufacturer/High quality/Best price/In stock

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 6-chlorohexan-2-one

Cas:10226-30-9

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-Chloro-5-hexanone

Cas:10226-30-9

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

6-Chloro-2-hexanone Basic information Product Name: 6-Chloro-2-hexanone Synonyms: 1-CHLORO-5-HEXANONE;1-CHLOROHEXAN-5-ONE;4-CHLOROBUTYL METHYL KETONE;6-CHLOROHEXAN-2-ONE;6-CHLORO-2-H

6-Chloro-2-hexanone 10226-30-9

Cas:10226-30-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

High Quality 6-Chloro-2-Hexanone Price CAS 10226-30-9

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Discount price CAS 10226-30-9 with best quality

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name: 6-Chloro-2-hexanone Synonyms: 1-CHLORO-5-HEXANONE;1-CHLOROHEXAN-5-ONE;4-CHLOROBUTYL METHYL KETONE;6-CHLOROHEXAN-2-ONE;6-CHLORO-2-HEXANONE;1-Chlorohexane-5-one;Chlorohexanone;6-CHLORO-2-HEXANON

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Appearance:Clear yellow to brown liquid Storage:room temperature Package:200kg/drum Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

6-Chloro-2-hexanone Manufacturer CAS:10226-30-9

Cas:10226-30-9

Min.Order:10 Gram

Negotiable

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

6-Chloro-2-hexanone 10226-30-9

Cas:10226-30-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

6-Chloro-2-hexanone CAS:10226-30-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter

6-Chloro-2-hexanone CAS:10226-30-9

Cas:10226-30-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

6-Chloro-2-hexanone/ LIDE PHARMA- Factory supply / Best price

Cas:10226-30-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

6-Chloro-2-hexanone cas 10226-30-9

Cas:10226-30-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $30.0 / 110.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Xinhao Biotechnology Co., Ltd.

Our Strengths 1.Place of Origin China with Super quality by reasonable price. 2.Fast delivery by safe express way to all the country. 3.Has a number of highly qualified engineers and experts to provide guidance for reagents. 4.When you meet problems

Factory supply 6-Chloro-2-hexanone with Good Price CAS NO.10226-30-9

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $10.0

Type:Trading Company

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 6-Chloro-2-Hexanone

Cas:10226-30-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colorless oil liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:For medicine , pesticide intermedi

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best Offer6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

6-chloro-2-hexanone

Cas:10226-30-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

6-Chloro-2-hexanone

Cas:10226-30-9

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Synthetic route

1-methylcyclopentanol
1462-03-9

1-methylcyclopentanol

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With sodium hydrogencarbonate; iron(II) sulfate In tetrachloromethane Ambient temperature; in the dark;100%
With lead(IV) acetate; lithium chloride at 20 - 35℃; for 4h; Oxidation; oxidative decyclization; mechanical activation;51%
(i) aq. NaOCl, (ii) AgNO3, NaOH, aq. NH3; Multistep reaction;
6-chlorohexene
928-89-2

6-chlorohexene

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With copper(l) iodide; oxygen; palladium dichloride In water; N,N-dimethyl-formamide for 48h;99%
1-chloro-5-hexyne
10297-06-0

1-chloro-5-hexyne

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With (cyclohexylisocyanide)gold(I) chloride; water; potassium tetrakis(pentafluorophenyl)borate In methanol at 20℃; for 24h; Reagent/catalyst;99%
With methanol; [Co((dimethylglyoximate)BF2)2•2H2O] at 65℃; for 2.5h; Sealed tube; Neutral conditions; regioselective reaction;98%
With silver hexafluoroantimonate; SPGS-550-M; NOK; C35H47O3P*Au(1+)*Cl(1-); trifluoroacetic acid In water; toluene at 20℃; for 24h; Green chemistry;90%
2-methyl-5,6-dihydro-4H-pyran-3-carboxylic acid methyl ester
57987-84-5

2-methyl-5,6-dihydro-4H-pyran-3-carboxylic acid methyl ester

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With hydrogenchloride at 50℃; for 3h;93%
1-methylcyclopentyl hypochlorite
33694-90-5

1-methylcyclopentyl hypochlorite

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
In tetrachloromethane at 70℃; for 6h; Irradiation;90%
at 40℃;
6-chloro-2-methoxy-1-hexene

6-chloro-2-methoxy-1-hexene

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With hydrogenchloride In tetrahydrofuran for 0.5h; Heating;85%
N'-[5-Chloro-1-methyl-pent-(Z)-ylidene]-N,N-dimethyl-hydrazine
876384-79-1

N'-[5-Chloro-1-methyl-pent-(Z)-ylidene]-N,N-dimethyl-hydrazine

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With water; copper dichloride In tetrahydrofuran; phosphoric acid84%
With boron trifluoride diethyl etherate In water; acetone64%
5-(1-Amino-5-chloro-pentylidene)-2,2-dimethyl-[1,3]dioxane-4,6-dione
77570-29-7

5-(1-Amino-5-chloro-pentylidene)-2,2-dimethyl-[1,3]dioxane-4,6-dione

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With hydrogenchloride Heating;73%
1-methylcyclopentanol
1462-03-9

1-methylcyclopentanol

A

1-methyl-1,4-epoxycyclopentane

1-methyl-1,4-epoxycyclopentane

B

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With pyridine; lead(IV) acetate; lithium chloride In benzene at 80℃; for 5h;A 15%
B 70%
Methyltriphenylphosphonium bromide
1779-49-3

Methyltriphenylphosphonium bromide

4-Chloro-N,O-dimethylbutyric acid amide
138344-21-5

4-Chloro-N,O-dimethylbutyric acid amide

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; hexane at -15℃;
Stage #2: 4-Chloro-N,O-dimethylbutyric acid amide In tetrahydrofuran; hexane at -78 - 20℃; Wittig reaction;
Stage #3: With hydrogenchloride In tetrahydrofuran; diethyl ether; hexane at 20℃;
68%
6-chloro-2-hexanol
18804-33-6

6-chloro-2-hexanol

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With C44H66O8P4Pd2; methyl vinyl ketone In water; toluene at 105℃; for 16h; Inert atmosphere; chemoselective reaction;65%
With pyridinium chlorochromate
2,3-dimethyl-2,3-butane diol
76-09-5

2,3-dimethyl-2,3-butane diol

6-chlorohexene
928-89-2

6-chlorohexene

A

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

B

2-(5-chloropentyl)-4,4,5,5-tetramethyl-1,3-dioxolane

2-(5-chloropentyl)-4,4,5,5-tetramethyl-1,3-dioxolane

Conditions
ConditionsYield
With dichloro bis(acetonitrile) palladium(II); oxygen; 2-Methyl-1,4-benzoquinone; copper(l) chloride; tert-butyl alcohol at 40℃; under 760.051 Torr; for 3h;A 8 %Spectr.
B 60%
6-chlorohexene
928-89-2

6-chlorohexene

A

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

B

6-chloro-2-hexanol
18804-33-6

6-chloro-2-hexanol

Conditions
ConditionsYield
With dichloro bis(acetonitrile) palladium(II); 1-hydroxytetraphenyl-cyclopentadienyl(tetraphenyl-2,4-cyclopentadien-1-one)-μ-hydrotetracarbonyldiruthenium(II); water; p-benzoquinone In methanol; isopropyl alcohol at 85℃; for 48h; Inert atmosphere; Glovebox; regioselective reaction;A 40%
B 9 %Spectr.
6-hydroxy-2-hexanone
21856-89-3

6-hydroxy-2-hexanone

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With hydrogenchloride; water
1-methyl-cyclopentyl hydroperoxide
27115-55-5

1-methyl-cyclopentyl hydroperoxide

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With hydrogenchloride; iron(II) sulfate In water
N-isopropyliden-cyclohexyl amine
6407-36-9

N-isopropyliden-cyclohexyl amine

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
(i) LiNEt2, THF, (ii) /BRN= 605278/, (iii) aq. HCl; Multistep reaction;
With n-butyllithium 1.) THF; Yield given. Multistep reaction;
1,3-Dioxolan-2-buttersaeure-ethylester
38049-07-9

1,3-Dioxolan-2-buttersaeure-ethylester

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With hydrogenchloride; lithium aluminium tetrahydride 1) ether, 4 h, room temp.; 30 min., reflux; 2) 2 h, reflux; Yield given. Multistep reaction;
5-chloro-2-(1-methylethenyl)pentanoic acid
194920-91-7

5-chloro-2-(1-methylethenyl)pentanoic acid

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
With pyridine; dimethylsulfide; ozone 1.) dichloromethane, -70 deg C, 2.) dichloromethane, room temperature, 15 h; Yield given. Multistep reaction;
5-chloro-2-(1-methylethenyl)pentanoic acid
194920-91-7

5-chloro-2-(1-methylethenyl)pentanoic acid

A

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

B

6-chloro-3-methylene-2-hexanone
89118-09-2

6-chloro-3-methylene-2-hexanone

Conditions
ConditionsYield
With ozone; triethylamine 1.) dichloromethane, -70 deg C, 2.) dichloromethane, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
6-chloro-2-(1-methylethenyl)hexanoic acid
194920-99-5

6-chloro-2-(1-methylethenyl)hexanoic acid

A

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

B

7-chloroheptan-2-one
4630-77-7

7-chloroheptan-2-one

Conditions
ConditionsYield
With pyridine; dimethylsulfide; ozone 1.) dichloromethane, -70 deg C, 2.) dichloromethane, room temperature, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
7-chloro-2-(1-methylethenyl)heptanoic acid

7-chloro-2-(1-methylethenyl)heptanoic acid

A

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

B

8-chloro-octan-2-one
72978-95-1

8-chloro-octan-2-one

Conditions
ConditionsYield
With pyridine; dimethylsulfide; ozone 1.) dichloromethane, -70 deg C, 2.) dichloromethane, room temperature, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
5-Chlorovaleroyl chloride
1575-61-7

5-Chlorovaleroyl chloride

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 70 percent / tetrahydrofuran / -78 °C
2.1: n-BuLi / tetrahydrofuran; hexane / -15 °C
2.2: tetrahydrofuran; hexane / -78 - 20 °C
2.3: 68 percent / aq. HCl / tetrahydrofuran; hexane; diethyl ether / 20 °C
View Scheme
5-chloro-pentanal
20074-80-0

5-chloro-pentanal

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: pyridinium chlorochromate
View Scheme
propylamine
107-10-8

propylamine

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

calcium carbide
75-20-7

calcium carbide

2-ethynyl-2-methyl-1-propylpiperidine

2-ethynyl-2-methyl-1-propylpiperidine

Conditions
ConditionsYield
Stage #1: propylamine; 6-chloro-2-hexanone; calcium carbide With copper(l) iodide; triethylamine In water; acetonitrile at 60℃; for 24h;
Stage #2: In water; acetonitrile for 2h; Reagent/catalyst; Solvent;
99%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

1-iodo-5-hexanone
4367-98-0

1-iodo-5-hexanone

Conditions
ConditionsYield
With sodium iodide In acetone at 60℃; for 12h; Sealed tube;97%
With sodium iodide In acetone at 60℃;87%
With sodium iodide In acetone
With sodium iodide In acetone Heating;
N-Methylpyrrole
96-54-8

N-Methylpyrrole

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

3-(5-chloro-1-methylpentyl)-1-methyl-1H-pyrrole
1152705-89-9

3-(5-chloro-1-methylpentyl)-1-methyl-1H-pyrrole

Conditions
ConditionsYield
With triethylsilane; indium(III) tris[bis(trifluoromethanesulfonyl)amide] In 1,4-dioxane at 85℃; for 5h; Schlenk technique; Inert atmosphere; regioselective reaction;97%
With triethylsilane; bis(trifluoromethanesulfonyl)amide In 1,4-dioxane at 100℃; for 10h; Schlenk technique; Inert atmosphere; regioselective reaction;86%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

calcium carbide
75-20-7

calcium carbide

phenethylamine
64-04-0

phenethylamine

2-ethynyl-2-methyl-1-phenethylpiperidine

2-ethynyl-2-methyl-1-phenethylpiperidine

Conditions
ConditionsYield
Stage #1: 6-chloro-2-hexanone; calcium carbide; phenethylamine With copper(l) iodide; triethylamine In water; acetonitrile at 60℃; for 24h;
Stage #2: In water; acetonitrile for 2h; Reagent/catalyst;
96%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-amino-N'-(2,4-dichlorophenyl)benzohydrazide

2-amino-N'-(2,4-dichlorophenyl)benzohydrazide

2-(4-chlorobutyl)-3-((2,4-dichlorophenyl)amino)-2-methyl-2,3-dihydroquinazolin-4(1H)-one

2-(4-chlorobutyl)-3-((2,4-dichlorophenyl)amino)-2-methyl-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With iodine; 1-n-butyl-3-methylimidazolim bromide at 80℃; for 15h; Reagent/catalyst; Temperature; Ionic liquid; Green chemistry; chemoselective reaction;93%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

6-azido-2-hexanone
84702-77-2

6-azido-2-hexanone

Conditions
ConditionsYield
With sodium azide; sodium iodide In dimethyl sulfoxide at 55℃; for 18h;92%
With sodium azide; sodium iodide In N,N-dimethyl-formamide at 80℃; for 5h; Inert atmosphere;81%
With sodium azide; sodium iodide In N,N-dimethyl-formamide at 80℃;67%
With sodium azide; sodium iodide In N,N-dimethyl-formamide at 80℃; for 2h; Inert atmosphere;59%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

5-(2-aminophenyl)-1H-pyrazole
111562-32-4

5-(2-aminophenyl)-1H-pyrazole

C15H17N3

C15H17N3

Conditions
ConditionsYield
With acetic acid for 4h; Reflux;92%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

C13H11Cl2N3O

C13H11Cl2N3O

6-chloro-2-(4-chlorobutyl)-3-((4-chlorophenyl)amino)-2-methyl-2,3-dihydroquinazolin-4(1H)-one

6-chloro-2-(4-chlorobutyl)-3-((4-chlorophenyl)amino)-2-methyl-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With iodine; 1-n-butyl-3-methylimidazolim bromide at 80℃; for 14h; Ionic liquid; Green chemistry; chemoselective reaction;92%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

7-Ethyl-3,8-dimethyl-3,7-dihydro-purine-2,6-dione
131598-86-2

7-Ethyl-3,8-dimethyl-3,7-dihydro-purine-2,6-dione

7-Ethyl-3,8-dimethyl-1-(5-oxo-hexyl)-3,7-dihydro-purine-2,6-dione

7-Ethyl-3,8-dimethyl-1-(5-oxo-hexyl)-3,7-dihydro-purine-2,6-dione

Conditions
ConditionsYield
With sodium ethanolate In N,N-dimethyl-formamide at 125℃; for 4h;91%
phthalimide
136918-14-4

phthalimide

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-(5-oxohexyl)-1H-isoindole-1,3(2H)-dione
71510-41-3

2-(5-oxohexyl)-1H-isoindole-1,3(2H)-dione

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 100℃; for 12h;91%
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 100℃; for 18h;73.2%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-amino-N'-phenylbenzohydrazide
30086-49-8

2-amino-N'-phenylbenzohydrazide

2-(4-chlorobutyl)-2-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

2-(4-chlorobutyl)-2-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With iodine; 1-n-butyl-3-methylimidazolim bromide at 80℃; for 15h; Ionic liquid; Green chemistry; chemoselective reaction;91%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

C13H12ClN3O
216311-70-5

C13H12ClN3O

7-chloro-2-(4-chlorobutyl)-2-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

7-chloro-2-(4-chlorobutyl)-2-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With iodine; 1-n-butyl-3-methylimidazolim bromide at 80℃; for 13h; Ionic liquid; Green chemistry; chemoselective reaction;91%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

C9H17ClO

C9H17ClO

Conditions
ConditionsYield
With manganese; TiCpCl2 In tetrahydrofuran at 20℃; for 2h; Inert atmosphere;91%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

7-benzyl-3-methylxanthine
56025-86-6

7-benzyl-3-methylxanthine

7-benzyl-3-methyl-1-(5-oxohexyl)-xanthine

7-benzyl-3-methyl-1-(5-oxohexyl)-xanthine

Conditions
ConditionsYield
90.4%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-amino-N-(4-methoxyphenyl)benzamide
20878-54-0

2-amino-N-(4-methoxyphenyl)benzamide

5-(4-methoxyphenyl)-4a-methyl-3,4,4a,5-tetrahydro-1H-pyrido[1,2-a]quinazolin-6(2H)-one

5-(4-methoxyphenyl)-4a-methyl-3,4,4a,5-tetrahydro-1H-pyrido[1,2-a]quinazolin-6(2H)-one

Conditions
ConditionsYield
With iodine at 80℃; for 8h; Ionic liquid;90%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

C14H14ClN3O

C14H14ClN3O

2-(4-chlorobutyl)-3-((3-chlorophenyl)amino)-2,8-dimethyl-2,3-dihydroquinazolin-4(1H)-one

2-(4-chlorobutyl)-3-((3-chlorophenyl)amino)-2,8-dimethyl-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With iodine; 1-n-butyl-3-methylimidazolim bromide at 80℃; for 11h; Ionic liquid; Green chemistry; chemoselective reaction;90%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

C14H11N3O2

C14H11N3O2

9a-methyl-7,8,9,9a-tetrahydro-6H-benzo[4,5]imidazo[1,2-c][1,3]dioxolo[4,5-g]pyrido[1,2-a]quinazoline

9a-methyl-7,8,9,9a-tetrahydro-6H-benzo[4,5]imidazo[1,2-c][1,3]dioxolo[4,5-g]pyrido[1,2-a]quinazoline

Conditions
ConditionsYield
With iodine at 80℃; for 9h; Ionic liquid;90%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

3-Ethyl-7,8-dimethyl-3,7-dihydro-purine-2,6-dione
131598-99-7

3-Ethyl-7,8-dimethyl-3,7-dihydro-purine-2,6-dione

3-Ethyl-7,8-dimethyl-1-(5-oxo-hexyl)-3,7-dihydro-purine-2,6-dione

3-Ethyl-7,8-dimethyl-1-(5-oxo-hexyl)-3,7-dihydro-purine-2,6-dione

Conditions
ConditionsYield
With sodium ethanolate In N,N-dimethyl-formamide at 125℃; for 4h;89%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-amino-N-(p-methoxybenzyl)benzamide
221539-30-6

2-amino-N-(p-methoxybenzyl)benzamide

5-(4-methoxybenzyl)-4a-methyl-3,4,4a,5-tetrahydro-1H-pyrido[1,2-a]quinazolin-6(2H)-one

5-(4-methoxybenzyl)-4a-methyl-3,4,4a,5-tetrahydro-1H-pyrido[1,2-a]quinazolin-6(2H)-one

Conditions
ConditionsYield
With iodine at 80℃; for 8h; Ionic liquid;89%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-Amino-5-chlor-N2-phenyl-benzoesaeure-hydrazid
18852-01-2

2-Amino-5-chlor-N2-phenyl-benzoesaeure-hydrazid

6-chloro-2-(4-chlorobutyl)-2-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

6-chloro-2-(4-chlorobutyl)-2-methyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With iodine; 1-n-butyl-3-methylimidazolim bromide at 80℃; for 11h; Ionic liquid; Green chemistry; chemoselective reaction;89%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-(aminophenyl)benzimidazole
5805-39-0

2-(aminophenyl)benzimidazole

9a-methyl-7,8,9,9a-tetrahydro-6H-benzo[4,5]imidazo[1,2-c]pyrido[1,2-a]quinazoline

9a-methyl-7,8,9,9a-tetrahydro-6H-benzo[4,5]imidazo[1,2-c]pyrido[1,2-a]quinazoline

Conditions
ConditionsYield
With iodine at 80℃; for 11h; Ionic liquid;89%
propylamine
107-10-8

propylamine

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

phenylacetylene
536-74-3

phenylacetylene

C17H23N

C17H23N

Conditions
ConditionsYield
With copper(I) oxide In acetonitrile at 90℃; for 24h; Inert atmosphere;88%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-amino-N-[2-(4-methoxyphenyl)ethyl]benzamide
565171-47-3

2-amino-N-[2-(4-methoxyphenyl)ethyl]benzamide

5-(4-methoxyphenylethyl)-4a-methyl-3,4,4a,5-tetrahydro-1H-pyrido[1,2-a]quinazolin-6(2H)-one

5-(4-methoxyphenylethyl)-4a-methyl-3,4,4a,5-tetrahydro-1H-pyrido[1,2-a]quinazolin-6(2H)-one

Conditions
ConditionsYield
With iodine at 80℃; for 8h; Ionic liquid;87%
2-methyl-1H-indole
95-20-5

2-methyl-1H-indole

6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

3-(5-chloro-1-methylpentyl)-2-methyl-1H-indole

3-(5-chloro-1-methylpentyl)-2-methyl-1H-indole

Conditions
ConditionsYield
With indium(III) tris[bis(trifluoromethanesulfonyl)amide]; methyldiphenylsilane In 1,4-dioxane at 50℃; for 24h; Inert atmosphere; Schlenk technique;87%
6-chloro-2-hexanone
10226-30-9

6-chloro-2-hexanone

2-amino-5-methyl-N'-phenylbenzohydrazide

2-amino-5-methyl-N'-phenylbenzohydrazide

2-(4-chlorobutyl)-2,6-dimethyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

2-(4-chlorobutyl)-2,6-dimethyl-3-(phenylamino)-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With iodine; 1-n-butyl-3-methylimidazolim bromide at 80℃; for 10h; Ionic liquid; Green chemistry; chemoselective reaction;87%

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