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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Isoamyl nitrite Manufacturer/High quality/Best price/In stock

Cas:110-46-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and

Isopentyl nitrite

Cas:110-46-3

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Iso-Amyl Nitrite supplier in China

Cas:110-46-3

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co., LTD is a professional research, development and production Cyromazine、lead diacetate trihydrate /Lead acetate trihydrateC、 2-phenylacetamide 、 4-Aminophenyl-1-phenethylpiperidine 、Citric acid monohydrate 、 Citric acid/c

110-46-3 Isoamyl nitrite

Cas:110-46-3

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Iso-Amyl Nitrite

Cas:110-46-3

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Isoamyl nitrite

Cas:110-46-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: Isoamyl nitrite Synonyms: Isoamyl nitrite,97%,stabilized;IsoaMyl nitrite, stabilized, 90% 100GR;IsoaMyl nitrite, 96%, stabilized;ISOPENTYL NITRITE EXTRA PURE STABILIZED;Nitrite isoaMyl acetate (110-46-3) - 2;sopentyl nitr

110-46-3 Isoamyl nitrite

Cas:110-46-3

Min.Order:1 Gram

FOB Price: $8900.0

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

Isoamyl Nitrite Manufacturer 110-46-3 For Anti-angina Drugs

Cas:110-46-3

Min.Order:10 Gram

Negotiable

Type:Other

inquiry

Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

Isoamyl nitrite CAS NO.110-46-3

Cas:110-46-3

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao

Isoamyl nitrite 110-46-3

Cas:110-46-3

Min.Order:1 Kilogram

FOB Price: $16.0 / 20.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Isoamyl nitrite

Cas:110-46-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Isoamyl Nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Isopentyl nitrite

Cas:110-46-3

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colourless or light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceu

Isoamyl nitrite

Cas:110-46-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

High purity Isoamyl nitrite

Cas:110-46-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

Isoamyl nitriteCAS NO.: 110-46-3

Cas:110-46-3

Min.Order:1 Gram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

SAGECHEM/Isoamyl Nitrite/SAGECHEM/Manufacturer in China

Cas:110-46-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Vanz Pharm Co.,Ltd

ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai

Isoamyl nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Isopentyl nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

99%

Isoamyl nitrite

Cas:110-46-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

Iso-Amyl Nitrite

Cas:110-46-3

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Isoamyl nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Isoamyl nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

Isoamyl nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory supply CAS 110-46-3 with competitive price

Cas:110-46-3

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

IsoaMyl Nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

Isoamyl nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

Isoamyl Nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Fandachem Co.,Ltd

Isoamyl nitrite,CAS:110-46-3 from fandachem Application:fine chemical Transportation:by air,by sea,by express

Isoamyl nitrite,CAS:110-46-3 from fandachem

Cas:110-46-3

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Koning Pharmchem Co., Ltd.

Isopentyl nitriteAppearance:yellow liquid Storage:In Shade Package:barrel or Customize Application:chemical research Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)

Isopentyl nitrite

Cas:110-46-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

i-Amyl alcohol
123-51-3

i-Amyl alcohol

isopentyl nitrite
110-46-3

isopentyl nitrite

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite In water at 0℃; for 0.0555556h; Temperature; Large scale;96%
With hydrogenchloride; sodium nitrite In water at 0℃; for 0.0555556h; Temperature; Flow reactor;94%
With nitrogen(II) oxide; potassium hydroxide at 3℃;92.3%
methyl nitrite
624-91-9

methyl nitrite

i-Amyl alcohol
123-51-3

i-Amyl alcohol

A

methanol
67-56-1

methanol

B

isopentyl nitrite
110-46-3

isopentyl nitrite

Conditions
ConditionsYield
In acetonitrile at 25℃; Equilibrium constant;
((isopentyloxy)methyl)benzene
122-73-6

((isopentyloxy)methyl)benzene

A

benzaldehyde
100-52-7

benzaldehyde

B

isopentyl nitrite
110-46-3

isopentyl nitrite

Conditions
ConditionsYield
With zinc(II) nitrate; silica gel In 2,2,4-trimethylpentane for 1h; Heating;A 84 % Chromat.
B 23 % Chromat.
i-pentyl bromide
107-82-4

i-pentyl bromide

silver nitrite

silver nitrite

A

1-nitro-3-methylbutane
627-67-8

1-nitro-3-methylbutane

B

isopentyl nitrite
110-46-3

isopentyl nitrite

isopentyl sulfate potassium

isopentyl sulfate potassium

isopentyl nitrite
110-46-3

isopentyl nitrite

Conditions
ConditionsYield
With nitric acid bei der Destillation;
i-Amyl alcohol
123-51-3

i-Amyl alcohol

nitrosyl tetrafluoroborate

nitrosyl tetrafluoroborate

isopentyl nitrite
110-46-3

isopentyl nitrite

Conditions
ConditionsYield
With sodium carbonate at -10℃;
potassium isopentyl sulfate

potassium isopentyl sulfate

isopentyl nitrite
110-46-3

isopentyl nitrite

Conditions
ConditionsYield
With alkali nitrite
With alkaline earth nitrite
i-Amyl alcohol
123-51-3

i-Amyl alcohol

cis-nitrous acid
7782-77-6

cis-nitrous acid

isopentyl nitrite
110-46-3

isopentyl nitrite

1,3-dihydro-1-methyl-5-phenyl-2H-pyrido<3,4-e>-1,4-diazepin-2-one
112175-39-0

1,3-dihydro-1-methyl-5-phenyl-2H-pyrido<3,4-e>-1,4-diazepin-2-one

isopentyl nitrite
110-46-3

isopentyl nitrite

2,3-dihydro-3-hydroxyimino-1-methyl-5-phenyl-1H-pyrido[3,4-e]-1,4-diazepine-2-one

2,3-dihydro-3-hydroxyimino-1-methyl-5-phenyl-1H-pyrido[3,4-e]-1,4-diazepine-2-one

Conditions
ConditionsYield
With acetic acid In water; ethyl acetate; toluene100%
With acetic acid In water; ethyl acetate; toluene100%
With acetic acid In water; ethyl acetate; toluene100%
With acetic acid In water; ethyl acetate; toluene100%
5-(4-methoxybenzyl)-5H-dibenzo[b,d]azepin-6(7H)-one
847926-44-7

5-(4-methoxybenzyl)-5H-dibenzo[b,d]azepin-6(7H)-one

isopentyl nitrite
110-46-3

isopentyl nitrite

5-(4-methoxybenzyl)-5H-dibenzo[b,d]azepine-6,7-dione-7-oxime
847926-87-8

5-(4-methoxybenzyl)-5H-dibenzo[b,d]azepine-6,7-dione-7-oxime

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran at 0℃; for 1.91667h;100%
1,2,3,4-tetrahydroisoquinoline
635-46-1

1,2,3,4-tetrahydroisoquinoline

isopentyl nitrite
110-46-3

isopentyl nitrite

N-nitroso-1,2,3,4-tetrahydroquinoline
5825-44-5

N-nitroso-1,2,3,4-tetrahydroquinoline

Conditions
ConditionsYield
With 4-(1,1-dimethylethyl)benzoic acid In dichloromethane at 20℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox;100%
isopentyl nitrite
110-46-3

isopentyl nitrite

isovaleraldehyde
590-86-3

isovaleraldehyde

Conditions
ConditionsYield
With iron(III) chloride; 1,1,1,3',3',3'-hexafluoro-propanol at 20℃; for 20h; Catalytic behavior; Time; Inert atmosphere;99%
With boron trifluoride diethyl etherate In diethyl ether for 4h; Ambient temperature;91%
With dimethyl sulfoxide at 70℃; for 6h;90.78%
3-(4-aminophenyl)prop-2-ynenitrile
1005420-89-2

3-(4-aminophenyl)prop-2-ynenitrile

isopentyl nitrite
110-46-3

isopentyl nitrite

3-(4-azidophenyl)prop-2-ynenitrile

3-(4-azidophenyl)prop-2-ynenitrile

Conditions
ConditionsYield
With trimethylsilylazide In ethyl acetate; acetonitrile99%
2-[(4R)-4,5-dihydro-4-phenyl-1,3-oxazolin-2-yl]benzenamine
169776-89-0

2-[(4R)-4,5-dihydro-4-phenyl-1,3-oxazolin-2-yl]benzenamine

isopentyl nitrite
110-46-3

isopentyl nitrite

3-((R)-2-hydroxy-1-phenylethyl)-1,2,3-benzotriazin-4(3H)-one

3-((R)-2-hydroxy-1-phenylethyl)-1,2,3-benzotriazin-4(3H)-one

Conditions
ConditionsYield
In methanol at 20℃;99%
2-[(4R)-4-ethyl-4,5-dihydro-1,3-oxazol-2-yl]aniline

2-[(4R)-4-ethyl-4,5-dihydro-1,3-oxazol-2-yl]aniline

isopentyl nitrite
110-46-3

isopentyl nitrite

3-((R)-1-hydroxybutan-2-yl)-1,2,3-benzotriazin-4(3H)-one

3-((R)-1-hydroxybutan-2-yl)-1,2,3-benzotriazin-4(3H)-one

Conditions
ConditionsYield
In methanol at 20℃;99%
2-(4,5-Dihydro-1,3-oxazol-2-yl)aniline
3416-93-1

2-(4,5-Dihydro-1,3-oxazol-2-yl)aniline

isopentyl nitrite
110-46-3

isopentyl nitrite

3-(2-hydroxyethyl)benzo[d][1,2,3]triazin-4(3H)-one
72553-67-4

3-(2-hydroxyethyl)benzo[d][1,2,3]triazin-4(3H)-one

Conditions
ConditionsYield
In methanol at 20℃;99%
4-(pyridin-3-yl)thiazol-2-amine
30235-27-9

4-(pyridin-3-yl)thiazol-2-amine

isopentyl nitrite
110-46-3

isopentyl nitrite

5-nitroso-4-(pyridin-3-yl)thiazol-2-amine

5-nitroso-4-(pyridin-3-yl)thiazol-2-amine

Conditions
ConditionsYield
With hydrogenchloride In ethanol at 0 - 5℃; for 2.66667h;98%
4-Bromo-2-nitroaniline
875-51-4

4-Bromo-2-nitroaniline

isopentyl nitrite
110-46-3

isopentyl nitrite

4-bromo-1-methylsulfanyl-2-nitro-benzene
345635-46-3

4-bromo-1-methylsulfanyl-2-nitro-benzene

Conditions
ConditionsYield
In Dimethyldisulphide; ethyl acetate97%
3-(acetoxymethyl)-6-methyl-N-(acetyl)aniline
220178-63-2

3-(acetoxymethyl)-6-methyl-N-(acetyl)aniline

isopentyl nitrite
110-46-3

isopentyl nitrite

1-acetyl-6-(acetoxymethyl)indazole
368426-62-4

1-acetyl-6-(acetoxymethyl)indazole

Conditions
ConditionsYield
With potassium acetate; acetic anhydride In chloroform; water95%
methyl 3-amino-2-(t-butylaminosulfonylmethyl)benzoate

methyl 3-amino-2-(t-butylaminosulfonylmethyl)benzoate

isopentyl nitrite
110-46-3

isopentyl nitrite

methyl 3-(t-butylaminosulfonyl)-1H-indazole-4-carboxylate

methyl 3-(t-butylaminosulfonyl)-1H-indazole-4-carboxylate

Conditions
ConditionsYield
With hydrogenchloride; potassium acetate; acetic anhydride In methanol; water; benzene94.1%
4-Bromo-2-methylaniline
583-75-5

4-Bromo-2-methylaniline

isopentyl nitrite
110-46-3

isopentyl nitrite

5-bromo-1H-indazole
53857-57-1

5-bromo-1H-indazole

Conditions
ConditionsYield
With hydrogenchloride; sodium hydroxide; potassium acetate; acetic anhydride In n-heptane; chloroform; water; ethyl acetate94%
hydrogenchloride
7647-01-0

hydrogenchloride

dicarbonyl(η5-carboxycyclopentadienyl)nitrosylchromium

dicarbonyl(η5-carboxycyclopentadienyl)nitrosylchromium

isopentyl nitrite
110-46-3

isopentyl nitrite

(η5-carboxycyclopentadienyl)chlorodinitrosylchromium
1007395-47-2

(η5-carboxycyclopentadienyl)chlorodinitrosylchromium

Conditions
ConditionsYield
In isopropyl alcohol (N2); Schlenk technique; HCl was bubbled through soln. of Cr complex in isopropanol for 10 min; cooled to 0-10°C; nitrite was slowly added; stirred for 40 min; solvent removed (vac.); washed (H2O); dried (vac.); recrystd. (hexane/THF, 5/2, 0°C, 48 h); elem. anal.;94%
tert-butyl [2-amino-5-(pentafluoro-λ6-sulfanyl)phenyl]acetate
1309569-21-8

tert-butyl [2-amino-5-(pentafluoro-λ6-sulfanyl)phenyl]acetate

acetic anhydride
108-24-7

acetic anhydride

isopentyl nitrite
110-46-3

isopentyl nitrite

tert-butyl 1-acetyl-5-(pentafluorosulfanyl)-1H-indazole-3-carboxylate

tert-butyl 1-acetyl-5-(pentafluorosulfanyl)-1H-indazole-3-carboxylate

Conditions
ConditionsYield
Stage #1: tert-butyl [2-amino-5-(pentafluoro-λ6-sulfanyl)phenyl]acetate; acetic anhydride With potassium acetate In toluene at 0 - 20℃; for 0.5h;
Stage #2: isopentyl nitrite In toluene at 80℃; for 12h;
94%
1,2-dimethoxyethane
110-71-4

1,2-dimethoxyethane

methyl 3-bromo-2-oxo-2H-pyran-5-carboxylate
42933-07-3

methyl 3-bromo-2-oxo-2H-pyran-5-carboxylate

anthranilic acid
118-92-3

anthranilic acid

isopentyl nitrite
110-46-3

isopentyl nitrite

methyl 1-bromo-3-naphthoate
5043-29-8

methyl 1-bromo-3-naphthoate

Conditions
ConditionsYield
trichloroacetic acid In toluene for 4h;93%
boron trifluoride diethyl etherate
109-63-7

boron trifluoride diethyl etherate

2,5-difluoroaniline
367-30-6

2,5-difluoroaniline

isopentyl nitrite
110-46-3

isopentyl nitrite

2,5-difluorobenzenediazonium tetrafluoroborate

2,5-difluorobenzenediazonium tetrafluoroborate

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; Inert atmosphere;92%
boron trifluoride-tetrahydrofuran complex
462-34-0

boron trifluoride-tetrahydrofuran complex

4-methoxy-aniline
104-94-9

4-methoxy-aniline

isopentyl nitrite
110-46-3

isopentyl nitrite

4-methoxybenzenediazonium tetrafluoroborate
459-64-3

4-methoxybenzenediazonium tetrafluoroborate

Conditions
ConditionsYield
Stage #1: boron trifluoride-tetrahydrofuran complex; 4-methoxy-aniline In tetrahydrofuran at 0℃; for 0.0833333h;
Stage #2: isopentyl nitrite In tetrahydrofuran at 0℃; for 0.25h;
92%
triphenylmethyl alcohol
76-84-6

triphenylmethyl alcohol

hypophosphorous acid
6303-21-5

hypophosphorous acid

isopentyl nitrite
110-46-3

isopentyl nitrite

tetraphenylmethane
630-76-2

tetraphenylmethane

Conditions
ConditionsYield
With concentrated aqueous hydrochloric acid; sulfuric acid; aniline In ethanol; acetic acid90%
(η5-benzoylcyclopentadienyl)dicarbonylnitrosylchromium

(η5-benzoylcyclopentadienyl)dicarbonylnitrosylchromium

hydrogen bromide
10035-10-6, 12258-64-9

hydrogen bromide

isopentyl nitrite
110-46-3

isopentyl nitrite

(η5-benzoylcyclopentadienyl)bromidodinitrosylchromium(0)

(η5-benzoylcyclopentadienyl)bromidodinitrosylchromium(0)

Conditions
ConditionsYield
In isopropyl alcohol byproducts: CO; (under N2, Schlenk); HBr bubbled through soln. of Cr-complex in isopropanol for 5 min, cooled to 0-10°C with stirring for 15 min, isoamylnitrite added slowly, stirred for 1 h; solvent removed, extd. with CH2Cl2, extract washed with H2O, dried with MgSO4, filtered, concd., dissolved in CH2Cl2, silica gel added, solvent removed under vac., residue added to silica gel column, eluted with hexane/ether (3:1); elem. anal.;90%
In isopropyl alcohol byproducts: CO; HBr bubbled through a Cr-compd. in 2-propanol for 5 min, cooled to 273-283 K with stirring for 20 min, isoamyl nitrite added slowly, stirred for 1 h; concentrated, CH2Cl2 added, filtered, washed with H2O, dried in vac.;90%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

2-[bis-(5-ethyl-furan-2-yl)-methyl]-4,5-dimethoxy-phenylamine
319432-08-1

2-[bis-(5-ethyl-furan-2-yl)-methyl]-4,5-dimethoxy-phenylamine

isopentyl nitrite
110-46-3

isopentyl nitrite

(Z)-1-[4-(5-ethyl-2-furyl)-6,7-dimethoxy-3-cinnolinyl]-1-penten-3-one

(Z)-1-[4-(5-ethyl-2-furyl)-6,7-dimethoxy-3-cinnolinyl]-1-penten-3-one

Conditions
ConditionsYield
In acetonitrile for 0.25h; Diazotisation;89%
hydrochloric acid-dioxane

hydrochloric acid-dioxane

2,3-dihydro-6-methyl-1H-inden-1-one
24623-20-9

2,3-dihydro-6-methyl-1H-inden-1-one

isopentyl nitrite
110-46-3

isopentyl nitrite

6-methyl-1H-inden-1,2(3H)-dione 2-oxime

6-methyl-1H-inden-1,2(3H)-dione 2-oxime

Conditions
ConditionsYield
In ethanol89%
carbon disulfide
75-15-0

carbon disulfide

2-Amino-5-methylbenzoic acid
2941-78-8

2-Amino-5-methylbenzoic acid

isopentyl nitrite
110-46-3

isopentyl nitrite

5-methyl-2-(3-methylbutoxy)-1,3-benzodithiole
67855-55-4

5-methyl-2-(3-methylbutoxy)-1,3-benzodithiole

Conditions
ConditionsYield
In 1,4-dioxane; i-Amyl alcohol; dichloromethane at 20 - 82℃; for 1.75h;88%
hydrogenchloride
7647-01-0

hydrogenchloride

(η5-ethylcyclopentadienyl)dicarbonylnitrosylchromium
1123299-11-5

(η5-ethylcyclopentadienyl)dicarbonylnitrosylchromium

isopentyl nitrite
110-46-3

isopentyl nitrite

chloro(η5-ethylcyclopentadienyl)dinitrosylchromium

chloro(η5-ethylcyclopentadienyl)dinitrosylchromium

Conditions
ConditionsYield
Stage #1: hydrogenchloride; (η5-ethylcyclopentadienyl)dicarbonylnitrosylchromium In water; isopropyl alcohol at 0℃; for 0.166667h; Inert atmosphere; Schlenk technique;
Stage #2: isopentyl nitrite In water; isopropyl alcohol at 0 - 10℃; for 0.5h; Inert atmosphere; Schlenk technique;
87.8%
hydrogenchloride
7647-01-0

hydrogenchloride

(η5-benzoylcyclopentadienyl)dicarbonylnitrosylchromium

(η5-benzoylcyclopentadienyl)dicarbonylnitrosylchromium

isopentyl nitrite
110-46-3

isopentyl nitrite

(η5-benzoylcyclopentadienyl)chlorodinitrosylchromium

(η5-benzoylcyclopentadienyl)chlorodinitrosylchromium

Conditions
ConditionsYield
Stage #1: hydrogenchloride; (η5-benzoylcyclopentadienyl)dicarbonylnitrosylchromium In isopropyl alcohol for 0.25h; Inert atmosphere; Schlenk technique;
Stage #2: isopentyl nitrite In isopropyl alcohol at 0 - 10℃; for 0.5h; Inert atmosphere; Schlenk technique;
87.5%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

7-[bis-(5-ethyl-furan-2-yl)-methyl]-2,3-dihydro-benzo[1,4]dioxin-6-ylamine
319432-10-5

7-[bis-(5-ethyl-furan-2-yl)-methyl]-2,3-dihydro-benzo[1,4]dioxin-6-ylamine

isopentyl nitrite
110-46-3

isopentyl nitrite

(Z)-1-[4-(5-ethyl-2-furyl)-7,8-dihydro[1,4]dioxino[2,3-g]cinnolin-3-yl]-1-penten-3-one

(Z)-1-[4-(5-ethyl-2-furyl)-7,8-dihydro[1,4]dioxino[2,3-g]cinnolin-3-yl]-1-penten-3-one

Conditions
ConditionsYield
In acetonitrile for 0.25h; Diazotisation;87%
4-bromo-2-trifluoromethyl-aniline
445-02-3

4-bromo-2-trifluoromethyl-aniline

isopentyl nitrite
110-46-3

isopentyl nitrite

(4-bromo-2-(trifluoromethyl)phenyl)(methyl)sulfane
300356-31-4

(4-bromo-2-(trifluoromethyl)phenyl)(methyl)sulfane

Conditions
ConditionsYield
In Dimethyldisulphide; ethyl acetate87%
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