N,N-dimethyl-N'-phenylsulfonamide
dichlorofluoromethanesulphenyl chloride
N-dichlorofluoromethylthio-N',N'-dimethyl-N-phenylsulfamide
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-N'-phenylsulfonamide With sodium hydride In toluene at 0 - 20℃; for 1h; Stage #2: dichlorofluoromethanesulphenyl chloride In toluene at 20℃; | 84.2% |
N,N-dimethyl-N'-phenylsulfonamide
triethylamine
dichlorofluoromethanesulphenyl chloride
N-dichlorofluoromethylthio-N',N'-dimethyl-N-phenylsulfamide
N-dichlorofluoromethylthio-N',N'-dimethyl-N-phenylsulfamide
bis(dichlorofluoromethyl)disulfane
Conditions | Yield |
---|---|
In acetone Irradiation (UV/VIS); together with other products; | |
In acetone Irradiation (UV/VIS); together with other products; |
1. | mmo-esc 10 µg/plate | MUREAV Mutation Research. 116 (1983),185. | ||
2. | mma-esc 100 µg/plate | MUREAV Mutation Research. 116 (1983),185. | ||
3. | orl-rat LD50:500 mg/kg | WRPCA2 World Review of Pest Control. 9 (1970),119. | ||
4. | ihl-rat LC50:300 mg/m3/4H | 85JFAN “Agrochemicals Handbook“, with updates, Hartley, D., and H. Kidd, eds., Nottingham, UK, Royal Soc. of Chemistry, 1983-86 A136 ,1986. | ||
5. | skn-rat LD50:1 g/kg | GUCHAZ Guide to the Chemicals Used in Crop Protection 6 (1973),179. | ||
6. | orl-mus LD50:1250 mg/kg | MEIEDD Merck Index. 10 (1983),442. | ||
7. | orl-cat LD50:1 g/kg | 85GYAZ Pflanzenschutz-und Schaedlingsbekaempfungsmittel: Abriss einer Toxikologie und Therapie von Vergiftungen 2nd ed.,Klimmer, O.R.,Hattingen, Germany.: Hundt-Verlag,1971,97. |
Moderately toxic by ingestion and skin contact. Mutation data reported. A pesticide. When heated to decomposition it emits very toxic fumes of Cl−, F−, NOx, and SOx.
Hazard Codes Xn,N,F
Risk Statements
11:Highly Flammable
20:Harmful by inhalation
21:Harmful in contact with skin
22:Harmful if swallowed
36:Irritating to the eyes
43:May cause sensitization by skin contact
50:Very Toxic to aquatic organisms
53:May cause long-term adverse effects in the aquatic environment
Safety Statements
16:Keep away from sources of ignition - No smoking
24:Avoid contact with skin
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36:Wear suitable protective clothing
37:Wear suitable gloves
60:This material and/or its container must be disposed of as hazardous waste
61:Avoid release to the environment. Refer to special instructions safety data sheet
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