Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:932-64-9
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:932-64-9
Min.Order:1
Negotiable
Type:Other
inquiry1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
Cas:932-64-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry932-64-9 Application:intermediate
Cas:932-64-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With sulfuric acid; nitric acid In water at 65℃; for 2h; | 96% |
With nitric acid at 50 - 85℃; for 0.5h; | 84% |
With nitric acid at 54.9 - 59.9℃; | |
With sulfuric acid; nitric acid | |
With sulfuric acid; nitric acid In water at 65℃; for 2h; |
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 5h; | 98% |
propynoic acid methyl ester
3-nitro-1,2,4-triazol-5-one
triphenylphosphine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 5h; | 98% |
3-nitro-1,2,4-triazol-5-one
triphenylphosphine
propynoic acid ethyl ester
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 5h; | 95% |
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
In water for 0.5h; Reflux; | 90% |
3,6-diamino-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
In water at 50℃; for 4h; | 89% |
Conditions | Yield |
---|---|
In water at 80℃; for 2h; | 88% |
Conditions | Yield |
---|---|
With hydrogenchloride for 7h; Substitution; Heating; | 85.7% |
formaldehyd
3-nitro-1,2,4-triazol-5-one
2-Hydroxymethyl-5-nitro-2,4-dihydro-[1,2,4]triazol-3-one
Conditions | Yield |
---|---|
In water; acetone for 8h; Ambient temperature; | 85% |
Conditions | Yield |
---|---|
With sulfuric acid In water at 20℃; for 24h; | 85% |
(E)-1,2-bis(3,4-diamino-1,2,4-triazol-5-yl)-ethene
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
In water at 60 - 100℃; for 1h; | 84.6% |
3,6,7-triamino-7H-[1,2,4]triazolo[4,3-b][1,2,4]triazolium
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
In water at 80 - 120℃; | 83.7% |
3-nitro-1,2,4-triazol-5-one
C4H4N8O3
Conditions | Yield |
---|---|
With sulfuric acid In water at 5 - 10℃; for 7h; Electrolysis; | 82% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 20℃; under 1551.44 Torr; for 5h; Reduction; | 70% |
2-deoxy-3,5-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl chloride
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
With sodium hydride In acetonitrile | 67% |
Conditions | Yield |
---|---|
With sulfuric acid In water at 20℃; for 1h; | 64% |
N-(hydroxymethyl)acetamide
3-nitro-1,2,4-triazol-5-one
1-acetamidomethyl-3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
In ethanol Ambient temperature; 1.)8 h 2.)overnight; | 53% |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 2h; | 43.2% |
3-nitro-1,2,4-triazol-5-one
A
C4H4N8O2
B
C4H4N8O3
C
5-amino-2,4-dihydro-3H-1,2,4-triazol-3-one
Conditions | Yield |
---|---|
With sodium sulfate In water pH=2 - 7; Electrolysis; | A n/a B n/a C 39% |
With sulfuric acid In water at 20℃; Electrolysis; | A n/a B n/a C 14% |
picryl fluoride
3-nitro-1,2,4-triazol-5-one
A
5-nitro-2-picryl-2,4-dihydro-3H-1,2,4-triazol-3-one-4-15N
B
5-nitro-2,4-dipicryl-2,4-dihydro-3H-1,2,4-triazol-3-one-4-15N
Conditions | Yield |
---|---|
In various solvent(s) for 16h; Ambient temperature; | A 34% B 26% |
picryl fluoride
3-nitro-1,2,4-triazol-5-one
A
5-nitro-2,4-dipicryl-2,4-dihydro-3H-1,2,4-triazol-3-one
B
5-nitro-2-picryl-2,4-dihydro-3H-1,2,4-triazol-3-one
Conditions | Yield |
---|---|
In various solvent(s) for 16h; Ambient temperature; | A 30% B 34% |
N-methyl-N-chloromethyl-N-nitroamine
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
Stage #1: 3-nitro-1,2,4-triazol-5-one With triethylamine In acetone for 0.0833333h; Stage #2: N-methyl-N-chloromethyl-N-nitroamine In acetone at 20℃; for 12h; | 33% |
methyl vinyl ketone
3-nitro-1,2,4-triazol-5-one
5-Nitro-2,4-bis-(3-oxo-butyl)-2,4-dihydro-[1,2,4]triazol-3-one
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 80℃; for 8h; Yield given; |
3-nitro-1,2,4-triazol-5-one
dimethyl sulfate
A
4-methyl-3-nitro-1,2,4-triazol-5(1H,4H)-one
B
1-methyl-3-nitro-1,2,4-triazol-5(1H,4H)-one
C
3-nitro-5-methoxy-1,2,4-triazole
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide at 18 - 20℃; for 8h; Product distribution; other solvent - water; var. ratio of reagents; | A 54 % Spectr. B 30 % Spectr. C 16 % Spectr. |
1-amino-2-azidoethane
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
In water Ambient temperature; |
cadmium(II) carbonate
3-nitro-1,2,4-triazol-5-one
Conditions | Yield |
---|---|
In water byproducts: CO2; stirring soln. of ligand, addn. of excess of Cd-salt (60°C), stirring (60°C, 30 min, pptn.); hot filtration, dissolving (EtOH), sepn. of CdCO3, standing (6 h, pptn.), recrystn. (H2O, 25°C); |
Conditions | Yield |
---|---|
With NaOH In water addn. of soln. of hydroxide to soln. of ligand, stirring (60°C, pH = 6 - 7), dropping this soln. to soln. of Pb-salt (60°C), stirring, heating (60°C, 30 min, pptn.); recrystn. (H2O, 25°C); |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View