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Cas:103-65-1
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inquiryPropylbenzene CAS No.:103-65-1 Name: Propylbenzene Synonyms: n-Propylbenzene Molecular Structure Molecular Formula: C9H12 Molecular Weight: 120.19
Cas:103-65-1
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inquiryProduct name N-PROPYLBENZENE Synonyms 1-PHENYLPROPANE;PROPYLBENZENE;N-PROPYLBENZENE;1-Propylbenzene;benzene,propyl-;Isocumene;propylbenzene solution;Phenylpropane Cas
N-Propylbenzene CAS:103-65-1 Specification Product name N-PROPYLBENZENE Synonyms 1-PHENYLPROPANE;PROPYLBENZENE;N-PROPYLBENZENE;1-Propylbenzene;benzene,propyl-;Isocumene;propylbenzene solution;Phenylpropane
Cas:103-65-1
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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Product name: N-Propylbenzene CAS No.:103-65-1 Molecule Formula:C9H12 Molecule Weight:120.19 Purity: 99.0% Package: 25kg/drum Description: Colorless transparent liquid Manufacture Standards:Enterprise Standard TEST
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:103-65-1
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inquiryN-PROPYLBENZENE Basic information Product Name: N-PROPYLBENZENE Synonyms: 1-PHENYLPROPANE;PROPYLBENZENE;N-PROPYLBENZENE;1-Propylbenzene;benzene,propyl-;Isocumene;Phenylpropane;propyl-benzen
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United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
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At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App
Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por
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Conditions | Yield |
---|---|
With Pt-Sn-citrate; hydrogen In methanol at 50℃; under 3800 Torr; for 3h; var. temperatures; var. pressures; | 100% |
With Pt-Sn-citrate; hydrogen In methanol at 50℃; under 3800 Torr; for 3h; | 100% |
With C49H60BF2IrN5(1+)*C32H12BF24(1-); hydrogen In 1,2-dichloro-ethane at 20℃; for 0.166667h; Reagent/catalyst; Schlenk technique; | 100% |
Conditions | Yield |
---|---|
With C28H18Co(1-)*K(1+)*2C4H10O2; hydrogen In toluene at 60℃; under 1500.15 Torr; for 24h; Temperature; Time; Reagent/catalyst; chemoselective reaction; | 100% |
With iron(III) chloride; lithium aluminium tetrahydride; hydrogen In tetrahydrofuran at 18℃; under 750.075 Torr; for 20h; Inert atmosphere; Sealed tube; | 100% |
In methanol for 0.5h; UV-irradiation; | 99% |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 39.84℃; under 760.051 Torr; for 5h; | 100% |
With hydrogen In 1,4-dioxane at 200℃; under 15001.5 Torr; | 95.8% |
Stage #1: 1-phenyl-propan-1-one With iron(III) chloride In methanol at 20℃; for 0.05h; Stage #2: In methanol at 20℃; for 0.166667h; chemoselective reaction; | 91% |
Conditions | Yield |
---|---|
With hydrogen; sodium triethylborohydride In tetrahydrofuran under 30003 Torr; for 20h; Catalytic behavior; Inert atmosphere; | 100% |
With water; zinc; chloro(1,5-cyclooctadiene)rhodium(I) dimer In 1,4-dioxane at 90℃; for 20h; | 99% |
With [Fe(nacnac)dippCH2SiMe3]; N-butylamine; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In benzene-d6 at 20℃; for 16h; Sealed tube; Schlenk technique; Glovebox; Inert atmosphere; | 99% |
1,1,3,3-Tetramethyldisiloxane
2-phenoxy-1-phenylpropane-1, 3-diol
Propylbenzene
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; water In dichloromethane at 20℃; for 16h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; acetonitrile; sodium iodide In hexane for 24h; Ambient temperature; | 99% |
With chloro-trimethyl-silane; acetonitrile; sodium iodide In hexane for 24h; Ambient temperature; | 99% |
With hydrogen In ethanol at 80℃; under 2250.23 Torr; for 3h; Catalytic behavior; Temperature; Solvent; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With LiCrH4*2LiCl*2THF In tetrahydrofuran at 25℃; for 12h; | 99% |
With indium(III) chloride; sodium tetrahydroborate In acetonitrile at 20℃; for 2h; | 95% |
With sodium tetrahydroborate; water In methanol at 20℃; for 0.5h; | 87% |
trimethylsilan
A
3-phenyl-propionaldehyde
D
Propylbenzene
E
trimethyl(3-phenylpropoxy)silane
Conditions | Yield |
---|---|
In benzene-d6 react. of Fe complex and HSiMe3 in benzene, 90°C, 9 h; yields detd. by (1)H-NMR (C5H5Fe(CO)H(SiMe3)2; elem. anal.) and GL-chromy. (other products); | A 0% B 91% C 10% D 0% E 98% |
Conditions | Yield |
---|---|
With hydrogen In methanol at 30℃; under 760.051 Torr; for 2h; | A 97% B 3% |
With hydrogen; poly(amidoamine) dendron-stabilised Pd(0) nanoparticle In dichloromethane at 25℃; under 760.051 Torr; for 1h; | A 96% B 4% |
With hydrogen; Et4N In 1,2-dimethoxyethane at 100℃; under 38000 Torr; for 18h; Product distribution; further unsaturated compounds of different types; | A 8% B 90% |
Propylbenzene
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran at 67℃; Irradiation; | 97% |
Conditions | Yield |
---|---|
With palladium dichloride In methanol at 40℃; for 18h; Inert atmosphere; Green chemistry; chemoselective reaction; | 96% |
With [IrCl(CO)(PPh3)2]; hydrazine hydrate; potassium hydroxide In methanol at 160℃; for 3h; Wolff-Kishner Reduction; Sealed tube; | 81% |
With [IrCl(CO)(PPh3)2]; hydrazine hydrate; potassium hydroxide In methanol at 160℃; for 3h; Sealed tube; | 81% |
Conditions | Yield |
---|---|
With potassium hydroxide; hydrogen; Aliquat 336; palladium on activated charcoal In 2,2,4-trimethylpentane at 50℃; for 0.833333h; Product distribution; various time, solvents; also in the presence of various aromatic halides as promoters; further benzylic alcohols; | A 96% B 4% |
trimethylstannane
A
3-phenyl-propionaldehyde
C
3-Phenyl-1-propanol
D
Propylbenzene
Conditions | Yield |
---|---|
In benzene-d6 react. of Fe complex and HSnMe3 in benzene, 120°C, 7 h; yields detd. by (1)H-NMR (C5H5Fe(CO)H(SnMe3)2; elem. anal.) and GL-chromy. (other products); | A <3 B 73% C 96% D 0% |
In benzene-d6 Irradiation (UV/VIS); irradn. of Fe complex and HSnMe3 in benzene for 6 h; yields detd. by (1)H-NMR and GL-chromy.; | A 79% B 82% C 0% D 0% |
Conditions | Yield |
---|---|
With tetrahydroxydiboron; palladium 10% on activated carbon; water In dichloromethane at 20℃; for 5h; Inert atmosphere; | 95% |
With 2C2H3O2(1-)*Pd(2+)*3Na(1+)*C18H12O9PS3(3-); hydrogen; glycerol at 100℃; under 2250.23 Torr; for 2h; Schlenk technique; | 92% |
With hydrogen; palladium on activated charcoal In hexane under 1520 Torr; Thermodynamic data; ΔH; |
N-benzyl-2-phenylethylamine
triethylaluminum
A
Propylbenzene
B
phenethylamine
C
1,1'-(1,2-ethanediyl)bisbenzene
D
toluene
Conditions | Yield |
---|---|
In benzene for 38h; Irradiation; | A 50% B 95% C n/a D 14% |
propyl bromide
triphenylphosphine
A
Propylbenzene
B
diphenylphosphinopropane
Conditions | Yield |
---|---|
Stage #1: triphenylphosphine With lithium In diethyl ether at 20℃; for 3h; Inert atmosphere; Stage #2: propyl bromide In diethyl ether at 0 - 30℃; for 2.5h; | A 94.8% B 92.4% |
Stage #1: triphenylphosphine With lithium In diethyl ether at 20℃; for 3h; Inert atmosphere; Stage #2: propyl bromide In diethyl ether at 0 - 30℃; for 1.5h; Inert atmosphere; |
Conditions | Yield |
---|---|
With triethylsilane; tris(pentafluorophenyl)borate In dichloromethane at 20℃; | 94% |
With triethylsilane; tris(pentafluorophenyl)borate In dichloromethane at 20℃; for 20h; | 94% |
With 1,1,3,3-Tetramethyldisiloxane; tris(pentafluorophenyl)borate In benzene-d6 at 23℃; for 1h; Glovebox; Schlenk technique; | 100 %Spectr. |
trimethylstannane
A
3-phenyl-propionaldehyde
C
3-Phenyl-1-propanol
D
Propylbenzene
Conditions | Yield |
---|---|
In benzene-d6 react. of Fe complex and HSnMe3 in benzene, 60°C, 13 h; yields detd. by (1)H-NMR (C5H5Fe(CO)H(SnMe3)2; elem. anal.) and GL-chromy. (other products); | A 0% B 88% C 94% D <3 |
In benzene-d6 Irradiation (UV/VIS); irradn. of Fe complex and HSnMe3 in benzene for 7 h; yields detd. by (1)H-NMR and GL-chromy.; | A 0% B 85% C <3 D 86% |
Conditions | Yield |
---|---|
With C41H38BFeN3P2; hydrogen In tetrahydrofuran at 20 - 90℃; under 7500.75 Torr; for 27h; Inert atmosphere; | A 94% B 11% |
With formic acid; para-xylene; 1,3-bis(2,4,6-trimethylphenyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium palladium (divinyltetramethyldisiloxane); triethylamine In acetonitrile at 80℃; for 2h; Catalytic behavior; Inert atmosphere; Schlenk technique; Reflux; chemoselective reaction; | |
With C42H44ClN4P2Ru(1+)*Cl(1-); potassium tert-butylate; isopropyl alcohol at 80℃; for 72h; Schlenk technique; Inert atmosphere; | A n/a B 77 %Spectr. |
With hydrogen; iron(II) acetate; diisobutylaluminium hydride In tetrahydrofuran; toluene at 30℃; under 1500.15 Torr; for 3h; stereoselective reaction; | A n/a B n/a |
1-Chloropropane
triphenylphosphine
A
Propylbenzene
B
diphenylphosphinopropane
Conditions | Yield |
---|---|
Stage #1: triphenylphosphine With lithium In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; Stage #2: 1-Chloropropane In tetrahydrofuran at 5 - 50℃; for 6.25h; | A 93.5% B 91.6% |
Cinnamyl acetate
Propylbenzene
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel dichloride In methanol at -20℃; for 0.5h; | 93% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); polystyrene-supported organotin catalyst In N,N-dimethyl acetamide at 80℃; for 6.5h; | 93% |
With indium(III) chloride; sodium tetrahydroborate In acetonitrile at 20℃; for 2h; | 90% |
With triethylsilane; indium(III) chloride; triethyl borane In hexane; dichloromethane at 20℃; for 2h; | 83% |
Multi-step reaction with 2 steps 1: tetrahydrofuran / 0.5 h / 20 °C / Glovebox; Sealed tube; Irradiation 2: sodium methylate / 12 h / 20 °C / Glovebox; Sealed tube; Irradiation View Scheme |
Conditions | Yield |
---|---|
With hydrogen; sodium triethylborohydride In tetrahydrofuran at 23℃; under 30003 Torr; for 20h; Reagent/catalyst; Autoclave; | 92% |
With hydrogen; sodium triethylborohydride In tetrahydrofuran at 23℃; under 30402 Torr; for 70h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 36% |
With hydrogen; sodium triethylborohydride In tetrahydrofuran at 23℃; under 30402 Torr; for 18h; Reagent/catalyst; Glovebox; Inert atmosphere; | 12% |
Conditions | Yield |
---|---|
With formic acid; palladium on activated charcoal In ethanol; benzene for 0.166667h; Heating; Yields of byproduct given; | A n/a B 92% |
With formic acid; palladium on activated charcoal In ethanol; benzene for 0.0833333h; Heating; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; water In methanol at 20℃; for 0.166667h; | 92% |
Conditions | Yield |
---|---|
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran at -78 - 67℃; | 91% |
trimethylstannane
A
3-phenyl-propionaldehyde
C
3-Phenyl-1-propanol
D
Propylbenzene
Conditions | Yield |
---|---|
In benzene-d6 react. of Fe complex and HSnMe3 in benzene, 120°C, 6 h; yields detd. by (1)H-NMR and GL-chromy.; | A <3 B 91% C 91% D <3 |
In benzene-d6 Irradiation (UV/VIS); irradn. of Fe complex and HSnMe3 in benzene for 24 h; yields detd. by (1)H-NMR and GL-chromy.; | A 0% B 0% C <3 D 37% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; water In methanol at 20℃; for 0.25h; | 91% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; aluminium trichloride In tetrahydrofuran for 2h; Heating; | A 90% B 7 % Chromat. |
With sodium tetrahydroborate; aluminium trichloride In tetrahydrofuran for 2h; Ambient temperature; Yield given. Yields of byproduct given; | |
With hydrogen In toluene at 80℃; under 15001.5 Torr; for 24h; Autoclave; chemoselective reaction; | |
With hydrogen In tetrahydrofuran at 50℃; under 15001.5 Torr; for 24h; Autoclave; chemoselective reaction; |
Conditions | Yield |
---|---|
With Ti8O8(14+)*6C8H4O4(2-)*4O(2-)*3.3Li(1+)*0.7Co(2+)*0.7C4H8O*0.7H(1-); hydrogen In neat (no solvent) at 120℃; under 37503.8 Torr; for 18h; | 100% |
With nickel at 220 - 240℃; under 73550.8 Torr; Hydrogenation; | |
With platinum(IV) oxide; acetic acid Hydrogenation; |
Propylbenzene
4-(methoxymethoxy)-4'-methoxybenzophenone
1-(4-methoxymethoxyphenyl)-1-(4-methoxyphenyl)-2-phenylbutan-1-ol
Conditions | Yield |
---|---|
Stage #1: phenylpropane With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium tert-butylate In tetrahydrofuran; hexane at 20℃; for 0.5h; Stage #2: 4-(methoxymethoxy)-4'-methoxybenzophenone In tetrahydrofuran; hexane at -78 - 20℃; for 4.5h; | 97% |
Stage #1: phenylpropane With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium tert-butylate Stage #2: 4-(methoxymethoxy)-4'-methoxybenzophenone | 97% |
Propylbenzene
2,4-dinitro-1-propylbenzene
Conditions | Yield |
---|---|
With nitric acid; Chloroacetic anhydride at 50℃; for 4h; | 96% |
With sulfuric acid; nitric acid at 0 - 20℃; | 89% |
With sulfuric acid; nitric acid | |
With sulfuric acid; nitric acid | |
With sulfuric acid; nitric acid at 0 - 20℃; for 0.5h; |
2-Iodobenzoic acid
Propylbenzene
1-(4-propylphenyl)-1H-1λ3-benzo[b]iodo-3(2H)-one
Conditions | Yield |
---|---|
Stage #1: 2-Iodobenzoic acid With Oxone; sulfuric acid at 5 - 20℃; for 0.5h; Stage #2: phenylpropane In dichloromethane at 5 - 20℃; for 3h; | 94% |
Conditions | Yield |
---|---|
With C20H24B10Cl4FeN6; dihydrogen peroxide In methanol at 20℃; for 6h; | 93% |
With lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); oxygen Kinetics; relative chain propagation rates; | |
With NADPH In dimethyl sulfoxide at 30℃; pH=7.4; Product distribution; Further Variations:; Reagents; | 99 % Chromat. |
Conditions | Yield |
---|---|
With potassium permanganate; Rexyn 101 H ion exchange resin In dichloromethane for 5.45h; Heating; | 93% |
With potassium permanganate on Zeolite beta In 1,2-dichloro-ethane for 96h; Ambient temperature; | 92% |
With sodium bromate; sulfuric acid; silica gel at 20℃; for 3h; | 92% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water In ethyl acetate at 60℃; for 6h; Wohl-Ziegler Bromination; | 93% |
With hydrogen bromide; oxygen In water; ethyl acetate at 20℃; for 10h; Irradiation; | 61% |
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