2-hydroxypyrimidine hydrochloride
5-iodo-2(1H)-pyrimidinone
Conditions | Yield |
---|---|
With methanol; iodine; silver sulfate at 20℃; for 16h; Darkness; | 94% |
Pyrimidin-2(1H)-one
5-iodo-2(1H)-pyrimidinone
Conditions | Yield |
---|---|
With N-iodo-succinimide In N,N-dimethyl-formamide for 48h; Ambient temperature; | 77.5% |
With N-iodo-succinimide In N,N-dimethyl-formamide | 11.35 g (77.5%) |
With N-iodo-succinimide In N,N-dimethyl-formamide | 11.35 g (77.5%) |
2-pyrimidinone hydrochloride
5-iodo-2(1H)-pyrimidinone
Conditions | Yield |
---|---|
With sodium dihydrogen phosphate; sodium iodine dichloride In water at 65℃; for 1.66667h; | 75% |
With Iodine monochloride; sodium chloride In water at 60℃; for 1h; | |
With N-iodo-succinimide In N,N-dimethyl-formamide at 20℃; for 48h; | |
With Iodine monochloride; acetic acid In water at 45 - 48℃; for 6h; Temperature; |
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