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sulfuric acid
water
sodium chloride
A
sodium hydrogensulfate monohydrate
Na hydrogensulfate
Conditions | Yield |
---|---|
In water Kinetics; exposure of powdered NaCl to H2SO4 soln. with compn. of NaCl:H2O:H2SO4 of 2:8:1 for 24 h at 85% rel. humidities; not isolated, detn. by Raman spectroscopy; |
sulfuric acid
water
sodium chloride
A
hydrogenchloride
B
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
In water Kinetics; exposure of powdered NaCl to H2SO4 soln. with compn. of NaCl:H2O:H2SO4 of 2:20:1 at 85% rel. humidities; not isolated, detn. by Raman spectroscopy; |
sulfuric acid
water
sodium chloride
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
In sulfuric acid Kinetics; exposure of NaCl with 96 wt% H2SO4 (0.5:1 H2SO4:NaCl) in dry bag; storage in desiccator for several days; exposure to environment of 100% rel. humidities for 40 min; not isolated, detn. by Raman spectroscopy; |
A
sodium hydrogensulfate monohydrate
B
sodium hydrogen oxalate monohydrate
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; mixing oxalic acid and Glauber's salt; completation of reaction after 24 h;; | |
In not given byproducts: H2O; reaction of Glauber's salt with oxalic acid;; | |
In neat (no solvent) byproducts: H2O; mixing oxalic acid and Glauber's salt; completation of reaction after 24 h;; |
sodium sulfate
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
In water crystallization from an acidic aq. soln. of Na2SO4 at ambient temperature;; | |
In water crystallization from an acidic aq. soln. of Na2SO4 at ambient temperature;; |
sodium hydrogensulfate monohydrate
1,3-bis-(diphenylphosphino)propane
water
palladium diacetate
[Pd(SO4)(1,3-bis(diphenylphosphino)propane)]
Conditions | Yield |
---|---|
In water; acetone acetone soln. of ligand added dropwise to soln. of Pd compd. (1:1), excess NaHSO4 in water added; pptd., stirred for 30 min, filtered off, washed (acetone/water=5/2, Et2O), dried (vac.), elem. anal.; | 90% |
sodium hydrogensulfate monohydrate
trimethylsilyl butyrate
cyclododecanone
N-cyclohexyl-cyclohexanamine
Cyclododecylene acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; n-butyllithium | 79% |
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
With pyridine In dichloromethane | 62.6% |
sodium hydrogensulfate monohydrate
Triisopropoxymethan
potassium isopropoxide
cyclopentanone
Conditions | Yield |
---|---|
In isopropyl alcohol | 51% |
sodium hydrogensulfate monohydrate
3-amino-3-(pyridin-3-yl)propanoic acid
di-tert-butyl dicarbonate
Conditions | Yield |
---|---|
With sodium hydroxide; magnesium sulfate In tetrahydrofuran; water |
sodium hydrogensulfate monohydrate
4-Aminomethylpiperidine
1-acetyl-4-aminomethylpiperidine
Conditions | Yield |
---|---|
With sodium hydroxide; acetic anhydride; benzaldehyde; triethylamine In water; benzene |
sodium hydrogensulfate monohydrate
sodium ethanolate
isobutyraldehyde
diethyl malonate
2-isopropyl-5,5-bis(carboethoxy)-1,3-dioxane
Conditions | Yield |
---|---|
With sulfuric acid; trimethyl orthoformate; paraformaldehyde In ethanol |
sodium hydrogensulfate monohydrate
chromium(VI) oxide
Conditions | Yield |
---|---|
With pyridine In dichloromethane |
sodium hydrogensulfate monohydrate
Dimethoxymethane
butyraldehyde
3,5-diethylpyridine
Conditions | Yield |
---|---|
In ammonium hydroxide; dichloromethane |
sodium hydrogensulfate monohydrate
L-arginine
di-tert-butyl dicarbonate
t-butyloxycarbonyl-L-arginine
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; water; butan-1-ol |
sodium hydrogensulfate monohydrate
methyl 7-((1R,2S,3R,5S)-5-acetoxy-2-hydroxymethyl-3-((tetrahydro-2H-pyran-2-yl)oxy)cyclopentyl)heptanoate
methyl 7-((1R,2R,3R,5S)-5-acetoxy-2-formyl-3-((tetrahydro-2H-pyran-2-yl)oxy)cyclopentyl)heptanoate
Conditions | Yield |
---|---|
With pyridine In dichloromethane; ethyl acetate; benzene |
sodium hydrogensulfate monohydrate
2α-(6-methoxycarbonyl-hex-cis-2-enyl)-3β-hydroxymethyl-4α-(2-tetrahydropyranyloxy)-cyclopentan-1α-ol
acetyl chloride
2α-(6-methoxycarbonylhex-cis-2-enyl)-3β-acetoxymethyl-4α-(2-tetrahydropyranyloxy)cyclopentan-1α-ol
Conditions | Yield |
---|---|
With pyridine In methanol; dichloromethane |
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
With pyridine In dichloromethane |
sodium hydrogensulfate monohydrate
2-(Trimethylsilyl)butansaeure-ethylester
(+/-)-ethyl 4-methyl-3-phenylpentanoate
Conditions | Yield |
---|---|
With hydrogenchloride; lithium diisopropyl amide; palladium-carbon In tetrahydrofuran; methanol; ethyl acetate |
Conditions | Yield |
---|---|
In solid byproducts: SiO2; investigation of solid state react. of kaolin and NaHSO4*H2O by DTA and thermogravimetry (up to 700 °C);; X-ray diffraction; |
Conditions | Yield |
---|---|
In solid byproducts: SiO2; investigation of solid state react. of kaolin and NaHSO4*H2O by DTA and thermogravimetry (closed vessel, low temp.);; X-ray diffraction; |
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
In water addition of 30 g pure Zr sulfate under stirring to a solution of 57.95 g NaHSO4*H2O in 110 ml H2O at 30°C; increase of temperature to 43°C after 10 minutes, then decrease after 20 minutes to 37°C;; evacuation of the filtrate in vacuum, washing 3 times with 15 ml water at 10°C and drying on air; yield 29 g;; | |
In water addition of 30 g pure Zr sulfate under stirring to a solution of 57.95 g NaHSO4*H2O in 110 ml H2O at 30°C; increase of temperature to 43°C after 10 minutes, then decrease after 20 minutes to 37°C;; evacuation of the filtrate in vacuum, washing 3 times with 15 ml water at 10°C and drying on air; yield 29 g;; |
sodium hydrogensulfate monohydrate
sodium sulfate
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; transition point 58.54 °C;; | |
In neat (no solvent) byproducts: H2O; transition point 58.54 °C;; |
Conditions | Yield |
---|---|
In melt | |
In melt |
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
In water evaporation of a solution of 10 g Zr sulfate and 16.8 g NaHSO4 in 40 ml H2O at room temperature over H2SO4 with formation of a transparent syrup;; solidifying on scrapeing with a glass stick; drying on air;; |
sodium hydrogensulfate monohydrate
Conditions | Yield |
---|---|
In not given addition of freshly precipitated Zr dioxide hydrate to a boiling concentrated solution of NaHSO4;; precipitation on cooling down of Zr sulfate, then of Na-Zr-sulfate, finally precipitation of the excess of hydrogensulfate;; | |
In not given addition of freshly precipitated Zr dioxide hydrate to a boiling concentrated solution of NaHSO4;; precipitation on cooling down of Zr sulfate, then of Na-Zr-sulfate, finally precipitation of the excess of hydrogensulfate;; |
sodium hydrogensulfate monohydrate
Na hydrogensulfate
Conditions | Yield |
---|---|
In neat (no solvent) heating NaHSO4*H2O to 120°C for 48 h; | |
In neat (no solvent, solid phase) NaHSO4*H2O heated at 420-440 K for 24 h; |
Conditions | Yield |
---|---|
at 399.84℃; for 12h; |
Conditions | Yield |
---|---|
at 20℃; |
sodium hydrogensulfate monohydrate
silica gel
Conditions | Yield |
---|---|
In water Heating; Inert atmosphere; | |
at 20℃; for 0.25h; |
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