• Name

  BIS(METHYLPHENYLTHIOCARBAMOYL)DISULFIDE

• EINECS
• CAS No. 10591-84-1
• Article Data17
• CAS DataBase
• Density 1.379g/cm³
• Solubility 10ng/L at 20℃
• Melting Point 168-170 °C(Solv: ethanol (64-17-5))
• Formula C16H16 N2 S4
• Boiling Point 478.3°Cat760mmHg
• Molecular Weight 364.58
• Flash Point 243.1°C
• Transport Information
• Appearance
• Safety
• Risk Codes
• Molecular Structure
• Hazard Symbols
• Synonyms Disulfide,bis(methylphenylthiocarbamoyl) (6CI,7CI,8CI); Bis(methylphenylthiocarbamoyl)disulfide;N,N'-Dimethyl-N,N'-diphenylthiuram disulfide; NSC 37161; Vulkacit J; VulkaciteJ
• PSA 121.26000
• LogP 5.21040

Synthetic route

75-15-0

carbon disulfide

100-61-8

N-methylaniline

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
With N,N-diethylnmethylamine; dihydrogen peroxide In toluene at 0 - 10℃; for 27.5h; Temperature; Reagent/catalyst; Solvent; Large scale;	98.9%
With sodium hydroxide at 50℃; for 6h;	75%
Stage #1: carbon disulfide; N-methylaniline With potassium hydroxide In tetrahydrofuran; water at 20℃; for 12h; Stage #2: With iodine In tetrahydrofuran; methanol; water at 20℃; for 1h;	67%

37600-51-4

methyl-phenyl-dithiocarbamic acid

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
With air; nitrogen oxides in sodaalkolische Loesung;

methyl-phenyl-thiocarbamoyl thiocyanate

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
With sodium sulfide; ethanol und Behandeln der mit Wasser versetzten Reaktionsloesung mit Bromcyan;

100-61-8

N-methylaniline

CS2

CS2

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
With ethanol; iodine durch Oxydation; oder mit einem anderen Oxydationsmittel;

salt of/the/ methyl-phenyl-dithiocarbamic acid

salt of/the/ methyl-phenyl-dithiocarbamic acid

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
With sodium trithionate; ethanol

19009-45-1

N-methyl-N-phenylthiocarbamoyl chloride

sodium salt of a(n) dialkylatedene thiuram disulfide

sodium salt of a(n) dialkylatedene thiuram disulfide

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

100-61-8

N-methylaniline

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: diethyl ether View Scheme

19009-45-1

N-methyl-N-phenylthiocarbamoyl chloride

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: ethanol 2: ethanol; sodium sulfide / und Behandeln der mit Wasser versetzten Reaktionsloesung mit Bromcyan View Scheme

506-68-3

bromocyane

39234-21-4

sodium N-methyl-N-phenyldithiocarbamate

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
With potassium iodide In water pH:6.2-6.7; in aqueous and non aqueous medium; titration method;

83559-31-3

potassium N-methyl-N-phenyl-dithiocarbamate

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In methanol; water at 0 - 5℃;

10591-84-1

N,N’-dimethyl-N,N’-diphenylthiuram disulfide

A

75-15-0

carbon disulfide

B

100-61-8

N-methylaniline

Conditions

Conditions	Yield
Beim Erhitzung unter vermindertem Druck;