sodium 4-amino-1-naphthalenesulfonate
Conditions | Yield |
---|---|
With sodium azide; carbon monoxide; palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In water-d2; dimethyl sulfoxide Sealed tube; | 44.8% |
Conditions | Yield |
---|---|
With sodium methylate In methanol |
Conditions | Yield |
---|---|
With sodium tetrahydroborate at 20℃; Kinetics; Reagent/catalyst; | |
With sodium tetrahydroborate In water Catalytic behavior; Kinetics; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In water at 20℃; Kinetics; Reagent/catalyst; Concentration; |
Conditions | Yield |
---|---|
Stage #1: 1-amino-naphthalene With sulfur trioxide In 1,2-dichloro-benzene at 40℃; for 0.833333h; Large scale; Stage #2: With sodium hydroxide In water; 1,2-dichloro-benzene at 85 - 190℃; for 3h; pH=7; Temperature; Solvent; Reagent/catalyst; Autoclave; Large scale; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In water |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In water for 0.0388889h; Kinetics; Time; |
Conditions | Yield |
---|---|
With sodium hydrogensulfite In water for 24h; Heating; | 90% |
sodium 4-amino-1-naphthalenesulfonate
p-methoxyphenylazobenzenethiosulfonate
2-(4-methoxyphenylazo)-1-aminonaphthalene-4-sulfonic acid
Conditions | Yield |
---|---|
With hydrogenchloride; sodium acetate at 40 - 60℃; for 3h; | 78% |
Conditions | Yield |
---|---|
With sodium carbonate In chloroform; water at 0 - 25℃; for 23h; | 60% |
water
sodium 4-amino-1-naphthalenesulfonate
[Pb2(μ3-4-amino-1-naphthalenesulfonic acid)2(μ2-Cl)2(H2O)2]n
Conditions | Yield |
---|---|
for 3h; Reflux; | 47% |
Conditions | Yield |
---|---|
With pyridine at 120 - 125℃; for 4.5h; | 31% |
sodium 4-amino-1-naphthalenesulfonate
Conditions | Yield |
---|---|
Stage #1: sodium 4-amino-1-naphthalenesulfonate With hydrogenchloride; sodium nitrite In water at 0℃; for 1h; Stage #2: With sodium iodide In water at 20 - 90℃; for 3.5h; | 29.8% |
sodium 4-amino-1-naphthalenesulfonate
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In water at 20℃; for 48h; | 22% |
Conditions | Yield |
---|---|
With water |
sodium 4-amino-1-naphthalenesulfonate
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid |
sodium 4-amino-1-naphthalenesulfonate
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite 2.) 2.5 h; Yield given. Multistep reaction; |
sodium 4-amino-1-naphthalenesulfonate
N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide
Conditions | Yield |
---|---|
With hydrogenchloride; sodium acetate; sodium carbonate; sodium nitrite 1.) THF, 5 deg C, 2 min, 2.) THF, 5 deg C, 1 h; Yield given; Multistep reaction; |
water
bromine
sodium 4-amino-1-naphthalenesulfonate
A
2,4-dibromo-1-naphthylamine
sodium 4-amino-1-naphthalenesulfonate
Conditions | Yield |
---|---|
Stage #1: 3,3'-dimethoxy-(1,1'-biphenyl)-4,4'-diamine With hydrogenchloride; sodium nitrite at 0℃; Stage #2: sodium 4-amino-1-naphthalenesulfonate With sodium carbonate at 0 - 50℃; |
Conditions | Yield |
---|---|
Stage #1: 3,3'-dichlorobenzidine With hydrogenchloride; sodium nitrite at 0℃; Stage #2: sodium 4-amino-1-naphthalenesulfonate With sodium carbonate at 0 - 50℃; | 66 mg |
Conditions | Yield |
---|---|
Stage #1: 3,3'-diaminodiphenyl sulfone With hydrogenchloride; sodium nitrite at 0℃; Stage #2: sodium 4-amino-1-naphthalenesulfonate With sodium carbonate at 0 - 20℃; |
Conditions | Yield |
---|---|
Stage #1: aniline With hydrogenchloride; sodium nitrite at 0 - 5℃; Stage #2: sodium 4-amino-1-naphthalenesulfonate With sodium carbonate at 0 - 20℃; | 71 mg |
Conditions | Yield |
---|---|
Stage #1: dapsone With hydrogenchloride; sodium nitrite at 0℃; Stage #2: sodium 4-amino-1-naphthalenesulfonate With sodium carbonate at 0 - 20℃; | 24 mg |
Molecule structure of 4-Amino-1-naphthalenesulfonic acid sodium salt (CAS NO.130-13-2) :
IUPAC Name: sodium 4-aminonaphthalene-1-sulfonate
Molecular Weight: 245.23019 g/mol
Molecular Formula: C10H8NNaO3S
Melting Point: 280 °C (dec.)(lit.)
Density: 1.6703
Appreance: pink to greyish-purple powder
Merck: 6403
log P (octanol-water): -2.34E+00
Water Solubility: 1.00E+06 mg/L
Vapor Pressure: 1.55E-14 mm Hg
Atmospheric OH Rate Constant: 4.39E-11 cm3/molecule-sec
H-Bond Donor: 1
H-Bond Acceptor: 4
Rotatable Bond Count: 1
Exact Mass: 245.012258
MonoIsotopic Mass: 245.012258
Topological Polar Surface Area: 83.2
Heavy Atom Count: 16
Complexity: 327
Canonical SMILES: C1=CC=C2C(=C1)C(=CC=C2S(=O)(=O)[O-])N.[Na+]
InChI: InChI=1S/C10H9NO3S.Na/c11-9-5-6-10(15(12,13)14)8-4-2-1-3-7(8)9;/h1-6H,11H2,(H,12,13,14);/q;+1/p-1
InChIKey: JWSRMCCRAJUMLX-UHFFFAOYSA-M
EINECS: 204-975-5
Product Categories: Intermediates of Dyes and Pigments
4-Amino-1-naphthalenesulfonic acid sodium salt (CAS NO.130-13-2) is used for the preparation of acidic dyes and food red pigment, but also for antidote of nitrite and iodine poisoning.
Hazard Codes: Xi
Risk Statements: 36/37/38
R36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 26
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
WGK Germany: 3
F: 3-8-23
HS Code: 29214500
4-Amino-1-naphthalenesulfonic acid sodium salt (CAS NO.130-13-2) is also called 1,4-Naphthionic monosodium salt ; AI3-19501 ; CCRIS 8901 ; NSC 168 ; Naphthemol ; Naphthionine ; Sodium 1-aminonaphthalene-4-sulfonate ; Sodium alpha-naphthylamine-4-sulfonate ; Sodium naphthionate . 4-Amino-1-naphthalenesulfonic acid sodium salt (CAS NO.130-13-2) is soluble in water, soluble in 95% ethanol, insoluble in ether, dissolved in a small amount of concentrated caustic alkali solution and ethanol solution.
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View